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61. 发明专利

JPH06300742A MEASURING APPARATUS FOR FREE CYANOGEN 失效
公开(公告)号：JPH06300742A
公开(公告)日：1994-10-28
申请号：JP13850693
申请日：1993-06-10
申请人： YOKOGAWA ELECTRIC CORP
发明人： MURAYAMA TAKESHI , OHARA HISAKI , AOYAMA YOSHIJI
IPC分类号： G01N30/14 , G01N30/26 , G01N30/88
摘要： PURPOSE:To measure free cyanogen with high selectivity and with high sensitivity by a method wherein a second changeover valve is changed over at a timing at which the peak of the free cyanogen is passed. CONSTITUTION:The standard solution at 1ppm of, e.g. CN is made to flow to a metering pipe 3 via a fourth changeover valve 13. In addition, an eluate is made to flow to a detector 6 via a first pump 1, a third changeover valve 10, a first changeover valve 2, a separating column 4, a second changeover valve 16 and a mixing coil 9, and a pH regulating liquid is made to flow to the side of the coil 9 from a second pump 8. Then, the flow passage of the valve 2 is changed over at a prescribed timing, the eluate takes into the standard solution in the metering pipe 3, it flows into the column 4, and CN ions are separated 4 and sent out to the detector 6. At this time, the passage time through the valve 16 of the CN ions is decided by subtracting a required time, and the valve 16 is changed over so as to match their passage timing. Then, a sample is made to flow to the metering pipe 3 via the valve 13, and the valves 2, 16 are changed over at the same timing. Thereby, only the CN ions in a plurality of components contained in the sample can be sent to the detector 6.

62. 发明专利

JPH06229996A METHOD AND DEVICE FOR GENERATING VOLATILE MATTER FROM MATRIX BY MICROWAVE IRRADIATION 失效
公开(公告)号：JPH06229996A
公开(公告)日：1994-08-19
申请号：JP2248093
申请日：1993-02-10
申请人： CANADA
发明人： JIEI AARU JIYOSURIN PEA
IPC分类号： G01N1/22 , B01D1/00 , B01D19/00 , B01J3/00 , B01J19/12 , G01N30/02 , G01N30/06 , G01N30/12 , G01N30/14
摘要： PURPOSE: To quickly separate volatile component(s) by irradiating a specimen with a microwave energy. CONSTITUTION: A vessel 10 transmits microwaves generated by a microwave generating device 12, and with them a sample contained in the vessel 10 is bombarded. The vessel 10 is sealed air-tightly with a lid 16. The amount of microwaves is controlled so that volatilation of prescribed component(s) or turning the desired substance into the supercritical condition maximizes in the shortest time and without ill affecting the component concerned. Therefore, appropriate parameters based upon the nature of the component, for example the absolute of dielectric constant, thermal capacity, or the like., are selected, and on the basis thereof the microwave energy is controlled. When volatilized substance is generated, a semi-permeable membrane 18 moves in compliance with increase in the pressure so that the gaseous phase is separated from the liquid or solid phase. The volatilized substance having permeated the membrane 18 is sent to a sampling tube 24 via a conduitpipe 20 and sampled out by a relief valve 22. Further the volatized substance is forwarded to an analyzing means 26 such as a gas chromatograph, infrared spectral analyzing device, or the like.

63. 发明专利

JPH0650951A ION ANALYSIS METHOD 失效
公开(公告)号：JPH0650951A
公开(公告)日：1994-02-25
申请号：JP4110593
申请日：1993-03-02
申请人： DIONEX CORP
发明人： KURISUTOFUAA ANDORIYUU POORU , ROZANNU UIRIAMUSON SURINGUSUBI , JIYON REIMONDO SUTEIRIAN , RISUZAADO GAJIEKU
IPC分类号： B01D15/04 , B01D15/08 , B01D61/24 , G01N30/02 , G01N30/14 , G01N30/26 , G01N30/38 , G01N30/60 , G01N30/84 , G01N30/96
摘要： PURPOSE: To suppress the electrolyte of an eluate in a flow by feeding an eluated effluent and a regenerant simultaneously through the flow channel of a suppressor unit, including an ion exchange position having outer surface of the same charge as the ion of a membrane sheet and a self-structure arranged in an effluent flow channel. CONSTITUTION: A sample passes through a solvent solution which passes through a sample injection valve 13. A solution separating from a chromatographic column 10 is directed toward a suppressor unit 11 where an electrolyte is converted into a weak conductive state. An effluent is treated in the suppressor unit 11, along with separated ions and passes through a conductivity cell 12. When an ion species is present in the cell 12, an electrical signal proportional to the quantity of ion substance is generated and the concentration of the ion species is detected. A regenerant is is then fed to a regenerant channel in an ion exchange membrane 17. Regenerant from a reservoir 16 is passed through a shunt valve 19 and separated into ducts 20, 22 before being discharged through a regenerant passage. An effluent flows from the column 10 to the membrane 17, thence to a conductivity detector 12.

64. 实用新型

JPH063453U 失效
公开(公告)号：JPH063453U
公开(公告)日：1994-01-18
申请号：JP710693
申请日：1993-02-25
IPC分类号： G01N33/68 , B01D29/01 , B01D29/05 , B01D29/085 , B01D29/46 , B01D29/62 , B01D29/66 , B01J19/00 , B01J19/24 , B04B7/16 , C40B40/10 , C40B60/14 , G01N30/00 , G01N30/14 , G01N30/46 , G01N30/60 , G01N33/48

65. 发明专利

JPH06500402A 失效
公开(公告)号：JPH06500402A
公开(公告)日：1994-01-13
申请号：JP50997292
申请日：1992-03-20
IPC分类号： B01D15/08 , G01N27/447 , G01N30/14 , G01N30/46 , G01N30/52 , G01N30/62 , G01N30/80 , G01N30/82 , G01N30/86 , G01N30/88

66. 发明专利

JPH05506715A 失效
公开(公告)号：JPH05506715A
公开(公告)日：1993-09-30
申请号：JP50671191
申请日：1991-04-02
IPC分类号： G01N1/00 , G01N1/02 , G01N1/24 , G01N1/28 , G01N1/34 , G01N30/00 , G01N30/04 , G01N30/06 , G01N30/12 , G01N30/14 , G01N30/18 , G01N30/24 , G01N33/18 , G01N35/04 , G01N35/10

67. 发明专利

JPH05240846A 失效
公开(公告)号：JPH05240846A
公开(公告)日：1993-09-21
申请号：JP4310292
申请日：1992-02-28
申请人： YOKOGAWA ELECTRIC CORP
发明人： KUMAGAI HIROKI
IPC分类号： G01N30/02 , G01N30/14
摘要： PURPOSE:To obtain a cation measuring method, which can simply measure cations contained in water-soluble organic solvent highly accurately. CONSTITUTION:A cation capturing column 8 filled with cation exchange resin is arranged between a sample introducing part and a separating column part. After the cations in a sample are captured, pure water is applied to wash out the water-soluble organic solvent. Thereafter, the cations, which are captured in the cation capturing colum 8, are introduced into a separating column part 10 with eluate.

68. 发明专利

JPH04305255A METHOD OF USING POLYTETRAALKYL AMMONIUM CONTAINING LIGAND BONDED WITH INORGANIC CARRIER AND POLYTRIALKYL AMINE FOR REMOVING DESIRED ION FROM SAID SUBSTANCE AND SOLUTION AND CONCENTRATING SOLUTION 失效
公开(公告)号：JPH04305255A
公开(公告)日：1992-10-28
申请号：JP28956591
申请日：1991-10-09
申请人： BURAIGAMU YANGU UNIV
发明人： RON BURIYUUNINGU , BURAION JIEI TAABETSUTO
IPC分类号： B01J20/26 , B01J20/22 , B01J20/32 , B01J41/04 , B01J41/14 , B01J45/00 , C02F1/42 , G01N30/14
摘要： PURPOSE: To remove desired ions from a source soln. containing larger concn. of other ions including H by allowing the source soln. to contact with a compd. containing the polytetraalkylammonium and/or polytrialkylamine containing the ligand covalently bonded through an org. spacer silicon group to a solid inorg. support. CONSTITUTION: The source soln. is brought into contact with the compd. containing the polytetraalkylammonium and/or polytrialkylamine containing the ligand covalently bonded through the org. spacer silicon group to the solid inorg. support SS. One example of the polytetraalkylammonium containing the ligand covalently bonded to the solid inorg. support SS is expressed by the formula. In such a way. the removal and the concentration of the desired ion (e.g.; PtCl6 ) from the source soln. containing larger concn. of other ions including H is executed.

69. 发明专利

JPH04274757A METHOD AND APPARATUS FOR ANALYZING ION SPECIES 失效
公开(公告)号：JPH04274757A
公开(公告)日：1992-09-30
申请号：JP3593791
申请日：1991-03-01
申请人： YOKOGAWA ELECTRIC CORP
发明人： MATSUURA TAMIZO , HANAOKA YUZURU
IPC分类号： G01N30/02 , G01N30/08 , G01N30/14
摘要： PURPOSE:To easily confirm performance of respective columns for concentrating, cutting and separating by concentrating sample by means of a first switch valve and removing interfering components by means of a second switch valve. CONSTITUTION:A first switch valve 5 is turned ON, and an internal flow path is changed to connection indicated by broken lines. A pump 3a is driven, and low concentration sample in a tank 1a is led to a concentration column 5g of the first switch valve 5 to be concentrated and retained. The first switch valve 5 is turned OFF and the internal flow path is returned to connection indicated by solid lines, wherein eluant which has passed through injectors 4a, 4b carries the sample concentrated and retained in the concentration column 5g to a cutting column 6g of a second switch valve 6. The second switch valve 6 is turned ON when unnecessary components in the sample is assumed to have reached the cutting column 6g so as to change the internal flow path to the connection indicated by the broken lines. Components of the sample concentrated and retained in the concentration column 5g which have not been collected into the cutting column are carried to a separation column 7 to be separated.

70. 发明专利

JPH04254756A GAS CHROMATOGRAPH 失效
公开(公告)号：JPH04254756A
公开(公告)日：1992-09-10
申请号：JP5626791
申请日：1991-02-06
申请人： SHIMADZU CORP
发明人： SAITO HISASHI
IPC分类号： G01N30/14
摘要： PURPOSE:To analyze a sample material of very low concentration contained in a solvent, by gas chromatography. CONSTITUTION:A precolumn 9 connected with a septum 5 at one end and with a column 2 for analysis at the other, a heating tank 1 heating the precolumn 9 discretely and a detector 17 for gas chromatograph connected to a discharge end of the column 2 for analysis are provided. A carrier gas supply port 15 is provided on the inflow port side of the column 2 for analysis, while an exhaust port 14 for discharging a solvent is provided between an outflow port of the precolumn 9 and the carrier gas supply port 15, and a sample prepared by diluting a sample material with the solvent in a large quantity is injected directly into the precolumn 9 by a microsyringe or the like, so as to ensure a high precision in determination. The solvent vaporized in the precolumn 9 is discharged outside a system from the exhaust port 14. Thereafter the temperature of the heating tank 1 is made to rise rapidly and a sample material component in the precolumn 9 is injected into the column 2 for analysis in a short time. Thereby the sample material component contained in the sample of a large quantity is injected into the column 2 for analysis in a concentrated manner without bringing forth expansion.

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