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    • 52. 发明专利
    • METHOD FOR GROWING SINGLE CRYSTAL
    • JPH08295594A
    • 1996-11-12
    • JP11903895
    • 1995-04-21
    • TDK CORP
    • OIDO ATSUSHIYAMAZAWA KAZUTO
    • C30B19/08C30B29/28H01F41/28
    • PURPOSE: To provide a single crystal film excellent in quality by using a furnace having a structure packed with heat resistant insulator partially shielding heat on side face of a crucible for growing a single crystal. CONSTITUTION: A platinum crucible 5 for growing a single crystal is housed in an alumina crucible supported on a crucible mount 4 and heat resistant insulators 7 such as ZrO2 or the like are packed around the platinum crucible 5. Next, a magnetic garnet constituting material which is obtained by blending Fe2 O3 , B2 O3 , PbO, Bi2 O3 , Ga2 O3 , Y2 O3 and La2 O3 or the like in a prescribed ratio, is filled up in the platinum crucible 5 and furnace temperature is raised up to about 1000 deg.C to melt and stir the materials in the platinum crucible 5. After that, temperature of the melt is fallen to 700-800 deg.C at a specified temperature discending velocity and by growing for about 5-20 hours on a substrate such as an MgZr-substituted Cd3 Ga5 O12 while revolving the substrate, magnetic garnet single crystal film of a specified thickness having (YLaBi)3 (FeGa)5 O12 composition and small in half value width (ΔH) is obtained.