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41. 发明专利

JP2004002742A Solid titanium catalyst component for olefin polymerization, olefin polymerization catalyst and method for polymerization of olefin 审中-公开
公开(公告)号：JP2004002742A
公开(公告)日：2004-01-08
申请号：JP2003080819
申请日：2003-03-24
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： MATSUNAGA KAZUHISA , NAKANO MASAO , OGISAWA MASAAKI , TSUTSUI TOSHIYUKI
IPC分类号： C08F4/654 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide a solid titanium catalyst component for olefin polymerization having high activity and giving an olefin (co)polymer having high stereospecificity, an olefin polymerization catalyst containing the component and an olefin polymerization method.
SOLUTION: The solid titanium catalyst component (S) containing titanium, magnesium, a halogen and an electron donor (b) is produced either by (A) contacting a solid addition product of a magnesium compound and an electron donor (a), another electron donor (b) and a liquid titanium compound in the presence of an inert hydrocarbon solvent in suspended state or by (B) contacting the above components in several separated steps. The olefin polymerization catalyst contains the solid titanium catalyst component (S) and an organic metal compound catalyst component (M) containing a metal selected from the group I to group III elements of the periodic table.
COPYRIGHT: (C)2004,JPO

42. 发明专利

JP2003313218A Multi-stage manufacturing method for olefin 审中-公开
标题翻译：油脂多级制造方法
公开(公告)号：JP2003313218A
公开(公告)日：2003-11-06
申请号：JP2002117099
申请日：2002-04-19
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TSUTSUI TOSHIYUKI , TAKAHASHI MAMORU , MATSUDA SHOTARO
IPC分类号： C08F4/64 , C08F4/6592 , C08F210/16
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method for an ethylene copolymer composition from which a film being excellent in moldability, and transparency and mechanical strengths, can be produced.
SOLUTION: A multi-stage manufacturing method for an olefin comprises the following steps [I] and [II]. The step [I] comprises copolymerizing ethylene and an α-olefin in the presence of a catalyst [d-1] carrying M
1 L
1
x [wherein M
1 is a group IVb transition metal; and at least two of L
1 are each a Cp group (means a cyclopentadienyl group) or a 1-10C hydrocarbon group-substituted Cp group] and [b] an organic aluminumoxy compound, or the like, on [c] a carrier to produce a copolymer (A). The step [II] comprises copolymerizing the ethylene, or the ethylene and the α-olefin in the presence of the above (A) and adding a catalyst [d-2] carrying M
2 L
2
x or M
3 L
3
x (wherein M
2 and M
3 are each the group IVb transition metal; L
2 is a crosslinking type Cp group, and at least two of L
3 are each a Cp group having 2-5 of an Me group (Me means a methyl group) or an Et group (Et means an ethyl group) on [c] the carrier to produce a copolymer (B).
COPYRIGHT: (C)2004,JPO
摘要翻译：要解决的问题：提供一种乙烯共聚物组合物的制造方法，由此可以制备成型性优异的膜，并且具有机械强度。解决方案：用于烯烃的多级制备方法包括以下步骤[I]和[II]。步骤[I]包括在载体为M 1 SP 1 / SP SP 1的催化剂[d-1]存在下共聚乙烯和α-烯烃 >其中M 1 是IVb族过渡金属; 并且L 1 中的至少两个各自为Cp基（意指环戊二烯基）或1-10C烃基取代的Cp基]和[b]有机铝氧基化合物等，在[c]载体上制备共聚物（A）。步骤[II]包括在上述（A）的存在下使乙烯或乙烯与α-烯烃共聚，并加入载有M 2的催化剂[d-2] 2 x 或M 3 L 3 x （其中M 2 和M 3 分别为IVb族过渡金属; L 2 为交联型Cp基团，L 3 中的至少两个为每个具有2-5个Me基团（Me表示甲基）或Et基团（Et表示乙基）的Cp基团在[c]载体上以产生共聚物（B）。版权所有（C） C）2004，JPO

43. 发明专利

JP2003012712A Method for producing ethylenic polymer composition, particle of the ethylenic polymer composition, and film obtained from the particle of the composition 有权
标题翻译：乙烯聚合物组合物的生产方法，乙烯聚合物组合物的颗粒和由组合物颗粒获得的膜
公开(公告)号：JP2003012712A
公开(公告)日：2003-01-15
申请号：JP2002119418
申请日：2002-04-22
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TSUTSUI TOSHIYUKI , YASHIKI TSUNEO , FUNAHARA YASUO
IPC分类号： C08J5/18 , C08F2/44 , C08F4/658 , C08F210/16 , C08F255/02
摘要： PROBLEM TO BE SOLVED: To obtain an ethylenic polymer composition (particles) excellent in particle properties, scarcely causing sintering, and excellent in moldabitity, to provide a method for efficiently producing the particles of the composition, and to prepare a film having small unevenness of thickness and excellent in tear strength. SOLUTION: This method for producing the ethylenic polymer composition comprises using a catalyst which contains a component obtained by bringing a liquid magnesium compound into contact with a liquid titanium compound in the presence of an organic silicon compound, and further includes (I) a process for producing an ethylene (co)polymer (i) the intrinsic viscosity ([η]) of which is at least 1.5 times the [η] of an ethylene (co)polymer (ii) and (II) a process for producing the ethylene (co)polymer (ii) the [η] of which is 0.3-3 dl/g, wherein the process (II) is conducted in the presence of the polymer (i), or the process (I) is conducted in the presence of the polymer (ii), so that the ethylenic polymer composition having an [η] of 1-6 dl/g and a density of >=0.94 g/cm is produced.
摘要翻译：要解决的问题为了获得颗粒性能优异，几乎不引起烧结并且具有优异的成型性的乙烯聚合物组合物（颗粒），可以提供有效地制备组合物颗粒的方法，并制备具有小的不均匀性的膜厚度和撕裂强度优异。解决方案：用于制备乙烯类聚合物组合物的方法包括使用含有在有机硅化合物存在下使液态镁化合物与液体钛化合物接触而获得的成分的催化剂，还包括（I）产生乙烯（共）聚合物（i）其特性粘度（[η]）至少为乙烯（共）聚合物（ii）的[η]的1.5倍和（II）乙烯的制备方法共聚）聚合物（ⅱ）[η]为0.3-3dl / g，其中方法（II）在聚合物（i）的存在下进行，或者方法（I）在聚合物（ⅱ），使得[η]为1-6dl / g，密度> 0.94g / cm 3的乙烯类聚合物组合物。

44. 发明专利

JP2003147010A METHOD FOR PRODUCING ETHYLENIC WAX 审中-公开
公开(公告)号：JP2003147010A
公开(公告)日：2003-05-21
申请号：JP2001347360
申请日：2001-11-13
申请人： MITSUI CHEMICALS INC
发明人： TSUTSUI TOSHIYUKI , OKAWA KAZUNORI
IPC分类号： C08F4/645 , C08F4/646 , C08F4/6592 , C08F110/02 , C08F210/16
摘要： PROBLEM TO BE SOLVED: To provide both an ethylenic wax having a narrow molecular weight distribution and further a narrow molecular weight distribution and composition distribution when applied to copolymerization of ethylene with a >=3C olefin and a method for efficiently producing the ethylenic wax. SOLUTION: This method for producing the ethylenic wax comprises homopolymerizing ethylene or copolymerizing the ethylene with the >=3C olefin in the presence of a catalyst for polymerizing an olefin comprising (A) a group IVb transition metal compound of the periodic table in which a polydentate coordinating compound having at least 2 mutually different cycloalkadienyl groups or a substitution product thereof is bound through a hydrocarbon group or silylene group or a substituted silylene group as a ligand, (B) a compound reactive with (A) and forming an ion pair and (C) an organoaluminum compound. Thereby, an ethylene (co)polymer having

45. 发明专利

JPH1184721A THERMALLY FIXABLE ELECTROPHOTOGRAPHIC DEVELOPER 失效
公开(公告)号：JPH1184721A
公开(公告)日：1999-03-30
申请号：JP33734297
申请日：1997-12-08
申请人： MITSUI CHEMICALS INC
发明人： TOYODA HIDEO , SAKAI HIDENORI , TSUTSUI TOSHIYUKI , MORISONO KENICHI
IPC分类号： G03G9/087 , C08L23/08
摘要： PROBLEM TO BE SOLVED: To provide a thermally fixable electrophotographic developer excellent in releasability particularly at the time of low energy fixation, blocking resistance and fixability, not causing offsetting phenomenon or contaminating a carrier, a photoreceptor, a heat roll, etc., and therefore suitable for use as an electrostatic toner. SOLUTION: This thermally fixable electrophotographic developer contains a bonding resin, a colorant and a releasing agent which is an ethylene.arom. vinyl compd. copolymer obtd. by copolymerizing ethylene with an arom. vinyl compd. in the presence of a metallocene catalyst or further degrading the resultant copolymer by heating.

46. 发明专利

JPH10251334A ETHYLENIC POLYMER 失效
公开(公告)号：JPH10251334A
公开(公告)日：1998-09-22
申请号：JP5619697
申请日：1997-03-11
申请人： MITSUI CHEMICALS INC
发明人： YANO KATSUNORI , TAKAHASHI MAMORU , TSUTSUI TOSHIYUKI , YAMAMOTO KUNIO
IPC分类号： C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/02 , C08F210/16
摘要： PROBLEM TO BE SOLVED: To obtain an ethylenic polymer excellent in moldability and giving films excellent in transparency and mechanical strength. SOLUTION: This ethylenic polymer is ethylene homopolymer or the copolymer of ethylene with a 4-20C α-olefin, and has the following characteristics. A density (d) is 0.880-0.980g/cm . A melt flow rate(MFR) is 0.01-200g/10min under a load of 2.16kg at 190 deg.C. A temperature [Tm( deg.C)] at the largest peak position in a heat absorption curve measured by a differential scanning calorimeter and the density (d) satisfy the inequality: Tm 2.2×MFR . An intrinsic viscosity [[η](dl/g)] measured in decalin at 135 deg.C and a melt flow rate (g/10min) satisfy the inequality: 2,00×MFR 1.58×MFR .

47. 发明专利

JP2003231716A PART FOR AUTOMOBILE INDUSTRY AND INDUSTRIAL RUBBER PRODUCT 审中-公开
公开(公告)号：JP2003231716A
公开(公告)日：2003-08-19
申请号：JP2003072483
申请日：2003-03-17
申请人： MITSUI CHEMICALS INC
发明人： KAWASAKI MASAAKI , OKADA KEIJI , TOJO TETSUO , AINE TOSHIHIRO , TSUTSUI TOSHIYUKI , NAKAHAMA HIDENARI
IPC分类号： C08K3/00 , C08F210/02 , C08F210/04 , C08F210/18 , C08K5/00 , C08L23/00 , C08L101/00
摘要： PROBLEM TO BE SOLVED: To provide an ethylene/α-olefin/non-conjugate polyene random copolymer obtained by random copolymerizing ethylene, a≥3C α-olefin, and a non- conjugated polyene with high activity and high conversion rate of the α-olefin, and the copolymer has narrow compositional distribution and excellent mechanical properties, low temperature flexibility. SOLUTION: This parts for the automobile industry or industrial rubber product is characterized by containing an ethylene/α-olefin/non-conjugated polyene random copolymer having a specific composition, iodine value, intrinsic viscosity, intensity ratio D (Tαβ/Tαα), B-value and glass transition temperature Tg. The vulcanizable rubber composition containing ethylene/α-olefin/non- conjugate polyene random copolymer is excellent in mechanical strength, weatherability, ozone resistance, processability, etc., as well as excellent in cold resistance (low temperature flexibility) and heat resistance, and thermal resistance. The parts used in the automobile industry or rubber products for industrial use are excellent in above mentioned features. COPYRIGHT: (C)2003,JPO

48. 发明专利

JP2003192718A CATALYST AND METHOD FOR POLYMERIZING OLEFIN 审中-公开
公开(公告)号：JP2003192718A
公开(公告)日：2003-07-09
申请号：JP2001394251
申请日：2001-12-26
申请人： MITSUI CHEMICALS INC
发明人： TSUTSUI TOSHIYUKI , YASHIKI TSUNEO , TANI MASAZUMI
IPC分类号： C08F4/654 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide an olefin polymerization catalyst for manufacturing, at a high polymerization activity, a polyolefin that has little amount of decane- soluble components and excellent stereoregularity, and to provide a method for polymerizing an olefin using this olefin polymerization catalyst. SOLUTION: The olefin polymerization catalyst comprises (A) a solid titanium catalyst ingredient containing magnesium, titanium, a halogen and a polyether, (B) an organoaluminum compound, and (C) a monoalkoxysilane compound represented by R a 3 Si(OR b ) (wherein R a is an alkyl group, a cycloalkyl group, an aryl group or an aralkyl group; and OR b is a methoxy group or an ethoxy group). An olefin may be prepolymerized with an olefin polymerization catalyst comprising the catalyst ingredient (A), (B) and optionally, (D) an electron donor. COPYRIGHT: (C)2003,JPO

49. 发明专利

JP2000136208A POLYMERIZATION CATALYST FOR OLEFIN AND PRODUCTION OF CATALYST AND OLEFIN POLYMER 失效
公开(公告)号：JP2000136208A
公开(公告)日：2000-05-16
申请号：JP31140198
申请日：1998-10-30
申请人： MITSUI CHEMICALS INC
发明人： MAKIO HARUYUKI , TSUTSUI TOSHIYUKI
IPC分类号： C08F4/64 , C08F4/605 , C08F4/6592 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To obtain the subject catalyst capable of efficiently producing a granular olefin polymer having a high bulk density and a narrow particle size distribution by pre-polymerizing a specific monomer in the presence of a porous carrier and a specific compound, etc., in a specific solvent. SOLUTION: This catalyst for polymerizing an olefin is obtained by pre- polymerizing (A) a monomer having a polymerizable double bond in the presence of (B) a porous carrier, (C) a transition metal compound, (D) an organic boron compound and/or (E) an organoaluminum compound in (F) a medium in which the ingredient C does not dissolve. As the ingredient A, an α-olefin, a polar group-containing compound, a vinyl compound, a polyene compound, etc., are cited. As the ingredient B, a carrier, etc., in which a polymer is filled in pores, is preferably used. As the ingredient C, a compound, etc., containing a transition metal of the 4th group of the periodic table, is preferably used. As the ingredient F, a fluorine-containing organic compound, etc., are cited.

50. 发明专利

JPH10282713A THERMAL FIXING TYPE ELECTROPHOTOGRAPHIC DEVELOPER 失效
公开(公告)号：JPH10282713A
公开(公告)日：1998-10-23
申请号：JP8920997
申请日：1997-04-08
申请人： MITSUI CHEMICALS INC
发明人： TOYODA HIDEO , SAKAI HIDENORI , SUGIMURA KENJI , TSUTSUI TOSHIYUKI
IPC分类号： G03G9/08 , G03G9/087
摘要： PROBLEM TO BE SOLVED: To provide a thermal fixing type electrophotographic developer excellent in meltability at a low temp., releasability in thermal fixing, particularly releasability and anti-blocking property in low temp. fixing, free from offset phenomenon and the contamination of a carrier, a photoreceptor, a heating roller or the like and then, capable of being used as the essential component of an electrostatic toner. SOLUTION: The developer contains a polyolefin wax (A) having a weight average molecular weight(MW) of 3,000-50,000 found by a gel permeation chromatography(GPC) and containing 0.2-0.8 mol% different kind bond caused by no 1,2-insertion reaction in polymerizing an α-olefin of a raw material monomer, a binder (B) and a coloring agent (C).

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