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31. 发明专利

JP2002193913A METHOD FOR PRODUCING SULFAMOYLPHENOL COMPOUND 失效
公开(公告)号：JP2002193913A
公开(公告)日：2002-07-10
申请号：JP2000398675
申请日：2000-12-27
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI
IPC分类号： C07C303/38 , C07C311/29
摘要： PROBLEM TO BE SOLVED: To provide a method for producing sulfamoylphenol compound in the short process in high yield. SOLUTION: The sulfamoylphenol compound shown by general formula I (wherein, X is an atom or a group which can be substituted by a benzene ring; m is an integer of 0-4; R1 and R2 are each independently H, an alkyl group or an aryl group, wherein, R1 and R2 may combine with each other to form five to seven membered ring along with N; M is hydrogen or a cation) is produced by reacting a phenolsulfonate compound shown by general formula II with a halogenation agent using no solvent or organic solvent excluding halogen-based organic solvent, and then reacting the product with an amine compound shown by general formula III.

32. 发明专利

JP2002187954A PRODUCTION METHOD FOR CELLULOSIC POLYMER 失效
公开(公告)号：JP2002187954A
公开(公告)日：2002-07-05
申请号：JP2001040751
申请日：2001-02-16
申请人： FUJI PHOTO FILM CO LTD
发明人： SATO TADAHISA , YAMAKAWA KAZUYOSHI , MATSUOKA MITSUYUKI , ONISHI HIROSHI , TSUJIMOTO TADAHIRO
IPC分类号： C08B3/06 , C08J3/11 , C08J3/14
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an easily soluble cellulosic polymer which is highly safe, loads the environment little, and can reduce the investment in plant and equipment; and a method for producing a cellulosic polymer solution which maintains safety, solves the problem with environmental load, and is excellent in the state of being dissolved. SOLUTION: A cellulosic polymer solution is produced by dissolving a raw material polymer in an organic non-chlorinous solvent at a temperatures and pressure belonging to a subcritical to supercritical region. After the raw material polymer is dissolved, the solvent is removed to give a powder of the polymer.

33. 发明专利

JP2002003465A METHOD FOR PRODUCING SULFONIC ACID HALIDE COMPOUND 失效
公开(公告)号：JP2002003465A
公开(公告)日：2002-01-09
申请号：JP2000188371
申请日：2000-06-22
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI , ASANUMA NAOKI , MOTOKI MASUSHI
IPC分类号： C07C303/02 , C07C309/88
摘要： PROBLEM TO BE SOLVED: To provide a new method for producing a sulfonic acid halide compound containing a hydroxyl group in the molecule by a short process in a high yield. SOLUTION: This method for producing a sulfonic acid halide compound containing a hydroxyl group in the molecule comprises reacting an alkali metal salt of a sulfonic acid compound containing a hydroxyl group in the molecule with an ammonium salt and then reacting the reaction product with a halogenating agent.

34. 发明专利

JP2001213902A METHOD FOR DECOMPOSING CELLULOSE ACETATE SUING WATER AND/OR ALCOHOLS 失效
公开(公告)号：JP2001213902A
公开(公告)日：2001-08-07
申请号：JP2000024364
申请日：2000-02-01
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI , SATO TADAHISA
IPC分类号： C08B3/24 , C08L101/16
摘要： PROBLEM TO BE SOLVED: To provide a method for decomposing a cellulose acetate to recyclable cellulose or a highly biodegradable sugar using water or an alcohol. SOLUTION: The method for decomposing a cellulose acetate comprises solvolysis of cellulose acetate using water and/or an alcohol in an amount having a pressure of 1 MPa or more at 200 deg.C.

35. 发明专利

JP2001213901A METHOD FOR MANUFACTURING CELLULOSE ACETATE 失效
公开(公告)号：JP2001213901A
公开(公告)日：2001-08-07
申请号：JP2000024360
申请日：2000-02-01
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI , MATSUOKA MITSUYUKI , SATO TADAHISA
IPC分类号： C08B3/06
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a cellulose acetate suitable for preparing a cellulose acetate solution (dope) in a milder condition using an organic solvent other than methylene chloride. SOLUTION: In the method for manufacturing a cellulose acetate comprising using cellulose as a raw material and subjecting to an acetylation reaction to produce a cellulose acetate, an acetic ester is used as an acetylating agent.

36. 发明专利

JP2001089426A NEW ACETYLENE COMPOUND 失效
公开(公告)号：JP2001089426A
公开(公告)日：2001-04-03
申请号：JP26064499
申请日：1999-09-14
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI
IPC分类号： C07C211/54 , C07C211/56 , C07C215/80 , C07C217/84 , C07C217/90 , C07C223/06 , C07C225/22 , C07C229/56 , C07C229/60 , C07C255/58 , C07C317/36 , C08G73/10
摘要： PROBLEM TO BE SOLVED: To provide a new acetylene compound useful as a synthetic intermediate for thermosetting resins, liquid crystal materials, non-linear optical materials, gas separation membrane materials, and so on. SOLUTION: This acetylene compound of the general formula (I) [R1 and R2 are each an alkyl, an aryl, a halogen atom, an alkoxy, an aryloxy, a perfluoroalkyl, carboxyl, an alkoxycarbonyl, hydroxy, an acyl, nitro, cyano, an alkylsulfonyl or an arylsulfonyl; and (m) and (n) are each independently an integer of 1 to 4; when (m) is an integer of >=2, plural R1 groups may be the same or different each other; when (n) is an integer of >=2, plural R2 groups may be the same or different each other].

37. 发明专利

JP2000327940A AZOMETHINE COMPOUND AND OILY MAGENTA INK 失效
公开(公告)号：JP2000327940A
公开(公告)日：2000-11-28
申请号：JP2000024454
申请日：2000-02-01
申请人： FUJI PHOTO FILM CO LTD
发明人： YAMAKAWA KAZUYOSHI , MOTOKI MASUSHI , ASANUMA NAOKI , SUZUKI AKIRA , SATO TADAHISA , MIKOSHIBA TAKASHI
IPC分类号： B41J2/01 , B41M5/00 , C09B55/00 , C09D11/00 , C09D11/328 , C09D11/36
摘要： PROBLEM TO BE SOLVED: To obtain a new compound of an oily dye, excellent in color reproductivity, preservability and solubility and useful for preparation of a magenta ink for an ink jet printing method. SOLUTION: This azomethine compound is represented by formula I [R1 is a 1-16C alkyl; R2 is a halogen, a 1-20C alkyl or the like; R3 is a 1-30C alkylene or the like; R4 is a 1-16C alkyl; L1 is a 1-30C alkylene or the like; L2 is CO-NH group or the like; X is cyano or the like; Y is H, a halogen or the like; m is 1-4; n is 1-18; p is 0-4; the number of the carbon atoms of R1, L1, L2, R3 and R4 totals 20-50] e.g. a compound of formula II. The compound of the formula I is obtained by reacting an azole-based compound of formula III, e.g. 2-[4- 3-(tetradecyloxycarbonyl)propanoylamino}phenyl]-6-tert-butyl-7- chloropyrazolo[1,5-b][1,2,4]triazol, with a p-phenylenediamine-based compound of formula IV under an oxidative condition.

38. 发明专利

JPH11217386A PRODUCTION OF SPIROCHROMANE COMPOUND 失效
公开(公告)号：JPH11217386A
公开(公告)日：1999-08-10
申请号：JP1978198
申请日：1998-01-30
申请人： FUJI PHOTO FILM CO LTD
发明人： TANIGUCHI MASAHIKO , YAMAKAWA KAZUYOSHI
IPC分类号： C07D493/10
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a spirochromane compound by condensing a phenol compound with a ketone compound in the presence of a sulfur-containing compound at as a low temperature as possible, capable of producing the spirochromane compound in a high selectivity in a high yield and in improved productivity at a high reaction speed. SOLUTION: This method for producing a spirochromane compound of formula III comprises condensing a phenol compound of formula I (R -R are each hydrogen, a 1-10C alkyl, a halogen or the like)(for example, methylhydroquinone) with a ketone compound of formula II (R and R are each hydrogen or a 1-20C alkyl) (preferably acetone). Therein, the reaction is carried out in the presence of a sulfur-containing compound of the formula: R -S-R (R is hydrogen or a substituent; R is a substitutent) (for example, thioglycolic acid). The phenol compound of formula I is preferably reacted with the ketone compound of formula II in an amount of 1-5 moles per mole of the phenol compound of formula I in the presence of the sulfur-containing compound in an amount of 0.01-100 mol.% based on the phenol compound of formula I under an acidic condition at temperatures of 20-100 deg.C for 4-24 hr.

39. 发明专利

JPH1129574A PRODUCTION OF SPIROCHROMAN COMPOUND 失效
公开(公告)号：JPH1129574A
公开(公告)日：1999-02-02
申请号：JP18810397
申请日：1997-07-14
申请人： FUJI PHOTO FILM CO LTD
发明人： TANIGUCHI MASAHIKO , YAMAKAWA KAZUYOSHI
IPC分类号： G03C7/392 , C07D493/10 , C08K5/15 , C08K5/1545
摘要： PROBLEM TO BE SOLVED: To produce the subject compound useful as a discoloration inhibitor, etc., in a photograph industry in good yield and selectivity by carrying out a condensation reaction of a hydroquinone compound with a ketone compound at a lowest temperature as much as possible. SOLUTION: (A) A hydroquinone compound of formula I (R to R are each independently H, 1-10C alkyl, a 6-20C aryl, a hydroxyl group, a halogen or the like) is condensed with (B) a ketone compound of formula II (R and R are each independently H, a 1-20C alkyl) by using hydrobromic acid or hydroiodic acid as a mineral acid and in the presence of an aqueous solution thereof to provide (C) a spirochroman compound of formula III in the method for producing the spirochroman compound. The concentration of the used mineral acid is preferably 35-80 wt.%. The reaction is preferably carried out by adding a metal compound (for example, an alkaline earth metal compound) at a temperature of 40-120 deg.C temperature for 1-36 hour, and keeping the temperature low and the reaction time long is more preferable.

40. 发明专利

JPH107614A 2,2-BISHALOMETHYLALKANECARBOXYLIC ACID HALIDE COMPOUND AND ITS PRODUCTION 失效
公开(公告)号：JPH107614A
公开(公告)日：1998-01-13
申请号：JP30070696
申请日：1996-11-12
申请人： FUJI PHOTO FILM CO LTD
发明人： TANIGUCHI MASAHIKO , YAMAKAWA KAZUYOSHI , SATO TADAHISA
IPC分类号： C07C51/60 , C07C53/50
摘要： PROBLEM TO BE SOLVED: To efficiently and simply produce the subject compound useful as a synthetic intermediate for yellow couplers for color photographic materials or germicides by reacting a specific OH-containing carboxylic acid compound with a specified halogen compound. SOLUTION: (A) A compound represented by the formula [R is a (cyclo)alkyl or an aryl] is reacted with (B) (B1 ) a bromide or an iodide of tri- or pentavalent phosphorous such as a compound represented by the formula PX3 (X is bromine or iodine) or R'3 R''PX [R' is an alkyl, an aryl(oxy), an alkoxy or X; R'' is an imide group or X] or (B2 ) a thionyl halide to produce a 2,2- bishalomethylalkanecarboxylic acid halide compound. Furthermore, the reaction is carried out by using the component B in an equiv. amount of 1-20 times, preferably 1-5 times based on the component A suitable at 50-200 deg.C, preferably at 100-150 deg.C temperature.

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