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11. 发明专利

JPH08259822A THERMOPLASTIC RESIN COMPOSITION 失效
公开(公告)号：JPH08259822A
公开(公告)日：1996-10-08
申请号：JP9154695
申请日：1995-03-24
申请人： DAICEL CHEM
发明人： OTSUKA YOSHIHIRO , AIZAWA KATSUMI , OSHINO YASUHIRO
IPC分类号： C08K5/098 , C08K5/09 , C08K5/45 , C08K5/46 , C08L25/04 , C08L25/12 , C08L53/00 , C08L101/00
摘要： PURPOSE: To obtain a thermoplastic resin composition convertible into a molded and processed product having the homogeneously and closely matte surface thereof. CONSTITUTION: This component comprises (A) 100 pts.wt. amorphous resin (except a rubber-like polymer), (B) 0.01-20 pts.wt. epoxidized diene-based block copolymer and (C) a polyfunctional compound containing at least two same or different functional groups selected from carboxyl, amino and carboxylic acid anhydride groups and units of the formula C(=X)-NH-C(=Y) (X and Y denote each oxygen or sulfur atom or either thereof denotes oxygen atom and the other denotes sulfur atom) and/or (D) a metallic carboxylate in an amount of 0.01-20 pts.wt.

12. 发明专利

JPH08259811A POLYPHENYLENE SULFIDE RESIN COMPOSITION 失效
公开(公告)号：JPH08259811A
公开(公告)日：1996-10-08
申请号：JP9154795
申请日：1995-03-24
申请人： DAICEL CHEM
发明人： OTSUKA YOSHIHIRO , AIZAWA KATSUMI , OSHINO YASUHIRO
IPC分类号： C08L9/00 , C08F8/08 , C08G59/34 , C08L21/00 , C08L23/00 , C08L33/04 , C08L33/06 , C08L53/00 , C08L53/02 , C08L63/08 , C08L81/02 , C08L87/00
摘要： PURPOSE: To obtain a composition, containing a polyphenylene sulfide resin an epoxidized diene-based block copolymer, another hydrogenated conjugated diene-based polymer, etc., excellent in toughness such as impact strength or tensile elongation and moldability and moldable without causing an increase in viscosity and gelation. CONSTITUTION: This composition contains (A) a polyphenylene sulfide resin, (B) an epoxidized diene type block copolymer obtained by epoxidizing double bonds derived from a conjugated diene compound of a block copolymer comprising at least one polymer block consisting essentially of an aromatic vinyl compound and at least one polymer block consisting essentially of a conjugated diene compound and (C) one or more polymers selected from a hydrogenated conjugated diene-based polymer other than the component (B), an olefinic copolymer and an acrylic rubber.

13. 发明专利

JPH08245756A PRODUCTION OF RESIN COMPOSITION FOR RECYCLING 失效
公开(公告)号：JPH08245756A
公开(公告)日：1996-09-24
申请号：JP7945795
申请日：1995-03-10
申请人： DAICEL CHEM
发明人： OTSUKA YOSHIHIRO , AIZAWA KATSUMI , OSHINO YASUHIRO
IPC分类号： C08J11/06 , B29B17/00 , B29B17/04 , B29K105/26 , C08G59/34 , C08L25/04 , C08L55/00 , C08L55/02 , C08L67/00 , C08L69/00 , C08L71/00 , C08L71/12 , C08L77/00 , C08L81/02
摘要： PURPOSE: To obtain the subject composition, excellent in various physical properties such as impact resistance and molding processability, capable of recarrying out the molding processing and useful for countermeasures for environmental problems by crushing a molded and processed product and melt kneading the crushed product with an epoxidized (partially hydrogenated)diene-based polymer. CONSTITUTION: (A) A molded and processed product comprising (i) a thermoplastic resin (preferably a saturated polyester resin or a polycarbonate resin) or (ii) a thermoplastic resin composition (preferably comprising at least two selected from the saturated polyester resin, the polycarbonate resin, a polyamide resin, an ABS-based resin, a polystyrene-based resin, an As resin, a polyarylene sulfide resin, a polyarylene ester resin and polyphenylene ether resin) is crushed. The resultant resin pieces in an amount of 100 pts.wt. are then melt kneaded with (B) 0.1-30 pts.wt. epoxidized (partially hydrogenated)diene-based polymer to afford the objective composition. Furthermore, the component (A) is preferably a crushed product of a bottle, etc., made of polyethylene terephthalate resin.

14. 发明专利

JPH0687954A PRODUCTION OF POLYCARBONATE 失效
公开(公告)号：JPH0687954A
公开(公告)日：1994-03-29
申请号：JP12568291
申请日：1991-03-07
申请人： DAICEL CHEM
发明人： OSHINO YASUHIRO , SUGANO TATSUYA
IPC分类号： C08G64/30 , C08G64/20
摘要： PURPOSE:To obtain a polycarbonate polymer having a high mol.wt. without employing toxic phosgene by melt-polycondensing a dihydric phenol with a carbonic diester in the presence of a catalyst such as a basic nitrogen compound and a catalyst such as (substituted)phenylacetic acid. CONSTITUTION:A dihydric phenol [e.g. 2,2-bis(4-hydroxyphenyl)propane] and a carbonic diester (e.g. diphenyl carbonate) are subjected to a melt- polycondensation reaction in the presence of a catalyst such as a nitrogen compound (e.g. 2-methylimidazole) and a catalyst such as a non-substituted or substituted phenylacetic acid of the formula (R1 is H, 1-5C alkoxy, nitro; R2, R3 are H, 1-5C alkyl, phenyl) (e.g. phenylacetic acid) to produce the objective high mol.wt. polycarbonate without using toxic phosgene, the melt- polycondensation reaction comprising stirring the raw materials at 180 deg.C in a nitrogen atmosphere for 1hr, subjecting the reaction product to the rise in temperature, while gradually lowering the pressure, and finally polycondensing the reaction product at 270 deg.C under 0.1Torr for 1hr, while distilling off the by-produced phenol.

15. 发明专利

JPH05148355A POLYCARBONATE 失效
公开(公告)号：JPH05148355A
公开(公告)日：1993-06-15
申请号：JP31473491
申请日：1991-11-28
申请人： DAICEL CHEM
发明人： OSHINO YASUHIRO , SUGANO TATSUYA
IPC分类号： C08G64/06 , C08G64/00 , C08G64/20 , C08G64/30
摘要： PURPOSE:To obtain a noncolored polycarbonate by specifying the iron concentration, chlorine concentration and terminal hydroxyl concentration of a polycarbonate. CONSTITUTION:1mol of a dihydroxy compound of any one of formulas I-IV (wherein R1 to R4 are each H 1-8C linear or branched alkyl or phenyl; X is halogen, (n) is 0-4; and (m) is 1-4) and 1.01-1.5mol of a carbonic diester are subjected to melt polycondensation at 100-300 deg.C in the presence of a transesterification catalyst comprising 10 to 10 mol, per mol of the dihydroxy compound, of an alkali (alkaline earth) metal compound and/or an electron- donating amine compound to obtain a polycarbonate of an iron concentration of 5ppm or below, Cr, Ni and Na concentrations of each 1ppm or below, a chlorine concentration of 10ppm or below, and a terminal hydroxyl concentration of 20mol% or below.

16. 发明专利

JPH05148354A PRODUCTION OF POLYCARBONATE 失效
公开(公告)号：JPH05148354A
公开(公告)日：1993-06-15
申请号：JP31473591
申请日：1991-11-28
申请人： DAICEL CHEM
发明人： OSHINO YASUHIRO , YAMATO TSUTOMU
IPC分类号： C08G64/30 , C08G64/20
摘要： PURPOSE:To obtain a colorless transparent high-molecular polycarbonate without using any phosgene by effecting the melt polycondensation of a dihydroxy compound with a carbonic ester in the presence of a specified transesterification catalyst. CONSTITUTION:1mol of a dihydroxy compound of any one of formulas I-IV (wherein R1 to R4 are each H 1-8C linear or branched alkyl or phenyl; X is halogen; (n) is 0-4; and (m) is 1-4) and 1.01-1.5mol of a carbonic diester are subjected to melt polycondensation at 100-300 deg.C in the presence of a transesterification catalyst comprising 10 to 10 mol, per mol of the, dihydroxy compound, of an electron-donating amine compound, 10 to 10 mol of an alkali (alkaline earth) metal compound and 10 to 10 mol of a phosphorus compound of any one of formulas V-IX (wherein R1 is a 1-30C hydrocarbon residue).

17. 发明专利

JPH041226A PRODUCTION OF POLYCARBONATE 失效
公开(公告)号：JPH041226A
公开(公告)日：1992-01-06
申请号：JP10359590
申请日：1990-04-19
申请人： DAICEL CHEM
发明人： OSHINO YASUHIRO , SUGANO TATSUYA
IPC分类号： C08K5/13 , C08G64/40 , C08K3/00 , C08K5/00 , C08K5/51 , C08K5/523 , C08L69/00
摘要： PURPOSE:To obtain a polycarbonate excellent in heat resistance, hydrolysis resistance and hue by mixing a polycarbonate obtained under specified conditions with a phosphite compound and a hindered phenol compound. CONSTITUTION:A polycarbonate obtained by transesterifying a dihydroxy compound [e.g. 2,2-bis(4-hydroxyphenyl)propane] with a bisaryl carbonate (e.g. diphenyl carbonate) in the presence of a transesterification catalyst (e.g. potassium borohydride) and melt-polycondensing the product is mixed with a phosphite compound, desirably a compound of formula I and a hindered phenol compound desirably having a structure of formula II (wherein R is a 1-30C hydrocarbon group).

18. 发明专利

JPH03149221A PRODUCTION OF POLYCARBONATE 失效
公开(公告)号：JPH03149221A
公开(公告)日：1991-06-25
申请号：JP28850989
申请日：1989-11-06
申请人： DAICEL CHEM
发明人： SUGANO TATSUYA , OSHINO YASUHIRO
IPC分类号： C08G64/20 , C08G64/30 , C08G64/38
摘要： PURPOSE:To produce a high-molecular polycarbonate contg. no chlorine ion without the necessity of using toxic phosgene, by the melt polycondensation of a dihydroxyl compd. with a bisaryl carbonate in the presence of a catalyst comprising a compd. contg. an element of the group Vb of the periodic table. CONSTITUTION:In the presence of at least one catalyst selected from the group consisting of compds. contg. an element of the group Vb of the periodic table, a dihyroxyl compd. (e.g. bisphenol A) is melt polycondensed with a bisaryl carbonate (e.g. bisphenyl carbonate) to give a polycarbonate, which is transparent and suitable for use as a window pane substitute. Examples of the catalyst include 2-methylimidazole, 4-dimethylaminopyridine carbonate, triphenylphosphine, and tetraphenylantimony.

19. 发明专利

JPH1180521A POLYMER ALLOY AND COMPOSITION CONTAINING THE SAME 失效
公开(公告)号：JPH1180521A
公开(公告)日：1999-03-26
申请号：JP26491597
申请日：1997-09-11
申请人： DAICEL CHEM
发明人： OTSUKA YOSHIHIRO , OSHINO YASUHIRO
IPC分类号： B60C1/00 , B29D30/04 , B60C9/04 , C08G59/34 , C08L7/00 , C08L9/00 , C08L21/00 , C08L23/16 , C08L33/18 , C08L53/02 , C08L63/08 , C08L67/02
摘要： PROBLEM TO BE SOLVED: To obtain a new polymer alloy and a composition obtained by compounding the polymer alloy with an unvulcanized rubber, and further to provide a tire part by using the composition. SOLUTION: This polymer alloy comprises (a) a polyester resin having 5-80 acid value, (b) an epoxidized dienic block copolymer and (c) an unvulcanized rubber. The composition is obtained by mixing the polymer alloy with (d) one or more kinds of unvulcanized rubbers derived from a dienic monomer and selected from synthetic rubbers and natural rubbers so that the total of the polyester resin (a) and the epoxidized dienic block copolymer (b) may be 2-25 pts.wt. based on 100 pts.wt. whole unvulcanized rubber in the composition. The tire parts are a tread base, a tread cap, a carcass ply, a cushion, a belt ply, a shoulder wedge, a bead area, an apex or a Shaffer comprising the polymer alloy or the composition.

20. 发明专利

JPH10147766A PAVING MIXTURE 失效
公开(公告)号：JPH10147766A
公开(公告)日：1998-06-02
申请号：JP32465896
申请日：1996-11-20
申请人： DAICEL CHEM
发明人： OTSUKA YOSHIHIRO , OSHINO YASUHIRO
IPC分类号： C08K3/00 , C08L53/02 , C08L63/08 , C09J195/00
摘要： PROBLEM TO BE SOLVED: To provide a paving mixture which can be applied at ordinary temperature and is used as a paving material for e.g. a sidewalk surface course and a cured product thereof. SOLUTION: This mixture comprises 100 pts.wt. aggregate, 1-5 pts.wt. filler, 1-15 pts.wt. hydraulic inorganic material and 3-15 pts.wt. modified asphalt emulsion containing an epoxidized diene block copolymer. The surface of the aggregate should by coated with the modified asphalt emulsion in which the filler and the inorganic material are dispersed.

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