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141. 发明专利

JPS61174103A PRODUCTION OF POROUS SPHERICAL AND PULVEROUS POWDER CONSISTING OF METALLIC OXIDE 失效
公开(公告)号：JPS61174103A
公开(公告)日：1986-08-05
申请号：JP1171885
申请日：1985-01-23
申请人： CATALYSTS & CHEM IND CO
发明人： SATO GORO , ARIMA YUSAKU , KOMATSU MICHIO , TANAKA HIROKAZU , TANAKA YOSHITSUNE , SHIMADA TAKEO
IPC分类号： C01B13/14 , C01B13/36 , C01B33/18 , C01F7/02 , C01G23/053 , C01G25/02
摘要： PURPOSE:To obtain porous spherical and pulverous powder having a desired grain size by spraying a slurry mixture composed of an inorg. oxide colloid and inorg. oxide gel into gaseous flow. CONSTITUTION:10-95pts. colloid liquid of the inorg. oxide or hydrous oxide of Si, Ti, Al, etc. and 5-90pts. gel of the inorg. oxide are mixed to prepare the slurry. The average grain size of the primary particles of such colloid liquid is preferably about

142. 发明专利

JPS6132335B2 失效
公开(公告)号：JPS6132335B2
公开(公告)日：1986-07-26
申请号：JP2151179
申请日：1979-02-27
申请人： AKZO NV
发明人： UORUFUGANGU RANGE , KURAUSU GERURATSUHA
IPC分类号： A61M1/22 , A61F2/00 , A61M1/16 , B01D39/00 , B01J4/00 , B01J31/06 , B01J37/02 , B01J37/03 , B05D3/04 , C01B13/02 , C01B13/36 , C08J3/20 , C08J5/00 , C08J5/18 , C08J7/00 , C08K3/02 , C08K3/08 , C08K3/10 , C09D101/08

143. 发明专利

JPS6168314A Production of porous silica, alumina, titania, and zirconia 失效
标题翻译：生产多孔二氧化硅，氧化铝，钛铁矿和ZIRCONIA
公开(公告)号：JPS6168314A
公开(公告)日：1986-04-08
申请号：JP18861184
申请日：1984-09-07
申请人： Agency Of Ind Science & Technol
发明人： MIZUKAMI FUJIO , NIWA SHUICHI , TSUCHIYA TORU , SHIMIZU KAZUO , IMAMURA JUICHI
IPC分类号： C01G23/053 , C01B13/32 , C01B13/36 , C01B33/152 , C01F7/36 , C01G25/00 , C01G25/02
CPC分类号： C01F7/36
摘要： PURPOSE: To produce uniform, amorphous, and porous silica, alumina, titania, and zirconia by prepg. specified soln. having uniform compsn. of each oxygen- contg. org. compd. of Si, Al, Ti or Zr, transforming the soln. to sol by hydrolysis, and transforming the sol to gel, and dissipating residual compd. in the gel.
CONSTITUTION: An oxygen-contg. org. compd. such as alkoxide, ketoalcohol, etc. of Si, Al, Ti, Zr, etc. is dissolved uniformly in a soln. contg. at least one kind of polar compd. having multidentate or crosslinking coordination power such as dihydric alcohol, aminoalcohol, etc. at 10W100°C. The compd. is hydrolyzed at 20W80°C to prepare uniform sol, and transforms further to agar-like gel. The gel is dried at low temp., crushed to appropriate size, heat-treated at 200W700°C under reduced pressure to dissipate and remove residual polar compd. Thus, uniform porous silica, alumina, titania, or zirconia, is obtd.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：制备均匀，无定形和多孔的二氧化硅，氧化铝，二氧化钛和氧化锆。指定的soln 有统一的compsn。的每个氧气组织 compd。的Si，Al，Ti或Zr，转化溶胶。通过水解溶胶，并将溶胶转化为凝胶，并消散残留的化合物。在凝胶中。构成：氧气不足组织 compd。如Si，Al，Ti，Zr等的醇盐，酮醇等均匀溶解于溶胶中。对比至少有一种极地化合物在10-100℃下具有多元醇或交联配位能，如二元醇，氨基醇等。 compd。在20-80℃下水解以制备均匀的溶胶，并进一步转化成琼脂样凝胶。将凝胶在低温下干燥，粉碎至适当的大小，在200-700℃减压下热处理，以消散和去除残留的极性化合物。因此，可以得到均匀的多孔二氧化硅，氧化铝，二氧化钛或氧化锆。

144. 发明专利

JPS6021802A METALLIC OXIDE HAVING UNIFORM PORE, ITS MANUFACTURE, AND CARRIER FOR CATALYST CONSISTING OF ITS METALLIC OXIDE 失效
公开(公告)号：JPS6021802A
公开(公告)日：1985-02-04
申请号：JP13011883
申请日：1983-07-15
申请人： DAIDO OXYGEN
发明人： WAKUI MASAHIRO , HANDA TADAHIKO
IPC分类号： C01B33/00 , B01J35/10 , C01B13/18 , C01B13/36 , C01B33/16 , C01B33/187 , C01F7/02 , C01F7/14 , C01F7/30
摘要： PURPOSE:To manufacture the titled amorphous metallic having narrow distribution of pore diameter by allowing to react a basic metallic acid salt with a specific organic compd. to obtain a solid which is extracted with an organic solvent, and removing the organic compd. CONSTITUTION:A soln. in an organic solvent of 0.1-500pts.wt. organic compd. (e.g. malonic acid) which is expressed by the formula (R is an organic group; X is a reaction goup; X' is H or a reaction group; (n) is 1-3) is allowed to react with an aq. soln. of l00pts.wt. basic metallic acid salt (e.g. water glass No. 2) having 1-50wt% concn. which is heated to 0-300 deg.C while agitating vigorously. Then an aq.soln. of mineral acid (e.g. hydrochloric acid) having 3-10wt% concn. is added to regulate the pH to 6-9, and a solid is obtained. The solid is washed until halogen is not detected, and extracted with an organic solvent (e.g. acetone) to recover the organic compd. Then the solid, afte drying at 110-120 deg.C for 4-5hr, is calcined to obtain the metallic oxide whose distribution of pore diameter is concentrated within the extremely narrow micropore range of 10- 100Angstrom .

145. 发明专利

JPS5839768B2 失效
公开(公告)号：JPS5839768B2
公开(公告)日：1983-09-01
申请号：JP4248675
申请日：1975-04-07
申请人： NIPPON PAINT CO LTD
发明人： OKAI TOSHIHIRO , WADA YUTAKA , KISHIMOTO TETSUO
IPC分类号： C01G9/02 , C01B13/36 , C01B25/30 , C01G9/00 , C01G49/00 , C01G49/02 , C01G53/00 , C01G53/04 , C02F1/62 , C23C22/00

146. 发明专利

JPS5823336B2 失效
公开(公告)号：JPS5823336B2
公开(公告)日：1983-05-14
申请号：JP8222072
申请日：1972-08-18
申请人： STICHTING REACTOR CENTRUM
发明人： OTAKAARU BOTOCHETSUKU
IPC分类号： B01D11/02 , B01J2/00 , C01B13/36 , C01G43/00 , C01G43/025 , C01G56/00 , G21C3/62 , C01G57/00

147. 发明专利

JPS5319555B2 失效
公开(公告)号：JPS5319555B2
公开(公告)日：1978-06-21
申请号：JP10463271
申请日：1971-12-24
IPC分类号： C01G1/00 , C01B13/14 , C01B13/36 , C01B21/48 , C01B32/60 , C01C3/20 , C01F7/00 , C01G3/02 , C01G49/00 , C01G51/00 , C01G53/00 , C07F1/00 , C07F7/22 , C07F7/24 , C07F13/00 , C09C1/00 , C09C3/00

148. 发明专利

JPS529556B2 失效
公开(公告)号：JPS529556B2
公开(公告)日：1977-03-16
申请号：JP6364273
申请日：1973-06-06
IPC分类号： C02F1/28 , C01B13/36

149. 发明专利

JPS5148393B2 失效
公开(公告)号：JPS5148393B2
公开(公告)日：1976-12-20
申请号：JP11729773
申请日：1973-10-18
IPC分类号： B01D53/50 , B01D53/77 , B01D61/44 , B01D61/50 , B01D61/54 , B01D65/04 , C01B13/36 , C01C1/24 , C01F11/46 , C02F1/469 , C02F1/58 , C02F9/00

150. 发明专利

JPS5186075A 失效
公开(公告)号：JPS5186075A
公开(公告)日：1976-07-28
申请号：JP1061075
申请日：1975-01-25
申请人： KOGYO GIJUTSUIN
发明人： MYATA KENICHI , NAKAHARA YOSHIKO
IPC分类号： B01J2/00 , B01J2/06 , C01B13/36 , C01B33/20 , C01F11/18 , C04B14/02 , C08K7/24

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