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91. 发明专利

JPS6240395B2 失效
公开(公告)号：JPS6240395B2
公开(公告)日：1987-08-27
申请号：JP7799777
申请日：1977-07-01
申请人： EXXON RESEARCH ENGINEERING CO
发明人： KURAIDO ERU OORUDORITSUJI , ROBII BEADEN JUNIA
IPC分类号： C10G1/06 , B01J23/00 , B01J31/00 , C10G1/08

92. 发明专利

JPS62185785A HIGH TEMPERATURE SEPARATION METHOD AND SEPARATOR 失效
公开(公告)号：JPS62185785A
公开(公告)日：1987-08-14
申请号：JP2370287
申请日：1987-02-05
申请人： RUHRKOHLE AG
发明人： FURIITOHERUMU BOORANDERU , KARURU HAINTSU FUETSUSHINGU , BUORUFUDEIITERU KURAIN , FURANKU MIRUTSUCHIYU
IPC分类号： C10G31/06 , B01D5/00 , C10G1/00 , C10G1/06 , C10G49/22

93. 发明专利

JPS62161889A LIQUEFACTION OF COAL 失效
公开(公告)号：JPS62161889A
公开(公告)日：1987-07-17
申请号：JP138186
申请日：1986-01-09
申请人： ASAHI CHEMICAL IND
发明人： YAMADA YOICHI , TAMURA NOBUHIRO
IPC分类号： C10G1/06 , B01J27/043
摘要： PURPOSE:To perform coal liquefaction simply in high activity and in economically advantageous manner, by using as catalyst a product prepared by calcination, under specified conditions in a sulfur oxide gas atmosphere, of ion oxide- contg. powder and carbonaceous matter-contg. powder. CONSTITUTION:The objective coal liquefaction is carried out by using, as catalyst, a product prepared by calcination, pref. using a fluidized bed furnace in a sulfur oxide gas atmosphere containing SO2, SO3, etc. at 600-1,200 (pref. 700-1,000) deg.C, of a mixture of iron oxide-contg. powder (FeO, Fe3O4, Fe2O3 etc.) and carbonaceous matter-contg. powder (coke, activated carbon, graphite, etc.).

94. 发明专利

JPS62152541A CATALYST FOR LIQUEFYING COAL 失效
公开(公告)号：JPS62152541A
公开(公告)日：1987-07-07
申请号：JP29761685
申请日：1985-12-26
申请人： SUMITOMO METAL IND
发明人： SUHARA YASUHIRO , KANO TAKUO , HAYASHI TAKASHI
IPC分类号： B01J27/02 , C10G1/06
摘要： PURPOSE:To enhance the yield of liquefied oil and to reduce cost, by forming a coal liquefying catalyst of a particulate material with a particle size of 350 mesh or less and moisture of 0.5% or less obtained by drying and grinding dust generated from an iron bath coal gasifying furnace. CONSTITUTION:Dust generated from an iron bath coal gasifying furnace is recovered along with water in a slurry state by a thickener and this recovered slurry is dehydrated, dried and ground to obtain a particulate material with a particle size of 350 mesh or less and moisture of 0.5% or less used as a coal liquefying catalyst. Drying after the aforementioned dehydration is performed using hot air of about 200 deg.C but, if necessary, N2-drying under atmospheric pressure is further employed. The fine grinding of dust is performed using a general ball mill and the adjustment of a particle size to a predetermined one is performed by a vibration screen. This catalyst can more enhance the yield of liquefied oil and reduces the cost of a liquefied oil product.

95. 发明专利

JPS62132994A HYDROGENATIVE LIQUEFACTION OF COAL 失效
公开(公告)号：JPS62132994A
公开(公告)日：1987-06-16
申请号：JP27254985
申请日：1985-12-05
申请人： MITSUI SHIPBUILDING ENG
发明人： ITO HIDENOBU
IPC分类号： C10G1/06
摘要： PURPOSE:To utilize excellent proton-donative property of a polycyclic aromatic hydrocarbon as a hydrogen-donative solvent and to especially improve the yield of light oil, by using the hydrocarbon obtained as a component of a hydroliquefaction oil as a medium oil for the hydroliquefaction reaction of coal. CONSTITUTION:Coal slurry dispersed in a medium oil is hydroliquefied in the presence of a catalyst, the produced oil is distilled in vacuum and the residue is subjected to dry distillation preferably at 500-700 deg.C. The dry distillation oil containing large amount of polycyclic aromatic hydrocarbon is hydrogenated to obtain hydrogenated dry-distillation oil, which is used as the above medium oil. The hydrogenation of the dry-distillation oil is usually carried out by using an Ni-Mo catalyst at 300-400 deg.C under 150-300kg/cm G pressure and an LHSV of 0.5-2.

96. 发明专利

JPS62131092A METHOD OF LIQUEFYING COAL THROUGH CATALYTIC HYDROGENATION 失效
公开(公告)号：JPS62131092A
公开(公告)日：1987-06-13
申请号：JP27060085
申请日：1985-12-03
申请人： MITSUI SHIPBUILDING ENG
发明人： MURATA KATSUHIDE , ITO HIDENOBU
IPC分类号： C10G1/06
摘要： PURPOSE:To obtain a hydroliquefied gas in a simple process in a high yield and at a low cost, by preheating and reacting a particular raw coal slurry in the presence of hydrogen and further preheating and hydroliquefying the coal slurry using a recovered heavy distillate liquefied oil as a medium oil. CONSTITUTION:A raw coal slurry 4 was prepared from 1kg (on the dry basis) of raw coal powder 1, 10-70g of a binary mixed hydrogenation catalyst 2 comprised of 1pt.wt. low-temp. active catalyst (e.g., nickel-based catalyst) and 1-10pts.wt. high- temp. active catalyst (e.g., Fe-based catalyst) and 1.1-5kg of a medium oil 3 comprised of a heavy distillate liquefied oil 16 having a b.p. of 300-538 deg.C which has been obtd. by distilling the hydroliquefied oil in vacuo is preheated in a first preheater to 250-450 deg.C together with a hydrogen gas 5 such as a hydrogen-rich gas obtd. by gas-liq. separation of the hydroliquefied product. The slurry is led to a preheated reactor 7 to cause a hydrogenation reaction, while the raw coal powder 1 is dissolved in the medium oil 3. It is preheated in a second preheater 8, hydroliquefied in a water stream liquefaction reactor 9. The reaction mixture is led to a gas-liq. separator 10, where it is separated into a hydrogen-rich gas 11 and an oil component 12. After removal of solid matter with a solid-liq. separator 13, the oil component 12 is separated into a light oil 15 and heavy distillate liquefied oil 16.

97. 发明专利

JPS62131091A PRODUCTION OF TAR OILS 失效
公开(公告)号：JPS62131091A
公开(公告)日：1987-06-13
申请号：JP27209485
申请日：1985-12-03
申请人： MITSUBISHI CHEM IND
发明人： YOSHINO YOSHIO , DOBASHI KOJI , TORIMARU HIROYUKI , TANIOKA SEIICHI
IPC分类号： C10B27/00 , C10G1/02 , C10G1/06
摘要： PURPOSE:To efficiently recover and collect tar oils, by recovering tar oils from a gas which has been produced in the first half period of carbonization from a coke oven gas, recovering a gas which has been produced in the second half period of carbonization through a switching operation and contacting them with coal having a low degree of coalification, thereby causing hydropyrolysis. CONSTITUTION:Coal is carbonized in a carbonization chamber of a chamber type coke oven 1. A tar-contg. gas, as shown in section I, produced in the first half period of the carbonization having a calorific value of 5,000kcal/Nm or more and a hydrogen concn. of 50-55vol% and a methane concn. of 30-35vol% is led to, e.g., a bent portion of a riser where aq. ammonia is sprayed to the gas to recover the gas and tar oils. A gas, as shown in section II, produced in the second half period of carbonization having a hydrogen concn. of 55-90vol%, a methane concn. of 30-0vol% and substantially free from tar is taken out of the coke oven 1 through a switching operation at an appropriate time. The gas thus obtd. is pressurized with a compressor 2 and, if necessary, preheated with a preheater 3. The gas is then led to a reactor 4. Powdery coal having a low degree of carbonization is supplied into the reactor via a feeder 5. In the reactor, the coal is contacted with the gas at 600-1,000 deg.C to cause hydropyrolysis. Char or the like is separated with a char separator 6. Liquid components contg. tar oils, etc., are separated and recovered with a liq. product separator 8 via a cooler 7.

98. 发明专利

JPS6218596B2 失效
公开(公告)号：JPS6218596B2
公开(公告)日：1987-04-23
申请号：JP12069282
申请日：1982-07-13
申请人： MITSUI SHIPBUILDING ENG
发明人： MIKAMI KOICHI , ITO HIDENOBU , MURATA KATSUHIDE , UEDA MIKIO
IPC分类号： C10L1/183 , C10G1/00 , C10G1/06 , C10L1/14 , C10L1/18 , C10L1/22 , C10L1/223 , C10L1/24 , C10L1/26 , C10L1/30

99. 发明专利

JPS6236490A METHOD OF CONTROLLING COAL LIQUEFYING REACTION 失效
公开(公告)号：JPS6236490A
公开(公告)日：1987-02-17
申请号：JP17573885
申请日：1985-08-12
申请人： SUMITOMO METAL IND
发明人： CHIKADA TSUKASA , HAYAKAWA KEIICHI
IPC分类号： C10G1/06
摘要： PURPOSE:To continuously liquefy coal in a high oil yield without occurrence of device troubles, by liquefying coal while controlling each operating factor so as to give a constant C of the given equation in a particular range. CONSTITUTION:1pt.wt. coal and 0.1pt.wt. or less catalyst such as iron powder are added to 1-2pts.wt. hydrogenated circulating solvent comprising a coal liquefied oil to prepare a slurry. The slurry is pressure fed together with hydrogen into a high temp. and high-pressure liquefying reactor. A liquefying reaction is conducted by concurrently ascending the slurry and gas, while the feed, G, of the hydrogen contg. gas is controlled so that the constant C in the equation [wherein G is the feed of the hydrogen contg. gas (Nl/hr); S is the feed of the slurry (l/hr); C is a constant; Po is the operating pressure (atm); Tb is the operating temp. (K); BP is the boiling point of the slurried solvent; alpha is the fraction of the weight of the solvent in the slurry] is in the range of 0.5-1.0. After completion of the reaction, the slurry is distilled to separate it into a light product oil, a circulating oil and a residue. The circulating oil is hydrogenated and the product is used as the hydrogenated circulating solvent for slurry.

100. 发明专利

JPS621432B2 失效
公开(公告)号：JPS621432B2
公开(公告)日：1987-01-13
申请号：JP3321479
申请日：1979-03-23
申请人： NIPPON OIL CO LTD
发明人： FUJIMUNE TOKUO
IPC分类号： C10G1/06 , C10G1/04

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