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91. 发明专利

JPS58194907A Production of vinyl chloride paste resin 失效
标题翻译：醋酸氯树脂树脂的生产
公开(公告)号：JPS58194907A
公开(公告)日：1983-11-14
申请号：JP7629682
申请日：1982-05-07
申请人： Mitsubishi Monsanto Chem Co
发明人： FUJINO SEIJI
IPC分类号： C08F14/00 , C08F6/00 , C08F6/06 , C08F6/22 , C08F14/06
摘要： PURPOSE: To facilitate separation of free water from solids to thereby produce the titled paste resin in good efficiency, by adding a specified water-soluble cationic high-molecular compound to a vinyl chloride (co)polymer latex and coagulating the particles in the latex.
CONSTITUTION: Use is made of a water-soluble cationic high-molecular compound of formula I or II [wherein R
1 WR
4 are each H or a 1W4C alkyl, Z is -(CH
2 )-, formula III, m and n are each 1W6, X and Y are each a halogen and n≥2], preferably, one having positive charges (surface charge density ≥ about 10
-5 C/cm
2 ) and a particle diameter of about 0.01W10μ. Namely, about 0.001W 5wt%, based on the weight of the contained particles, above high-molecular compound is added to a vinyl (co)polymer latex to coagulate the particles without flocculating them, the free water is removed by decantation, filter pressing or a like operation, and the obtained cake (solids concentration about 65W78%) is dried.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：为了促进游离水与固体分离，从而通过向氯乙烯（共）聚合物胶乳中加入特定的水溶性阳离子高分子化合物并使胶乳中的颗粒凝结，从而高效率地制备标题糊状树脂。构成：使用式I或II的水溶性阳离子高分子化合物[其中R 1 -R 4各自为H或1-4C烷基，Z为 - （CH 2） - ，式III，m和n为每个1-6，X和Y各自为卤素并且n> = 2]，优选具有正电荷（表面电荷密度> =约10 -5 C / cm 2）和具有约 0.01-10亩即，基于所含颗粒的重量，约0.001-5wt％，将高分子化合物上述的高分子化合物加入到乙烯基（共）聚合物胶乳中，使颗粒凝结而不使其絮凝，通过倾析除去游离水，过滤或类似的操作，并将获得的滤饼（固体浓度约65-78％）干燥。

92. 发明专利

JPS5887102A PROCESS AND APPARATUS FOR PRODUCING COAGULATED LATEX 失效
公开(公告)号：JPS5887102A
公开(公告)日：1983-05-24
申请号：JP18664481
申请日：1981-11-19
申请人： KANEGAFUCHI CHEMICAL IND
发明人： YASUI HIDEO , MIKI YASUHIRO
IPC分类号： C08F6/00 , B29C65/00 , C08C1/00 , C08C1/14 , C08F6/06 , C08F6/22 , C08J3/16
摘要： PURPOSE:To produce a coagulated latex of a wide softening point range, by spraying a polymer latex and a coagulant into a coagulation chamber to which superheated steam is being introduced, thereby coagulating the latex, collecting the produced coagulated particles in water flowing down along the side wall and the bottom surface. CONSTITUTION:A liquid film 4a of water or an organic solvent is formed by means for distributing a flowing liquid in such a manner that the entire surface of the side wall 1a of the coagulation chamber 1 is covered with the film, and this liquid film is allowed to flow down along the side wall 1a. At the same time, superheated steam is introduced through an inlet 9 into the chamber 1, and the chamber is evacuated by suction means 11 so that the pressure of the upper portion of the chamber 1 is controlled at approximately the atmospheric pressure. Then, a polymer latex fed through a feed pipe 16 is divided into liquid drops of a suitable diameter and dispersed by spray means 2 and, at the same tiem, a coagulant is sprayed through spray means 3 and dispersed in the form of gas or mist, whereby the iquid drops of the polymer latex are contacted with the gas or mist-form coagulant in the space to heat and coagulate the latex. The coagulated particles together with the flowing liquid is separated from the gas phase in a gas-liquid contact portion 6 and passes through a receiving part 7, discharge port 8 and discharge line 12 to a receiving tank 13 where the coagulated particles are separated.

93. 发明专利

JPS5761004A Supply tube for polymer latex 失效
标题翻译：用于聚合物漆的供应管
公开(公告)号：JPS5761004A
公开(公告)日：1982-04-13
申请号：JP13810980
申请日：1980-10-01
申请人： Kanegafuchi Chem Ind Co Ltd
发明人： KATOU SHINJI , OGAWA NOBUO , YASUI HIDEO
IPC分类号： B05B9/03 , C08F6/00 , C08F6/22
摘要： PURPOSE: To obtain a supply tube capable of preventing the adherence of scale and also clogging due to the coagulation of polymer latex, by providing a tube diameter enough to obtain more than a specific value of shearing stress on the inner wall of the tube and also a buffing finish of a specific degree on the inner surface.
CONSTITUTION: In a latex manufacturing apparatus in which polymer latex is dispersed in droplets into an atmosphere containing a cogulant by means of a sprayer, a latex supply tube through which the polymer latex is supplied to the sprayer has a diameter enough to give a shearing stress of 100g/cm.sec
2 or more to the inner wall of the tube and also a buffing finish corresponding to at least one using a No.200 buff for the inner surface. Thus, the adherence of scale to the inner wall of the supply tube and also clogging of the tube can be pevented. If a water pipe is connected to the supply tube and water is automatically switched to the latex at the beginning of latex supply, or the latex is automatically switched to water at the time of latex supply stoppage, clogging trouble due to coagulation of the latex in the supply tube and the sprayer can be avoided, and therefore, after the downtime of operation, coating operation can be soon started.
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：目的：为了获得能够防止水垢附着和由于聚合物胶乳凝结引起的堵塞的供应管，通过提供足够的管直径以获得管的内壁上的多于剪切应力的特定值，并且还内表面具有特定程度的抛光表面。构成：在其中聚合物胶乳通过喷雾器分散在含有凝结剂的气氛中的胶乳制造装置中，将聚合物胶乳通过其供给到喷雾器的胶乳供应管具有足够的直径以产生剪切应力 100g / cm 2·sec以上，并且还具有对应于至少一个使用了用于内表面的No.200抛光的抛光饰面。因此，能够使水垢附着在供给管的内壁上，同时也堵塞管子。如果水管连接到供应管，并且在胶乳供应开始时水自动切换到胶乳，或者在胶乳供应停止时胶乳自动切换到水中，则由于胶乳的凝结导致的堵塞问题可以避免供应管和喷雾器，因此在操作停机后，即将开始涂装操作。

94. 发明专利

JPS578124B2 JPS578124B2 - 失效
公开(公告)号：JPS578124B2
公开(公告)日：1982-02-15
申请号：JP81073
申请日：1972-12-25
IPC分类号： C08F14/00 , C08F6/00 , C08F6/22 , C08F214/18 , C08J3/16 , C08K5/17 , C08K5/34 , C08L1/00 , C08L27/00 , C08L27/12

95. 发明专利

JPS56104916A MANUFACTURE OF ALPHA METHYLSTYRENE 失效
公开(公告)号：JPS56104916A
公开(公告)日：1981-08-21
申请号：JP489881
申请日：1981-01-16
申请人： STAMICARBON
发明人： BIRUHERUMASU JIERARUDASU DAIJI , JIYOUJIFU RAMUBERUTASU MARIA F , YAN TEIISEN
IPC分类号： C08F6/00 , C08F6/06 , C08F6/22 , C08F212/08

96. 发明专利

JPS5695905A PREPARATION OF COAGULATED LATEX 失效
公开(公告)号：JPS5695905A
公开(公告)日：1981-08-03
申请号：JP16789380
申请日：1980-11-27
申请人： KANEGAFUCHI CHEMICAL IND
发明人： KATOU SHINJI , OGAWA NOBUO , KAWANAMI NORIO , ONDA TAKASHI
IPC分类号： C08F6/00 , C08F6/22 , C08F6/24 , C08F279/00 , C08F279/02 , C08L7/00 , C08L21/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L51/04
摘要： PURPOSE:To efficiently coagulate and recover a high-molecular latex consisting of a thermoplastic polymer, by means of a conbination of specified precosses. CONSTITUTION:A recovering liquid (hot water kept at a temperature for the formation of a coagulated latex particle) 7 is flowed down on the inner wall surface of coagulation chamber 6 in the form of a thin film, and at the same time a latex- coagulating agent is supplied at least as a fumy substance consisting of a droplet which falls down in accordance with Stokes' low, forming a coagulating atmosphere, which is kept in a temperature range for the formation of a coagulated latex particle. Then latex 1 is sprayed through a nozzle into the coagulation chamber 6 at a rate of about 5.7-20l/sec.m , as a droplet of diameter

97. 发明专利

JPS5521403A PREPARATION OF TERPOLYMER RUBBER 失效
公开(公告)号：JPS5521403A
公开(公告)日：1980-02-15
申请号：JP9253778
申请日：1978-07-31
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： NOBUYO KOUJI , TAKEMURA YASUHIKO , FURUTA ISAO
IPC分类号： C08F6/00 , C08C1/00 , C08C1/14 , C08F6/06 , C08F6/22 , C08F220/00 , C08F220/10 , C08F220/42 , C08F236/00 , C08F236/04
摘要： PURPOSE:To prepare a terpolymer rubber having excellent oil resistance, heat resistance and solvent resistance, by the emulsion polymerization of a conjugated diene, an unsaturated nitrile compound and an unsaturated carboxylic acid ester, followed by the treatment of the resulting polymer with an alkali and the coagulation of the product with a specific coagulant. CONSTITUTION:A terpolymer latex consisting of 5-50wt.% of a conjugated diene, 10-50wt.% of an alpha, beta-unsaturated nitrile compound and 10-80wt.% of an alpha, beta- unsaturated carboxylic acid ester, is prepared by emulsion polymerization. An alkali metal hydroxide (2-30 times mole on the basis of the amount of the residual unsaturated carboxylic acid) is added to the latex and stirred at 50-80 deg.C for >= 10 min. An aqueous solution containing 0.1-1.0% of an inorganic acid and 1- 10% of an alkali metal salt or an aqueous solution containing 0.5-5% of aluminum sulfate [200-600 parts by weight on the basis of 100 parts by weight of the latex (solid content 15-30%)], is added to the mixture as a coagulant to coagulate the terpolymer rubber.

98. 发明专利

JPS5450587A METHOD OF RECOVERING POLYMER FROM DISPERSION IN LIQUID MEDIUM 失效
公开(公告)号：JPS5450587A
公开(公告)日：1979-04-20
申请号：JP10983778
申请日：1978-09-08
申请人： DU PONT
发明人： AACHII ROBAATO BAISU , DONARUDO KEISU BAACHIETSUTO
IPC分类号： C08F6/00 , B29C48/76 , C08C1/14 , C08F2/00 , C08F6/06 , C08F6/14 , C08F6/22 , C08F6/24 , C08F36/00 , C08F36/18 , C08J3/12

99. 发明专利

JPS5335995B2 失效
公开(公告)号：JPS5335995B2
公开(公告)日：1978-09-29
申请号：JP4980176
申请日：1976-04-30
IPC分类号： C08F2/00 , C08F2/22 , C08F2/38 , C08F6/22 , C08F279/00 , C08F279/02

100. 发明专利

JPS5339390A PROCESS FOR PRODUCING GRAFT RUBBER LATEX FREE FROM SOLIDFIED SUBSTANCE 失效
公开(公告)号：JPS5339390A
公开(公告)日：1978-04-11
申请号：JP11275477
申请日：1977-09-21
申请人： MONSANTO CO
发明人： UIRIAMU OOUEN DARUTON , GUREN BAGUREI HIRUTON
IPC分类号： C08F279/00 , C08F6/22

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