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1. 发明专利

JP2000336281A ORGANIC/INORGANIC COMPOSITE GRADIENT MATERIAL, AND ITS PREPARATION AND USE 失效
公开(公告)号：JP2000336281A
公开(公告)日：2000-12-05
申请号：JP26459299
申请日：1999-09-17
申请人： UBE NITTO KASEI CO , WATABE TOSHIYA , HASHIMOTO KAZUHITO , FUJISHIMA AKIRA
发明人： TAKAMI KAZUYUKI , NAKAYAMA NORIHIRO , SUZUKI TARO , TANAKA NAOKI , TACHIBANA EISUKE , ADACHI TATSUHIKO , WATABE TOSHIYA , HASHIMOTO KAZUHITO , FUJISHIMA AKIRA
IPC分类号： C08J5/10 , B32B7/02 , C08F8/42 , C08L101/00 , C09D201/00 , C08L101/16
摘要： PROBLEM TO BE SOLVED: To provide an organic/inorganic composite gradient material whose composition continuously varies in the thickness direction and which is useful in various applications as a new functional material. SOLUTION: An organic/inorganic composite gradient material comprises a composite in which an organic polymer compound and a metallic compound have been chemically bonded and has a structure in which the content of the metallic compound continuously varies in the direction from the depth of the material to its surface. A method of preparing the organic/inorganic composite gradient material comprises forming a coated film composed of a specific organic/inorganic composite film-forming coating solution on an organic substrate and drying the resulting film with heating. A film-forming coating material is composed of the organic/inorganic composite gradient material. An article is coated with the film-forming coating material.

2. 发明专利

JP2007076366A Production process of flexible metal foil laminate 有权
标题翻译：柔性金属箔层压板的生产工艺
公开(公告)号：JP2007076366A
公开(公告)日：2007-03-29
申请号：JP2006224742
申请日：2006-08-21
申请人： Ube Ind Ltd , Ube Nitto Kasei Co Ltd , 宇部日東化成株式会社 , 宇部興産株式会社
发明人： MINEKI YOSHITAKA , SUZUKI TARO , KATO KATSUZO , NARUI KOJI
IPC分类号： B29C65/02 , B29K79/00 , B32B15/088 , H05K1/03
CPC分类号： B29C66/71
摘要： PROBLEM TO BE SOLVED: To carry out a process of separating two or more sets of laminates into separate sets smoothly without spoiling surface smoothness of each set.
SOLUTION: The process comprises a thermo-compression bonding step P1 to form laminates A and B simultaneously, and a separation step P2 to separate the metal foil laminates into separate sets, wherein the metal foil laminates A and B are obtained by thermo-compression bonding a thermo-compression bondable organic film and a metal foil, and are discharged together from the thermo-compression bonding step P1. The surface smoothness of each set is kept from spoilage by cooling the metal foil laminates A and B in contact state, during the separation step P2.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：进行将两组或多组层压板平滑分离成不同的各种表面平滑度的方法。解决方案：该方法包括同时形成层压体A和B的热压粘合步骤P1和分离步骤P2，以将金属箔层压体分离成单独的组，其中金属箔层压体A和B通过热将热压接合有机膜和金属箔压接，并从热压接工序P1排出。在分离步骤P2期间，通过在接触状态下冷却金属箔层压体A和B，使每组的表面平滑度不变质。版权所有（C）2007，JPO＆INPIT

3. 发明专利

JP2004262981A Preparation process for polyorganosiloxane particle and preparation process for silica particle 审中-公开
公开(公告)号：JP2004262981A
公开(公告)日：2004-09-24
申请号：JP2003050417
申请日：2003-02-27
申请人： Ube Nitto Kasei Co Ltd , 宇部日東化成株式会社
发明人： SUZUKI TARO
IPC分类号： C01B33/12 , C08G77/06
摘要： PROBLEM TO BE SOLVED: To provide a process for efficiently preparing a monodisperse particulate polyorganosiloxane which is especially suitable for a liquid crystal display spacer and has a relatively large particle diameter (about 1-30 μm) controllable to a desired value in a nm order.
SOLUTION: A silicon compound having a silicon-bonded non-hydrolyzable group or groups and a silicon-bonded hydrolyzable alkoxyl group or groups is dissolved in water, then hydrolyzed and condensed to give a seed particle liquid. To this liquid, an aqueous solution containing the silicon compound or its hydrolyzate is added to conduct a seed-particle growth reaction. During the reaction, the particle diameter is measured continuously or intermittently at a fixed time interval. Thus, the objective particulate polyorganosiloxane is prepared.
COPYRIGHT: (C)2004,JPO&NCIPI

4. 发明专利

JP2002226588A ORGANIC-INORGANIC COMPOSITE GRADIENT MATERIAL AND ITS USE 失效
公开(公告)号：JP2002226588A
公开(公告)日：2002-08-14
申请号：JP2001028211
申请日：2001-02-05
申请人： UBE NITTO KASEI CO
发明人： KOIKE TADASHI , SUZUKI TARO , KOBAYASHI AKIHIRO , TACHIBANA EISUKE
IPC分类号： C08J7/04 , C08F230/04 , C08G77/442 , C08G81/02 , C09D133/00 , C09D183/10 , C09D185/00
摘要： PROBLEM TO BE SOLVED: To obtain an organic-inorganic composite gradient material with which a coating film having a relatively thick film thickness, controlling crack occurrence can be formed by a spray coating and deterioration of the coating film by a photocatalyst can be controlled when used as an intermediate film of a photocatalytically active material layer. SOLUTION: This organic-inorganic composite gradient material is formed by using (A) an organic polymer compound having a hydrolyzable metal- containing group and (B) a substance obtained by hydrolyzing a mixture comprising (b1) a specific hydrolyzable metal-containing compound and (b2) a specified hydrolyzable phenyl group-containing compound in a specific ratio.

5. 发明专利

JP2002206059A ORGANIC-INORGANIC COMPOSITE GRADIENT MATERIAL AND USE THEREOF 失效
公开(公告)号：JP2002206059A
公开(公告)日：2002-07-26
申请号：JP2001003648
申请日：2001-01-11
申请人： UBE NITTO KASEI CO
发明人： TACHIBANA EISUKE , SUZUKI TARO , NAKAYAMA NORIHIRO
IPC分类号： B32B5/14 , C08F230/04 , C08G81/02 , C08K3/00 , C08L101/02 , C09D7/12 , C09D143/00 , C09D201/02
摘要： PROBLEM TO BE SOLVED: To obtain an organic-inorganic composite gradient material having a component gradient structure in which the content of a metal component is continuously changed in the thickness direction of the material and capable of well suppressing deterioration with oxygen, light, heat, photocatalyst oxidation, etc. SOLUTION: This organic-inorganic composite gradient material includes a composite in which an organic polymer is chemically bound to a metal oxide compound and has a gradient structure in which the content of the metal component is continuously changed from the surface of the material in the depth direction and the content of a stabilizer for the polymer is substantially zero in the surface layer of the material and is continuously increasing in the depth direction.

6. 发明专利

JP2001240796A ORGANIC/INORGANIC HYBRID-INORGANIC COMPOSITE GRADIENT MATERIAL AND ITS USE 失效
公开(公告)号：JP2001240796A
公开(公告)日：2001-09-04
申请号：JP2000054018
申请日：2000-02-29
申请人： UBE NITTO KASEI CO
发明人： NAKAYAMA NORIHIRO , SUZUKI TARO , TACHIBANA EISUKE
IPC分类号： B32B9/00 , C08G77/26 , C09D1/00 , C09D175/04 , C09D183/00 , C09J1/00 , C09J175/04
摘要： PROBLEM TO BE SOLVED: To provide an organic/inorganic composite gradient material which has a component-gradient structure wherein the content of inorganic components continuously changes in the direction of the thickness of the material, generates little crack and may be formed on the surface of any kind of a substrate. SOLUTION: The organic/inorganic hybrid-inorganic composite gradient material having a component-gradient structure wherein the content of inorganic components continuously changes in the direction of the depth from the surface of the material, is formed using a coating liquid containing (a) tetraisocyanate silane and (b) an organosilicon compound of formula (I): R1nSi(OR2)4-n, wherein R1 is a (un) saturated non-hydrolyzable organic group; R2 is a 1-6C alkyl group; and n is an integer of 1-3 and/or its hydrolysate/condensate.

7. 发明专利

JP2004292644A Twin polyorganosiloxane particle and manufacturing process therefor 有权
公开(公告)号：JP2004292644A
公开(公告)日：2004-10-21
申请号：JP2003087075
申请日：2003-03-27
申请人： Ube Nitto Kasei Co Ltd , 宇部日東化成株式会社
发明人： SUZUKI TARO
IPC分类号： G02F1/1339 , C01B33/12 , C08G77/06
摘要： PROBLEM TO BE SOLVED: To provide a polyorganosiloxane particle as a spacer for a liquid crystal display that has a larger contact area per particle than conventional spherical particle spacers and a shape which does not require a sophisticated press control in manufacturing a liquid crystal display and a manufacturing process therefor.
SOLUTION: The polyorganosiloxane particle is twin-shaped. The diameter in the direction vertical to the longitudinal direction of the twin particle is minimum in the neighborhood of the center in the longitudinal direction. When the average diameter is L
3a in the direction vertical to the longitudinal direction of the twin particle, the maximum diameters L
1a and L
2a of the twin particle satisfy equations: 0.8≤L
1a /L
2a ≤1 and 20.5≤L
3a /[(L
1a +L
2a )/2]≤0.951 μm≤(L
1a +L
2a )/2≤30 μm. The manufacturing process therefor is also disclosed.
COPYRIGHT: (C)2005,JPO&NCIPI

8. 发明专利

JP2004277476A Method for producing polyorganosiloxane particle 有权
标题翻译：生产聚硅氧烷类颗粒的方法
公开(公告)号：JP2004277476A
公开(公告)日：2004-10-07
申请号：JP2003067777
申请日：2003-03-13
申请人： Ube Nitto Kasei Co Ltd , 宇部日東化成株式会社
发明人： SUZUKI TARO
IPC分类号： C01B33/12 , C08G77/06
摘要： PROBLEM TO BE SOLVED: To provide a method for producing polyorganosiloxane particles, by which the polyorganosiloxane particles having an average particle diameter of, for example, >10μm and having a single dispersed particle diameter distribution can efficiently be produced, while effectively controlling the particle diameter.
SOLUTION: This method for producing the polyorganosiloxane particles is characterized by comprising a process for hydrolyzing and condensing an aqueous solution containing a silicon compound (an alkoxysilane having non-hydrolyzable groups) in the presence of a basic catalyst to form the seed particles comprising the polyorganosiloxane particles and a process for growing the seed particles, wherein a particle diameter-growing liquid containing an anionic surfactant in a concentration satisfying the following relational expression (II): Y=α×(a×X)/(A×R) (II) [(a) is a theoretical value obtained by dividing the mol. wt. of the product produced by hydrolyzing and condensing the silicon compound by the mol. wt. of the silicon compound; Y is the concentration (mass %) of the anionic surfactant in the particle diameter-growing liquid; X is the mass (g) of the raw material used for the synthesis of the seed particles; A is the total mass of the solution used in the particle-growing process; R is the average particle diameter (μm) of the seed particles; α is a coefficient of 4.0 to 75] is added to the seed particle-forming liquid to grow the seed particles, in the process for growing the seed particles.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决问题：为了提供聚有机硅氧烷颗粒的制造方法，通过该方法可有效地制造平均粒径为例如>10μm并具有单一分散粒径分布的聚有机硅氧烷颗粒，同时有效地控制粒径。解决方案：该聚有机硅氧烷颗粒的制造方法的特征在于，在碱性催化剂的存在下，含有含有硅化合物（具有不可水解基团的烷氧基硅烷）的水溶液水解和缩合的方法，形成种子粒子包含聚有机硅氧烷颗粒和生长种子颗粒的方法，其中含有浓度满足以下关系式（II）的阴离子表面活性剂的粒径生长液：Y =α×（a×X）/（A×R ）（II）[（a））是通过除去摩尔得到的理论值。重量。通过将硅化合物水解和缩合而得到的产物。重量。的硅化合物; Y是粒径生长液中阴离子表面活性剂的浓度（质量％）; X是用于合成种子颗粒的原料的质量（g）; A是在颗粒生长过程中使用的溶液的总质量; R是种子颗粒的平均粒径（μm）; 在种子颗粒的生长过程中，将α为4.0〜75的系数加入到形成种子颗粒的液体中以生长种子颗粒。版权所有（C）2005，JPO＆NCIPI

9. 发明专利

JP2005306002A Manufacturing equipment for flexible metal foil laminate, and manufacturing method using it 有权
标题翻译：柔性金属箔层压板的制造设备及其使用的制造方法
公开(公告)号：JP2005306002A
公开(公告)日：2005-11-04
申请号：JP2005025187
申请日：2005-02-01
申请人： Ube Nitto Kasei Co Ltd , 宇部日東化成株式会社
发明人： SUZUKI TARO , MINEKI YOSHITAKA
IPC分类号： B32B15/088 , B29C43/28 , B29C43/30 , B29C43/48 , B29K20060101 , B29K79/00 , B29L9/00 , B29L31/34 , B30B5/06 , B32B15/08 , B32B27/06
CPC分类号： B29C2043/483
摘要： PROBLEM TO BE SOLVED: To provide double belt pressing equipment and the like, which enable a flexible metal foil laminate with a good appearance to be stably formed, even if the flexible metal foil laminate is continuously manufactured over a long period of time.
SOLUTION: This double belt pressing equipment is fitted with an endless belt wherein 0.2% proof stress on condition of 300°C is 1,100 N/mm
2 or more. Since this enables an increase in the durability of the endless belt and the securement of the surface smoothness of the endless belt, a scratch is prevented from being transferred to a product. Thus, the flexible metal foil laminate with the good appearance can be continuously manufactured.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：即使柔性金属箔层压板长时间连续地制造，也能够提供能够稳定地形成具有良好外观的柔性金属箔层叠体的双带式冲压装置等。。
解决方案：该双带压制设备配有环形带，其中在300℃条件下的0.2％屈服应力为1,100N / mm 2 或更高。由于能够提高环形带的耐久性和确保环形带的表面平滑性，因此防止了划痕被转移到产品。因此，可以连续地制造具有良好外观的柔性金属箔层压体。版权所有（C）2006，JPO＆NCIPI

10. 发明专利

JP2004339296A Manufacturing method for polymer particle and apparatus used for the same 审中-公开
标题翻译：用于聚合物颗粒的制造方法和用于其的装置
公开(公告)号：JP2004339296A
公开(公告)日：2004-12-02
申请号：JP2003135238
申请日：2003-05-14
申请人： Ube Nitto Kasei Co Ltd , 宇部日東化成株式会社
发明人： SUZUKI TARO
IPC分类号： C01B33/12 , C08G77/06 , C08G77/18
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method for a polymer particle wherein the manufacturing yield and CV value (standard deviation (μm) of microparticle) of the particle size are improved through inhibition of coalescence or aggregation of a seed particle at manufacturing of a polymer such as a polyorganosiloxane particle used as a spacer for a liquid crystal display device or as a standard particle. SOLUTION: In the manufacturing method for the polymer particle, a monomer having an alkoxyl group and/or a hydroxyl group is reacted in the presence of a catalyst to form the seed particle. Then, an aqueous solution containing the monomer or its hydrolysate is added to the seed particle to grow the seed particle. Here, the formation and the growth of the seed particle are performed in a reaction vessel of an inverted-cone shape. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种聚合物颗粒的制造方法，其中通过抑制种子颗粒的聚结或聚集来改善粒径的制造产率和CV值（微粒的标准偏差（μm））制造聚合物，例如用作液晶显示装置的间隔物的聚有机硅氧烷颗粒或标准颗粒。解决方案：在聚合物颗粒的制造方法中，具有烷氧基和/或羟基的单体在催化剂的存在下反应以形成种子颗粒。然后，将含有单体或其水解产物的水溶液加入到种子颗粒中以生长种子颗粒。这里，种子粒子的形成和生长在倒圆锥形状的反应容器中进行。版权所有（C）2005，JPO＆NCIPI

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