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    • 3. 发明专利
    • Detection method of solidification structure for steel
    • 钢的固结结构检测方法
    • JP2012247382A
    • 2012-12-13
    • JP2011121307
    • 2011-05-31
    • Nippon Steel & Sumitomo Metal新日鐵住金株式会社Astec Irie Co Ltd株式会社アステック入江
    • SEZE AKIFUMITANI MASAHIROFUKUNAGA SHINICHIKAMIMURA KENICHINISHIMOTO TAKUMISUEYOSHI SHOTASAKURA IKUOTAKAMUNE KENJI
    • G01N33/20
    • PROBLEM TO BE SOLVED: To provide a detection method of solidification structure for a steel type of which the concentration difference caused by segregation of a solute element being solidified is comparatively small, in particular, for low-carbon steel of which the carbon concentration is lower than or equal to 0.01 mass%.SOLUTION: A sample cross section of a steel cast piece is polished. Thereafter ultrasonic waves of two or more kinds of frequencies different from each other are alternately and intermittently applied, within a range of 30 kHz to 3 MHz, to a corrosion liquid 15 using water containing micro bubbles as a solvent. While water-resonating the corrosion liquid 15, the sample cross section is corroded and a solidification structure of steel appears. Thereafter, the steel cast piece is washed and dried, a corrosion pit formed on the sample cross section is filled with polishing powder, and a transparent adhesive tape is stuck to the sample cross section. After the polishing powder in the corrosion pit is adhered to the transparent adhesive tape, the transparent adhesive tape is released and next, the transparent adhesive tape is stuck on a white pasteboard.
    • 要解决的问题:提供一种由固化的固体元素的偏析引起的浓度差较小的钢型凝固组织的检测方法,特别是对于碳 浓度低于或等于0.01质量%。

      解决方案:抛光钢铸件的样品横截面。 此后,使用含有微气泡作为溶剂的水,在30kHz〜3MHz的范围内交替地和间歇地施加两种以上彼此不同的频率的超声波。 当腐蚀液体15产生水谐振时,样品横截面被腐蚀并出现钢的凝固结构。 然后,对钢铸件进行清洗干燥,在样品横截面上形成的腐蚀坑填充有研磨粉末,将透明胶带粘贴在试样截面上。 在腐蚀坑中的抛光粉末粘附到透明胶带上之后,透明胶带被释放,接下来将透明胶带粘贴在白色粘贴板上。 版权所有(C)2013,JPO&INPIT

    • 5. 发明专利
    • Method for detecting solidification structure of steel
    • 检测钢的固结结构的方法
    • JP2011226993A
    • 2011-11-10
    • JP2010098985
    • 2010-04-22
    • Astec Irie Co LtdNippon Steel Corp新日本製鐵株式会社株式会社アステック入江
    • SEZE AKIFUMITANI MASAHIROFUKUNAGA SHINICHIUEMURA KENICHINISHIMOTO TAKUMISUEYOSHI SHOTASAKURA IKUOTAKAMUNE KENJI
    • G01N1/32G01N1/28G01N33/20
    • PROBLEM TO BE SOLVED: To provide a method for detecting solidification structure of a type of steel which has relatively low differences in concentrations of solute elements due to segregation during solidification, particularly of a low-carbon steel which has a carbon concentration of 0.01 mass% or less.SOLUTION: After a cross section of a sample of steel cast slab is polished, the cross section of the sample is corroded to cause solidification structure of the steel to appear while applying supersonic waves of 30 kHz to 3 MHz to a corrosive liquid 15 in which microbubble-containing water is used as a solvent to subject the corrosive liquid 15 to water resonance. The sample is then washed and dried, and corroded holes formed in the cross section of the sample are filled with polishing powder. After transparent adhesive tape is stuck on the cross section of the sample to adhere the polishing powder in the corroded holes to the transparent adhesive tape, the transparent adhesive tape is removed and then stuck on a white mount.
    • 要解决的问题:提供一种用于检测固化期间由于偏析导致的固溶元素浓度差异较小的钢的固化结构的方法,特别是碳浓度低的低碳钢 0.01质量%以下。

      解决方案:抛光钢板样品的横截面后,样品的横截面被腐蚀,导致钢的凝固结构出现,同时将30 kHz至3 MHz的超声波施加到腐蚀性液体 15,其中使用含微泡的水作为溶剂使腐蚀性液体15进行水共振。 然后将样品洗涤并干燥,并在样品的横截面中形成的腐蚀孔填充有抛光粉末。 将透明胶粘带粘贴在样品的横截面上,将腐蚀的孔中的抛光粉末粘附到透明胶带上,将透明胶带除去,然后粘贴在白色的底座上。 版权所有(C)2012,JPO&INPIT

    • 6. 发明专利
    • Method for detecting steel hardened texture
    • 检测钢硬化纹理的方法
    • JP2010127759A
    • 2010-06-10
    • JP2008302567
    • 2008-11-27
    • Astec Irie Co LtdNippon Steel Corp新日本製鐵株式会社株式会社アステック入江
    • SEZE AKIFUMIFUKUNAGA SHINICHIIWASAKI JUNYAHIRATA GOKINISHIO WATARU
    • G01N33/20C23F1/00C23F1/28
    • G01N33/20C23F1/28
    • PROBLEM TO BE SOLVED: To provide a method for causing a hardened texture to appear by corrosion, and detecting the hardened texture of steel even if a type of the steel, especially low-carbon steel with a carbon concentration of 0.01 mass% or less has a low solute element concentration within the steel and it is conventionally difficult to clearly detect the hardened texture.
      SOLUTION: In the method for causing the hardened texture of the steel, a cross section of a sample of a steel casting piece is polished. A polished surface 2 of the sample 1 is downwardly placed. An immersion depth d of the polished surface 2 of the sample is 10 mm or less. The polished surface 2 is corroded. While one or both of the sample and a corrosion liquid are vibrated by ultrasonic waves, the polished surface is corroded. Since only a portion of the sample including the polished surface (the corroded surface) of the sample is immersed into the corrosion liquid and corroded, the hardened texture appears in a type of the steel, especially the low-carbon steel with a carbon concentration of 0.01 mass% or less whose hardened texture is conventionally difficult to appear.
      COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:为了提供一种使腐蚀出现硬化织构的方法,并且即使是一种钢,特别是碳浓度为0.01质量%的低碳钢,也可以检测钢的硬化织构, 以下,钢中的溶质元素浓度低,通常难以清楚地检测硬化的织构。 解决方案:在引起钢的硬化织构的方法中,对铸造件的样品的横截面进行抛光。 样品1的抛光表面2向下放置。 样品的抛光面2的浸渍深度d为10mm以下。 抛光表面2被腐蚀。 当样品和腐蚀液中的一种或两种都被超声波振动时,抛光表面被腐蚀。 由于只有包括样品的抛光表面(腐蚀表面)的样品的一部分浸入腐蚀液中并被腐蚀,所以硬化的织构呈现出一种类型的钢,特别是碳浓度低的钢 通常难以出现其硬化织构的0.01质量%以下。 版权所有(C)2010,JPO&INPIT
    • 9. 发明专利
    • Method of detecting solidification structure of steel
    • 检测钢的固结结构的方法
    • JP2010138436A
    • 2010-06-24
    • JP2008314720
    • 2008-12-10
    • Astec Irie Co LtdNippon Steel Corp新日本製鐵株式会社株式会社アステック入江
    • SEZE AKIFUMIFUKUNAGA SHINICHIOKAWA TAKESHIINOUE TSUTOMUUWAGAWA HIRONORI
    • C23F1/00B22D11/00G01N1/28
    • PROBLEM TO BE SOLVED: To provide a method of detecting a solidification structure of steel by revealing the solidification structure by corrosion, even in a grade in which solute element concentration in steel is so low that a clear solidification structure is previously difficult to be detected, especially in low carbon steel with carbon concentration of ≤0.01 mass%.
      SOLUTION: In the method of detecting the solidification structure of steel, a cross-section of a sample of a steel casting piece is polished, a surface other than a polished surface 2 of a sample 1 is electrically insulated to be an electrically insulated surface 3, and the polished surface 2 is corroded. The solidification structure is revealed even in the grade in which the solidification structure is previously difficult to be revealed, especially in low carbon steel with carbon concentration of ≤0.01 mass%, by electrically insulating the surface other than the polished surface (corroded surface) of the sample, and advancing corrosion only on the polished surface.
      COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:提供一种通过暴露出腐蚀的凝固结构来检测钢的凝固组织的方法,即使在钢中的溶质元素浓度低到以前难以清除凝固结构的等级 特别是在碳浓度≤0.01质量%的低碳钢中。 解决方案:在检测钢的凝固结构的方法中,对钢铸件的样品的横截面进行抛光,将除了样品1的抛光表面2以外的表面电绝缘为电 绝缘表面3,并且抛光表面2被腐蚀。 即使在预先难以显示固化结构的级别,特别是在碳浓度为≤0.01质量%的低碳钢中,通过将除了抛光表面(腐蚀表面)以外的表面电绝缘, 样品,并仅在抛光表面上推进腐蚀。 版权所有(C)2010,JPO&INPIT
    • 10. 发明专利
    • Method for detecting solidified structure of steel
    • 检测钢的固结结构的方法
    • JP2010125483A
    • 2010-06-10
    • JP2008302566
    • 2008-11-27
    • Astec Irie Co LtdNippon Steel Corp新日本製鐵株式会社株式会社アステック入江
    • SEZE AKIFUMIFUKUNAGA SHINICHIIWASAKI JUNYASAKURA IKUOYOSHIOKA KEIGO
    • B22C9/00C23F1/00
    • C23F1/28C21D1/55G01N33/20
    • PROBLEM TO BE SOLVED: To provide a method for detecting a solidified structure of steel, even of low carbon steel in which a solute element concentration in the steel is low, and especially a carbon concentration is ≤0.01 mass%, by identifying the solidified structure by corrosion.
      SOLUTION: In the method for detecting the solidified structure of steel, a cross-section of a sample of a steel cast piece is polished, and the sample is heated at 40-90°C; then the polished surface of the sample is contacted to corrosive liquid, and the polished surface is corroded. Additionally, the corrosive liquid is heated at 40-90°C, and then the polished surface of the sample is contacted to the corrosive liquid. Even after the sample is contacted to the corrosive liquid, the corrosive liquid is not decreased in temperature, corrosion performance when using hot corrosive liquid is maintained in high level, electrochemical corrosion using potential difference by a difference in solute concentration is developed in a short period of time, and a clear solidified structure is identified. The temperature of the corrosive liquid is preferably -10 to -5°C, or +5°C or more to the temperature of the sample.
      COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:提供一种用于检测钢的固化结构的方法,即使是钢中的固溶元素浓度低的碳素钢,特别是碳浓度≤0.01质量%的低碳钢,通过鉴定 凝固结构受腐蚀。 解决方案:在钢的凝固结构检测方法中,对铸钢件样品的截面进行抛光,将样品加热至40〜90℃; 然后将样品的抛光表面与腐蚀性液体接触,并抛光表面被腐蚀。 此外,将腐蚀性液体加热至40-90℃,然后将样品的抛光表面与腐蚀性液体接触。 即使样品与腐蚀性液体接触,腐蚀性液体的温度也不会降低,使用热腐蚀性液体时的腐蚀性能保持在高水平,电解腐蚀使用电位差由溶质浓度差异在短时间内发展 的时间,并确定了明确的固化结构。 腐蚀性液体的温度相对于样品的温度优选为-10〜-5℃或+ 5℃以上。 版权所有(C)2010,JPO&INPIT