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    • 2. 发明公开
    • EQUILIBRIUM BOMB FOR STUDYING PHASE BEHAVIOUR OF HYDROCARBONS
    • 平衡活塞调查烃类相行为
    • EP1677100A4
    • 2008-04-30
    • EP03751659
    • 2003-09-15
    • OBSCHESTVO S OGRANICHENNOI OTV
    • KOUVANDYKOV ILIS SHARIFOVICHGAFAROV NAIL ANATOLIEVICH
    • G01N25/02G01N25/22G01N25/08G01N33/28
    • G01N33/2823G01N25/08G01N25/70
    • The inventive equilibrium bomb for studying phase behaviour of hydrocarbons comprises a thermostatic high-pressure cylindrical container (1) provided with viewing ports (2) embodied at the level on a light source (3), top (10) and bottom (11) reflectors which are disposed inside the container and rigidly connected to each other by means of a membrane (12) and a dividing piston (13) fixed to the bottom reflector (11). Said top reflector (10) is embodied in the form of cylinder whose base comprises a recess on the side of the membrane which forms two symmetrical mirror surfaces tilted at an angle of 45 DEG with respect to the cylinder axis. The bottom reflector (11) is embodied in the form of a cylinder whose one base comprises two flat mirror faces symmetrically tilted at an angle of 45 DEG with respect to the cylinder axis, the other base thereof is provided with a radial slot which is oriented perpendicularly to the plane of the membrane (12). The reflectors are spaced with respect to the internal wall of the container. Said bomb is provided with a bypass tube (15) which connects spaces above and below the piston by means of a closing valve. The radial slot of the bottom reflector is arranged in a perpendicular direction with relation to the membrane (12) which is fixed with the aid of two grooves embodied on the internal surface of the container (1) in a perpendicular direction to the axis of the viewing ports (2).
    • 3. 发明公开
    • EQUILIBRIUM BOMB FOR STUDYING PHASE BEHAVIOUR OF HYDROCARBONS
    • GLEICHGEWICHTSKOLBEN ZUR UNTERSUCHUNG DES PHASENVERHALTENS VON KOHLENWASSERSTOFFEN
    • EP1677100A1
    • 2006-07-05
    • EP03751659.8
    • 2003-09-15
    • Obschestvo S Ogranichennoi Otvetstvennostju "Orenburggasprom"
    • KOUVANDYKOV, Ilis SharifovichGAFAROV, Nail Anatolievich
    • G01N25/02
    • G01N33/2823G01N25/08G01N25/70
    • The inventive equilibrium bomb for studying a phase behavior of hydrocarbons comprises a temperature-controlled high-pressure cylindrical container (1) provided with viewing ports (2) embodied at a level of a light source (3), top (10) and bottom (11) reflectors being disposed inside the container and rigidly connected to each other by means of a membrane (12) and a dividing piston (13) fixed to the bottom reflector (11). Said top reflector (10) is made to the shape of a cylinder whose base comprises a recess as viewed from the membrane which forms two symmetrical mirror surfaces tilted at an angle of 45° with respect to the cylinder axis. The bottom reflector (11) is made to the shape of a cylinder whose one base comprises two flat mirror faces symmetrically tilted at an angle of 45° with respect to the cylinder axis, the other base thereof is provided with a radial slot which is oriented perpendicular to the plane of the membrane (12). The reflectors are spaced with respect to a container interior wall. Said bomb is provided with a bypass tube (15) which connects spaces above and below the piston to each other by means of a stop valve. The radial slot of the bottom reflector is arranged in a perpendicular direction with relation to the membrane (12) which is fixed with the aid of two grooves on the interior surface of the container (1) in a perpendicular direction to the axis of the viewing ports (2).
    • 用于研究碳氢化合物相行为的本发明的平衡弹簧包括温度控制的高压圆柱形容器(1),其设置有在光源(3),顶部(10)和底部(10)的水平上实现的观察口(2) 11)反射器设置在容器内部并且通过膜(12)和固定到底部反射器(11)的分隔活塞(13)彼此刚性地连接。 所述顶部反射器(10)制成汽缸的形状,其底部包括从膜观察的凹部,其形成相对于气缸轴线以45°的角度倾斜的两个对称的镜面。 底部反射器(11)制成圆柱体,其一个底座包括相对于气缸轴线以45°的角度对称倾斜的两个平面镜面,另一个底座设有径向槽 垂直于膜(12)的平面。 反射器相对于容器内壁间隔开。 所述炸弹设置有旁通管(15),其通过截止阀将活塞的上方和下方的空间相互连接。 底部反射器的径向槽相对于膜(12)在垂直方向上布置,膜(12)借助于容器(1)的内表面上的两个凹槽在与观察轴线垂直的方向上固定 港口(2)。
    • 7. 发明公开
    • Verfahren zur Messung eines Partialdrucks und Vorrichtung zur Durchführung des Verfahrens
    • Verfahren zur Messung eines Partialdrucks und Vorrichtung zurDurchführungdes Verfahrens
    • EP1669744A1
    • 2006-06-14
    • EP04405766.9
    • 2004-12-10
    • Gmeiner, Paul
    • Gmeiner, Paul
    • G01N25/70
    • G01N25/70G01N33/0016
    • Das Verfahren dient der Messung des Partialdrucks (p 0L , p 0W§ ) einer Komponente (L, W) eines in einem Trocknungsprozess anfallenden Gemischs aus einem Inertgas (L) und dem Dampf wenigstens einer Flüssigkeit (W, S) mit guter Genauigkeit im Messbereich zwischen 0,02 und 2 mbar. Es werden folgende Verfahrensschritte ausgeführt:

      das Gemisch wird in einer evakuierbaren Messkammer (1) durch Verkleinern des Volumens der Messkammer (1) mit einem Kompressionsfaktor komprimiert,
      beim Komprimieren werden der Verlauf des Totaldrucks und der Temperatur des Gemischs in Abhängigkeit vom Kompressionsfaktor erfasst,
      der Kompressionsvorgang wird solange fortgeführt wird bis Kondensation des Dampfs einsetzt, und
      aus hierbei ermittelten Werten des Totaldrucks (p 1tot (T), p 1.1tot (T)), der Temperatur (T) und des Kompressionsfaktors (KF 1 , KF 1.1 ) zumindest beim und/oder nach dem Einsetzen der Kondensation sowie gegebenenfalls dem Totaldruck (p 0tot (T)) vor der Kondensation und/oder dem Kondensationsdruck (p 1w (T)) des Dampfs bei der Kondensationstemperatur (T) wird dann der Partialdruck (p 0L (T), p 0w (T)) der Komponente (L, W) bestimmt.

      Alternativ kann am komprimierten Gemisch der Taupunkt gemessen und hieraus und aus dem Kompressionsfaktor bei der Taupunktsmessung der Partialdruck (pow) des Dampfs ermittelt werden.
    • 在0.02毫巴和2毫巴之间的测量范围内,在包括惰性气体和至少一种流体的蒸气的干燥过程中测量混合物的组分的分压,其测量范围高精度。 混合物在可抽空测量室中以压缩因子压缩,其体积减小。 进行压缩处理,直到发生蒸气冷凝。 至少在冷凝发生期间和/或之后从总压力(p1 tot(T),p1.1 tot(T)),温度(T)和压缩因子(KF1,KF1.1)获得的值 并且可能在冷凝温度(T),分压(P OL(T)),p(...)之间的冷凝前和/或冷凝压力(1w(T))之间的总压力(p0 tot(T) 确定组分(L,W)的OW(T)。