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    • 1. 发明公开
    • COMPOSITE DEFOAMING METHOD FOR HIGH-VISCOSITY PURE-CHITOSAN SPINNING SOLUTION
    • ZUSAMMUSTRETZTESENTSCHÄUMUNGSVERFAHRENFÜRHOCHVISKOSESPINNLÖSUNGAUS REINEM CHITOSAN
    • EP3042706A1
    • 2016-07-13
    • EP14841045.9
    • 2014-09-01
    • Hismer Bio-technology Co., Ltd.
    • ZHOU, JiacunHU, Guangmin
    • B01D19/02
    • B01D19/02D01D1/103D01F9/00
    • The present invention discloses a combined degassing method for a high-viscosity pure-chitosan spinning solution, comprising the following steps of:
      step 1, thoroughly dissolving the spinning solution in a dissolution vessel for subsequent use, the viscosity thereof reaching 450,000-500,000 mpa·s;
      step 2, delivering the spinning solution in step 1 to the feed port of a degassing vessel from the dissolution vessel after filtration;
      step 3, in the degassing vessel, under the conditions of vacuumizing and maintaining the inner pressure of the degassing vessel to be 500-3,000 Pa, performing continuous treatment by a combined degassing process integrating separation, film-scraping, lifting and shear; and
      step 4, sampling at a sampling port for the detection of degassing degree, finishing the degassing operation if the detection result is eligible, otherwise repeating step (3) until the detection result is eligible.
      The degassing method provided by the present invention has high degassing efficiency and good degassing effect, and is applicable to spinning solutions of a wide range of viscocity.
    • 本发明公开了一种高粘度纯壳聚糖纺丝溶液的组合脱气方法,其特征在于包括以下步骤:步骤1,将纺丝溶液彻底溶解在溶解容器中,随后使用,其粘度达到45万〜50万mpa· S; 步骤2,在步骤1中将纺丝溶液从过滤后的溶解容器输送到脱气容器的进料口; 步骤3,在除气容器中,在真空并保持脱气容器的内部压力为500-3000Pa的条件下,通过一体化分离,刮膜,提升和剪切的脱气工艺进行连续处理; 步骤4,在取样口采样以检测脱气度,如果检测结果合格,则完成脱气操作,否则重复步骤(3),直到检测结果符合条件。 本发明提供的脱气方法具有高脱气效率和良好的脱气效果,适用于宽范围粘度的纺丝溶液。
    • 4. 发明公开
    • ELECTROSPINNING APPARATUS
    • 电子设备
    • EP2987894A1
    • 2016-02-24
    • EP14785421.0
    • 2014-02-26
    • Finetex Ene, Inc.
    • PARK, Jong-Chul
    • D01D5/00D01D4/00D01D13/00
    • D01D5/0069D01D1/09D01D1/103D01D5/34D01F13/00Y02P70/625
    • The present invention relates to an electrospinning apparatus, and the purpose of the present invention is to provide an electrospinning apparatus capable of producing nanofiber having various ingredients and thicknesses by controlling the temperature of at least one solution discharged from nozzles mounted on the tubular bodies of a nozzle block and thus controlling the viscosity of the solution which is electrospun; producing nanofiber having uniform quality without applying a density difference and a voltage difference by disposing the front end portions of the nozzles in a flare shape; and mass-producing nanofiber at a low cost as well as reducing the amount of the solution used by removing an overflow prevention system and using a metering pump alone or by using the metering pump and the overflow prevention system alternatively or in a hybrid manner.
    • 本发明涉及一种电纺丝装置,并且本发明的目的是提供一种电纺丝装置,该装置能够通过控制从安装在管状体上的喷嘴排出的至少一种溶液的温度来制造具有各种成分和厚度的纳米纤维, 喷嘴块并因此控制电纺溶液的粘度; 通过将喷嘴的前端部设置成喇叭形而不施加密度差和电压差,从而生产具有均匀质量的纳米纤维; 并且以低成本批量生产纳米纤维,并且通过单独使用计量泵或者通过使用计量泵和溢出防止系统交替地或以混合方式来减少通过去除溢出防止系统而使用的溶液的量。
    • 9. 发明公开
    • DEFOAMING APPARATUS FOR HIGH-VISCOSITY PURE-CHITOSAN SPINNING SOLUTION
    • 消泡适用于高粘度纺丝溶液纯壳聚糖
    • EP3042705A4
    • 2016-08-17
    • EP14841017
    • 2014-09-01
    • HISMER BIO TECHNOLOGY CO LTD
    • ZHOU JIACUNHU GUANGMIN
    • B01D19/02B01D19/00
    • B01D19/02B01D19/0052D01D1/103D01F9/00
    • A degassing device for high-viscocity pure-chitosan spinning solutions is provided, comprising a reaction vessel (1) and a stirring device (2). A feed port (3) and a vacuum port (5) are disposed at the upper part of the reaction vessel (1), an inner cylinder body (9) is fixedly disposed in the center position of the reaction vessel (1) which is also provided with a discharge port (4), the upper cylinder opening of the inner cylinder body (9) is closed and the lower cylinder opening is open, an umbrella-shaped dispersion plate (10) is fixedly disposed at the periphery of the upper half part of the inner cylinder body (9), a gap is formed between the outer edge of the umbrella-shaped dispersion plate (10) and the inner wall of the reaction vessel (1), and small liquid outlet holes (11) are distributed on the part of the inner cylinder body (9) above the umbrella-shaped dispersion plate (10). The stirring device (2) comprises a stirring shaft (12) with a screw propeller (14) and a stirring power unit (13), the upper end of the stirring shaft (12) is mounted to the stirring power unit (13), the stirring shaft (12) passes through a mechanical sealing device (16) and enters the reaction vessel (1) with the lower end being fixed on a seat-mounted bearing (6), the stirring shaft (12) is superposed with the axial line of the inner cylinder body (9), and a gap is formed between the inner wall of the inner cylinder body (9) and the screw propeller (14).
    • 10. 发明公开
    • DEFOAMING APPARATUS FOR HIGH-VISCOSITY PURE-CHITOSAN SPINNING SOLUTION
    • 用于高粘度纯化壳聚糖纺丝溶液的消泡装置
    • EP3042705A2
    • 2016-07-13
    • EP14841017.8
    • 2014-09-01
    • Hismer Bio-technology Co., Ltd.
    • ZHOU, JiacunHU, Guangmin
    • B01D19/02
    • B01D19/02B01D19/0052D01D1/103D01F9/00
    • A degassing device for high-viscocity pure-chitosan spinning solutions is provided, comprising a reaction vessel (1) and a stirring device (2). A feed port (3) and a vacuum port (5) are disposed at the upper part of the reaction vessel (1), an inner cylinder body (9) is fixedly disposed in the center position of the reaction vessel (1) which is also provided with a discharge port (4), the upper cylinder opening of the inner cylinder body (9) is closed and the lower cylinder opening is open, an umbrella-shaped dispersion plate (10) is fixedly disposed at the periphery of the upper half part of the inner cylinder body (9), a gap is formed between the outer edge of the umbrella-shaped dispersion plate (10) and the inner wall of the reaction vessel (1), and small liquid outlet holes (11) are distributed on the part of the inner cylinder body (9) above the umbrella-shaped dispersion plate (10). The stirring device (2) comprises a stirring shaft (12) with a screw propeller (14) and a stirring power unit (13), the upper end of the stirring shaft (12) is mounted to the stirring power unit (13), the stirring shaft (12) passes through a mechanical sealing device (16) and enters the reaction vessel (1) with the lower end being fixed on a seat-mounted bearing (6), the stirring shaft (12) is superposed with the axial line of the inner cylinder body (9), and a gap is formed between the inner wall of the inner cylinder body (9) and the screw propeller (14).
    • 本发明提供了一种高粘度纯壳聚糖纺丝原液脱气装置,包括反应釜(1)和搅拌装置(2)。 在反应容器(1)的上部配置有供给口(3)和真空口(5),在反应容器(1)的中心位置固定有内筒体(9) 还设有排气口(4),内筒体(9)的上筒开口关闭,下筒开口打开,伞状分散板(10)固定设置在鞋帮 在内筒体9的一半部分,在伞形分散板10的外缘与反应容器1的内壁之间形成间隙,小出液孔11为 分布在伞状分散板(10)上方的内筒体(9)的部分上。 搅拌装置(2)包括带有螺旋桨(14)和搅拌动力装置(13)的搅拌轴(12),搅拌轴(12)的上端安装在搅拌动力装置(13)上, 搅拌轴(12)通过机械密封装置(16)进入反应容器(1),其下端固定在座椅安装轴承(6)上,搅拌轴(12)与轴向 内筒体9的内壁与内筒体9的内壁与螺旋桨14之间形成间隙。