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1. 发明公开

EP3169456A1 RECOVERY AND USE OF WOOD ACETYLATION FLUID 有权
标题翻译：木材乙酰化液的回收利用
公开(公告)号：EP3169456A1
公开(公告)日：2017-05-24
申请号：EP15738680.6
申请日：2015-07-17
申请人： Tricoya Technologies Ltd
发明人： BENSTEAD, Stephen John , PAINTER, Benjamin Thomas
IPC分类号： B08B3/06 , B27K3/34 , C07C51/44
CPC分类号： C07C51/56 , B27K3/34 , B27K3/346 , C07C51/44 , C07C53/08 , C07C53/12
摘要： Disclosed is the integration of the production of acetic anhydride from ketene, and the acetylation of wood using acetylation fluid comprising acetic acid and acetic anhydride. The invention involves recirculating acetylation fluid recovered from wood acetylation to a unit for the production of acetic anhydride from acetic acid and ketene. The acetic anhydride product stream can, in turn, be directly used as a wood acetylation fluid.
摘要翻译：公开了乙烯酮生产乙酸酐的集成和乙酸乙酰化流体（包括乙酸和乙酸酐）对木材的乙酰化。本发明涉及将从木材乙酰化回收的乙酰化流体再循环至由乙酸和乙烯酮生产乙酸酐的单元。乙酸酐产物流又可以直接用作木材乙酰化液。

2. 发明公开

EP2964602A2 PROCESS 审中-公开
标题翻译：处理
公开(公告)号：EP2964602A2
公开(公告)日：2016-01-13
申请号：EP14709238.1
申请日：2014-03-06
申请人： BP Chemicals Limited
发明人： HENNIGAN, Sean, Anthony
IPC分类号： C07C51/12 , C07C53/08 , C07C53/12
CPC分类号： C07C51/56 , C07C51/12 , C07C51/42 , C07C51/44 , C07C51/573 , C07C53/08 , C07C53/12
摘要： A continuous process for the co-production of acetic acid and acetic anhydride by (a) contacting carbon monoxide with a liquid reaction composition comprising methyl acetate, dimethyl ether or a mixture thereof, a Group VIII metal catalyst, methyl iodide, acetic acid, acetic anhydride, water in a concentration of 0.1 wt % or less, (b) withdrawing liquid reaction composition from the reaction zone and introducing at least a portion of the withdrawn liquid reaction composition into a flash separation zone, and (c) removing from the flash separation zone a vapour fraction comprising acetic anhydride, acetic acid and methyl iodide and a liquid fraction comprising acetic anhydride, and Group VIII metal catalyst in which at least one of the liquid reaction composition and the withdrawn liquid reaction composition introduced into the flash separation zone comprises at least one metal salt selected from salts of Group IA and Group IIA metals and the molar ratio of acetic acid to acetic anhydride in the vapour fraction removed from the flash separation zone is maintained at greater than or equal to 1, preferably greater than or equal to 1.2.
摘要翻译：（a）使一氧化碳与包含乙酸甲酯，二甲醚或其混合物，第VIII族金属催化剂，甲基碘，乙酸，乙酸的液体反应组合物接触酸酐，浓度为0.1重量％或更低的水，（b）从反应区取出液体反应组合物，并将至少一部分取出的液体反应组合物引入闪蒸分离区，和（c）从闪蒸中除去分离区，包含乙酸酐，乙酸和甲基碘的蒸气馏分和包含乙酸酐的液体馏分;以及第VIII族金属催化剂，其中引入闪蒸分离区中的液体反应组合物和引出的液体反应组合物中的至少一种包含至少一种选自IA族和IIA族金属盐的金属盐和乙酸与乙酸酐的摩尔比将从闪蒸分离区移出的蒸气馏分中的e保持在大于或等于1，优选大于或等于1.2。

3. 发明公开

EP2938592A1 SYSTEMS AND METHODS FOR PROCESSING VARIABLE ACETYL STREAMS 有权
标题翻译：系统VERFAHREN ZUR VERARBEITUNGVERÄNDERLICHERACETYLSTRÖME
公开(公告)号：EP2938592A1
公开(公告)日：2015-11-04
申请号：EP13821315.2
申请日：2013-12-19
申请人： Eastman Chemical Company
发明人： WELLMAN, Gregory, Abbott, Jr. , BAYS, Joseph, Nathaniel , KLINE, Robert, Sterling
IPC分类号： C07C51/087 , C07C51/44 , C07C51/573 , C07C53/08 , C07C53/12
CPC分类号： B01J19/00 , C07C51/087 , C07C51/44 , C07C51/573 , C07C67/00 , C07C53/08 , C07C53/12
摘要： The invention provides systems and processes for concentrating acetic acid and acetic anhydride streams. The systems allow operation of equipment used for such concentrations in two or more modes of operation. At least one mode is intended to produce a concentrated or purified acetic acid stream. At least one other mode is intended to produce a concentrated or purified acetic anhydride stream.
摘要翻译：本发明提供用于浓缩乙酸和乙酸酐流的系统和方法。这些系统允许在两种或更多种操作模式中操作用于这种浓度的设备。至少一种模式旨在产生浓缩或纯化的乙酸流。至少一种其他模式旨在产生浓缩或纯化的乙酸酐流。

4. 发明公开

EP2637998A1 PROCESS FOR REFINING CRUDE ACETYLS MIXTURE 有权
标题翻译：精炼乙酰混合物的方法
公开(公告)号：EP2637998A1
公开(公告)日：2013-09-18
申请号：EP11791113.1
申请日：2011-11-09
申请人： Eastman Chemical Company
发明人： MAYFIELD, George, Geiger , LANE, Donald, Wayne , SCHISLA, Robert, Melvin , DYSON, Henry , BEWLEY, Jerry, Lee
IPC分类号： C07C51/44 , C07C51/573 , C07C53/08 , C07C53/12
CPC分类号： C07C67/54 , C07C51/44 , C07C51/573 , C07C69/18 , C07C53/08 , C07C53/12
摘要： Disclosed is a process for refining a crude acetyls mixture produced by carbonylation wherein the mixture comprises acetic anhydride, acetic acid, ethylidene diacetate and iodine-containing compounds to produce a mixture of acetic anhydride and acetic acid containing reduced levels of iodine and ethylidene diacetate impurities.
摘要翻译：本发明公开了一种精制羰基化产生的粗制乙酰基混合物的方法，其中混合物包含乙酸酐，乙酸，二乙酸亚乙基酯和含碘化合物以产生含有降低水平的碘和亚乙基二乙酸酯杂质的乙酸酐和乙酸的混合物。

5. 发明授权

EP2137128B1 HIGH SHEAR SYSTEM AND PROCESS FOR THE PRODUCTION OF ACETIC ANHYDRIDE 有权
标题翻译：系统和方法高剪切生产乙酸酸酐
公开(公告)号：EP2137128B1
公开(公告)日：2013-04-24
申请号：EP08770729.5
申请日：2008-06-11
申请人： H R D Corporation
发明人： BAGHERZADEH, Ebrahim , HASSAN, Abbas , ANTHONY, Rayford G. , BORSINGER, Gregory R. , HASSAN, Aziz
IPC分类号： B01J19/18 , B01F7/00 , B01F13/10 , C07C51/54 , C07C51/12 , C07C51/15
CPC分类号： C07C51/56 , B01F7/00766 , B01F13/1013 , B01F13/1016 , B01J8/025 , B01J8/20 , B01J19/0066 , B01J19/1806 , B01J2219/00006 , B01J2219/00779 , Y02P20/582 , C07C53/12

6. 发明公开

EP2137128A1 HIGH SHEAR SYSTEM AND PROCESS FOR THE PRODUCTION OF ACETIC ANHYDRIDE 有权
标题翻译：系统和方法高剪切生产乙酸酸酐
公开(公告)号：EP2137128A1
公开(公告)日：2009-12-30
申请号：EP08770729.5
申请日：2008-06-11
申请人： H R D Corporation
发明人： BAGHERZADEH, Ebrahim , HASSAN, Abbas , ANTHONY, Rayford G. , BORSINGER, Gregory R. , HASSAN, Aziz
IPC分类号： C07C51/54 , C07C51/12 , C07C51/15
CPC分类号： C07C51/56 , B01F7/00766 , B01F13/1013 , B01F13/1016 , B01J8/025 , B01J8/20 , B01J19/0066 , B01J19/1806 , B01J2219/00006 , B01J2219/00779 , Y02P20/582 , C07C53/12
摘要： A system and method for a high shear mechanical device incorporated into a process for the production of acetic anhydride as a reactor device is shown to be capable of decreasing mass transfer limitations, thereby enhancing the process. A system for the production of acetic anhydride including the mixing of catalyst and acetic acid via a high shear device.

7. 发明授权

EP1558556B1 FLEXIBLES VERFAHREN ZUR GEMEINSAMEN HERSTELLUNG VON (I) AMEISENSÄURE,(II) EINER CARBONSÄURE MIT MINDESTENS ZWEI KOHLENSTOFFATOMEN UND/ODER DEREN DERIVATEN UND (III) EINES CARBONSÄUREANHYDRIDS 有权
标题翻译：灵活的方法为（I）甲酸，（II）炭酸与至少两个碳原子和/或其衍生物以及（III）的羧酸酐THE PRODUCTION
公开(公告)号：EP1558556B1
公开(公告)日：2009-03-18
申请号：EP03769425.4
申请日：2003-10-21
申请人： BASF SE
发明人： PASTRE, Jörg , EXNER, Kai Michael , STÜER, Wolfram , GEISSLER, Elke , MACHHAMMER, Otto
IPC分类号： C07C51/54 , C07C51/09 , C07C67/10 , C07C51/56 , C07C53/122 , C07C53/124 , C07C63/313 , C07C53/02 , C07C69/14 , C07C53/12
CPC分类号： C07C51/54 , C07C51/09 , C07C51/56 , Y02P20/582 , C07C53/02 , C07C57/04 , C07C53/124 , C07C53/122 , C07C63/313 , C07C53/12
摘要： Disclosed is a method for jointly producing (i) formic acid (III); (ii) a carboxylic acid comprising at least two carbon atoms (II) and/or the derivatives thereof; and (iii) a carboxylic acid anhydride (VII). According to said method, (a) a formic acid ester (I) is transesterified to formic acid (III) and the corresponding carboxylic acid ester (IV) by means of a carboxylic acid comprising at least two carbon atoms (II); (b) at least one portion of the carboxylic acid ester (IV) formed in step (a) is carbonylated in order to obtain the carboxylic acid anhydride (V); and (c) at least one portion of the carboxylic acid anhydride (V) formed in step (b) is further dehydrated by means of a carboxylic acid (VI) so as to form a carboxylic acid anhydride (VII) and the carboxylic acid (II).

8. 发明公开

EP1966115A1 CARBONYLATION PROCESS 有权
标题翻译：羰基化
公开(公告)号：EP1966115A1
公开(公告)日：2008-09-10
申请号：EP06808636.2
申请日：2006-11-22
申请人： BP Chemicals Limited
发明人： BEAVIS, Richard , HENNIGAN, Sean, Anthony , MUSKETT, Michael, James
IPC分类号： C07C51/12 , C07C53/08
CPC分类号： C07C51/44 , C07C51/12 , Y02P20/582 , C07C53/12 , C07C53/08
摘要： A process for the carbonylation of an alcohol and/or reactive derivative thereof, in which one or more reaction zone feed streams are fed to a reaction zone in which exothermic carbonylation takes place to produce one or more product streams. Heat from at least a portion of the one or more product streams is fed to a first heat-exchange stream, such as a supply of pressurised steam. The process is characterised by heat from a second heat-exchange stream, having a temperature lower than that of the one or more product streams, being transferred to a reaction zone feed stream, so that the one or more product streams comprise heat originating from the second heat-exchange stream and heat generated by the exothermic carbonylation reaction. Thus, heat originating from the second heat-exchange stream can be transferred to the first heat-exchange stream, resulting in reduced heat loss and greater process efficiency.

9. 发明公开

EP1778613A1 ACETATE ANHYDRIDE AND ACETATE ESTER CO-PRODUCTION 有权
公开(公告)号：EP1778613A1
公开(公告)日：2007-05-02
申请号：EP05851206.2
申请日：2005-08-11
申请人： Celanese International Corporation
发明人： WARNER, R., Jay
IPC分类号： C07C51/56 , C07C53/12 , C07C67/08 , C07C69/14 , C07C45/89 , C07C49/90
CPC分类号： C07C51/56 , C07C45/89 , C07C67/08 , C07C49/88 , C07C53/12 , C07C69/14
摘要： A method of co-producing acetic anhydride and an acetate ester includes pyrolizing acetic acid at elevated temperature to produce a first ketene stream, the first ketene stream being a vapor phase stream comprising ketene, acetic acid and water; cooling the first ketene stream to condense acetic acid and water therefrom, thereby generating (i) a weak acid aqueous stream and (ii) a ketene feed stream; feeding the ketene feed stream to an acetic anhydride reactor where the ketene is reacted with acetic acid to produce acetic anhydride; concurrently with step (c ), feeding the weak acid aqueous stream to an esterification reactor wherein acetic acid in the weak acid stream is reacted with an organic alcohol to produce an acetate ester. Preferably, the organic alcohol is selected from organic alcohols which (i) form acetate esters which esters and optionally alcohols provide azeotropic mixtures with water and (ii) wherein the azeotropic mixtures have a water content greater than the amount of water generated by reaction of the alcohol with acetic acid to facilitate azeotropically separating the acetate ester from the reaction mixture.

10. 发明授权

EP0665210B2 PROCESS FOR PRODUCING ACETIC ANHYDRIDE ALONE OR BOTH OF ACETIC ANHYDRIDE AND ACETIC ACID 失效
标题翻译：用于生产乙酸酐或乙酸酐和乙酸的混合物
公开(公告)号：EP0665210B2
公开(公告)日：2005-11-23
申请号：EP94922379.6
申请日：1994-08-16
申请人： DAICEL CHEMICAL INDUSTRIES, LTD.
发明人： MORIMOTO, Yoshiaki , TANIGAWA, Hiroto , AKITA, Kazuyuki
IPC分类号： C07C53/08 , C07C53/12 , C07C51/12 , C07C51/44 , B01J31/16 , C07C51/56 , C07C51/573
CPC分类号： C07C51/56 , C07C51/12 , C07C51/44 , C07C51/573 , C07C53/08 , C07C53/12
摘要： A process for producing acetic anhydride alone or both of acetic anhydride and acetic acid by the reaction of methyl acetate and/or dimethyl ether and, as optional component(s), water and/or methanol with carbon monoxide alone or both of carbon monoxide and hydrogen in the presence of a rhodium compound and methyl iodide as the principal catalysts, wherein trace impurities causative of tar generation is removed by separating the same through distillation in the evaporator and/or in the subsequent refining step, thus reducing the generation of the tar which otherwise turns into a contaminant.

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