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    • 3. 发明公开
    • METHOD AND SYSTEM FOR PREPARING HIGH-PURITY HYDROGEN CHLORIDE
    • VERFAHREN UND SYSTEM ZUR HERSTELLUNG VON HOCHREINEM CHLORWASSERSTOFF
    • EP2617678A4
    • 2014-03-05
    • EP12830913
    • 2012-03-09
    • HONG IN CHEMICAL CO LTD
    • LEE JAE KUNLEE BUM YONG
    • C01B7/07B01D3/14B01D15/08B01D53/26C01B7/01C07B63/00
    • C01B7/012B01D53/261C01B7/0712C01B7/0743
    • The present invention provides a method for producing high-purity hydrogen chloride, comprising the steps of: purifying each of crude hydrogen and crude chlorine as raw materials to a purity of 99.999% or higher; reacting an excessive molar amount of the purified hydrogen with the purified chlorine at a temperature ranging from 1,200 °C to 1,400 °C to synthesize hydrogen chloride; converting the hydrogen chloride to a liquid state by compression; and purifying the hydrogen chloride and separating unreacted hydrogen by fractional distillation. The invention also provides a system for carrying out the method. According to the method and system, an environmentally friendly production process can be provided, which can easily produce a large amount of hydrogen chloride having a purity of 3 N (99.9%)-6 N (99.9999%) in a cost-effective manner and enables energy consumption to be significantly reduced.
    • 本发明提供高纯度氯化氢的制造方法,其特征在于,以粗纯氢和粗氯为原料纯化纯度为99.999%以上的步骤。 在1200℃至1400℃的温度范围内使纯化氢与纯化氯反应过量,合成氯化氢; 通过压缩将氯化氢转化为液态; 并通过分馏纯化氯化氢和分离未反应的氢。 本发明还提供了一种用于执行该方法的系统。 根据该方法和系统,可以提供一种环保生产方法,其可以以成本有效的方式容易地产生纯度为3N(99.9%)-6N(99.9999%)的大量氯化氢, 能够显着降低能耗。
    • 7. 发明公开
    • VERFAHREN ZUR HERSTELLUNG VON CHLOR AUS CHLORWASSERSTOFF UND SAUERSTOFF
    • EP2027064A1
    • 2009-02-25
    • EP07725513.1
    • 2007-05-21
    • Bayer MaterialScience AG
    • WEBER, RainerBULAN, AndreasHAAS, MichelWARSITZ, RafaelWERNER, Knud
    • C01B7/04
    • B01D53/22B01D53/1456B01D2257/2045B01D2257/2064C01B7/04C01B7/0743Y02P20/154
    • The invention relates to a method for producing chlorine by a) the thermal reaction of hydrogen chloride with oxygen using catalysts and/or by the non-thermally activated reaction of hydrogen chloride with oxygen, in which b) the gaseous mixture produced during the reaction a), consisting at least of the target products chlorine and water, non-converted hydrogen chloride and oxygen, additional minor constituents such as carbon dioxide and nitrogen and optionally phosgene, is cooled to condense hydrochloric acid, c) the liquid hydrochloric acid thus produced is isolated from the gaseous mixture, and in which a gas with a maximum oxygen content of 99 vol. % is used during said reaction a). In a step d) chlorine is isolated from the gas mixture produced in step c) by the gas permeation of oxygen, carbon dioxide and nitrogen and optionally also of other minor constituents.
    • 本发明涉及一种通过以下方法生产氯的方法:a)使用催化剂和/或通过氯化氢与氧的非热活化反应氯化氢与氧的热反应,其中b)反应过程中产生的气体混合物a ),其至少由目标产物氯和水,未转化的氯化氢和氧气,另外的次要组分如二氧化碳和氮气以及任选的光气组成,冷却以浓缩盐酸,c)由此产生的液体盐酸是 从气体混合物中分离出来,并且其中最大氧含量为99体积% 在所述反应a)期间使用%。 在步骤d)中,通过氧气,二氧化碳和氮气以及任选地还有其他次要组分的气体渗透,从步骤c)中产生的气体混合物中分离出氯气。