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    • 6. 发明公开
    • METHOD FOR PREPARING LITHIUM IRON PHOSPHATE MATERIAL COATED WITH CARBON NANORIBBON
    • 碳纳米管包覆磷酸铁锂材料的方法
    • EP3309125A1
    • 2018-04-18
    • EP17195773.1
    • 2017-10-10
    • Optimum Battery Co., Ltd.
    • YANG, Guo longWANG, Hai tao
    • C01B25/00C01B32/18
    • H01M4/0416C01B25/00C01B32/18C01P2004/84H01M4/0471H01M4/1397H01M4/366H01M4/5825H01M4/587H01M10/0525
    • The present application provides a method for preparing a lithium iron phosphate material coated with carbon nanoribbon, including the steps of: 1) fully and uniformly dispersing carbon nanoribbons in an aqueous solution by means of stirring and ultrasonic dispersion, and obtaining a mixture; 2) adding a lithium source, an iron source and a phosphorous source at a molar ratio of Li: Fe: P = 1:1:1 into the mixture of step 1) under the protection of inert gas, adding water and stirring to form a slurry, and refluxing the slurry; 3) washing and drying the slurry to obtain a primary lithium iron phosphate material coated with carbon nanoribbon; and 4) annealing the primary lithium iron phosphate material coated with carbon nanoribbon of step 3) at high-temperature in a protective atmosphere of argon containing 5-10%v/v of hydrogen, and obtaining the lithium iron phosphate material coated with carbon nanoribbon.
    • 本发明提供了一种碳纳米带包覆磷酸铁锂材料的制备方法,包括以下步骤:1)通过搅拌和超声分散将碳纳米带完全均匀分散于水溶液中,得到混合物; 2)在惰性气体保护下,将锂源,铁源和磷源以Li:Fe:P = 1:1:1的摩尔比加入到步骤1)的混合物中,加入水并搅拌以形成 浆液,并回流浆液; 3)将所述浆料洗涤并干燥,得到涂覆有碳纳米带的磷酸铁锂一次材料; 和4)在含有5-10%v / v氢气的氩气保护气氛中高温退火步骤3)的碳纳米带包覆的磷酸铁锂一次材料,得到碳纳米带包覆的磷酸铁锂材料 。