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1. 发明公开

EP3307020A1 MICROWAVE PROCESSING DEVICE AND PROGRAM 有权
标题翻译：微波加工装置和程序
公开(公告)号：EP3307020A1
公开(公告)日：2018-04-11
申请号：EP17796199.2
申请日：2017-05-10
申请人： Microwave Chemical Co., Ltd.
发明人： TSUKAHARA, Yasunori , TANAKA, Yuya , KURIHARA, Hideshi , KINJYO, Ryuhei , WATANABE, Hisao
IPC分类号： H05B6/80 , B01J19/12 , H05B6/68 , H05B6/72
CPC分类号： B01J19/126 , B01J19/12 , B01J19/18 , B01J2219/00141 , B01J2219/1269 , B01J2219/1275 , B01J2219/1296 , H05B6/68 , H05B6/72 , H05B6/80
摘要： In order to provide a microwave treatment apparatus capable of properly controlling microwave irradiation, a microwave treatment apparatus 1 includes: an irradiating portion 101 that performs microwave irradiation from multiple emitting portions 12; a moving portion 102 that individually moves the multiple emitting portions 12; and a control portion 107 that controls movements of the emitting portions 12 by the moving portion 102, wherein the irradiating portion 101 is such that phases of microwaves that are emitted from the multiple emitting portions 12 are changeable, and the control portion 107 controls phases of microwaves that are emitted by the irradiating portion 101 from the multiple emitting portions 12.
摘要翻译：为了提供能够适当地控制微波照射的微波处理设备，微波处理设备1包括：照射部101，其从多个发射部12进行微波照射; 移动部分102，其单独地移动多个发射部分12; 以及控制部分107，其控制移动部分102的发射部分12的移动，其中照射部分101使得从多个发射部分12发射的微波的相位是可变的，并且控制部分107控制由照射部分101从多个发射部分12发射的微波。

2. 发明公开

EP2196467A1 Process and apparatus for preparing metal or nonmetal phthalocyanine 审中-公开
标题翻译： Verfahren und Apparat zur Herstellung von Metall- bzw Nichtmetallphthalocyanin
公开(公告)号：EP2196467A1
公开(公告)日：2010-06-16
申请号：EP09153910.6
申请日：2004-05-14
申请人： Daehan Solvay Special Chemicals Co., Ltd
发明人： Jung, KiSuck , Kwon, Jong Ho , Park, Seong Soo , Son, Woo Ho
IPC分类号： C07D487/22 , B01J19/10
CPC分类号： C07D487/22 , B01J19/10 , B01J19/126 , B01J2219/00063 , B01J2219/089 , B01J2219/0892 , B01J2219/123 , B01J2219/1275
摘要： Disclosed herein is a process for preparing a metal or nonmetal phthalocyanine by using both microwave and a milling device. Specifically, according to the process, anhydrous phthalic acid, phthalimide, 1,3-diiminoisoindoline, 1,2-dicyanobenzene, an halogen derivative thereof, an alkyl derivative thereof or an alkoxy derivative thereof is mixed with a metal chloride or an alkoxy metal and milled at 130∼250°C for 0.25∼15 hours by using microwave at a frequency of 0.1∼100GHz and a power of 100∼4,000W.
Further disclosed is an apparatus for preparing a metal or nonmetal phthalocyanine.
摘要翻译：本文公开了通过使用微波和研磨装置来制备金属或非金属酞菁的方法。具体地，根据该方法，将无水邻苯二甲酸，邻苯二甲酰亚胺，1,3-二亚氨基异吲哚啉，1,2-二氰基苯，其卤素衍生物，其烷基衍生物或其烷氧基衍生物与金属氯化物或烷氧基金属混合，通过使用频率为0.1¼100GHz的微波和100¼4,000W的功率，在130±250℃下研磨0.25±15小时。进一步公开了一种制备金属或非金属酞菁的装置。

3. 发明公开

EP1515799A1 REACTION AND TEMPERATURE CONTROL FOR HIGH POWER MICROWAVE-ASSISTED CHEMISTRY TECHNIQUES 有权
标题翻译：反应和温度控制的高性能，微波辅助化学过程
公开(公告)号：EP1515799A1
公开(公告)日：2005-03-23
申请号：EP03736565.7
申请日：2003-05-07
申请人： CEM Corporation
发明人： HAYES, Brittany, L. , COLLINS, Michael, J.
IPC分类号： B01J19/12 , H05B6/80
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/0006 , B01J2219/00094 , B01J2219/002 , B01J2219/00213 , B01J2219/0024 , B01J2219/00306 , B01J2219/00495 , B01J2219/00601 , B01J2219/00698 , B01J2219/00716 , B01J2219/1275 , C07B61/00 , C40B60/14
摘要： A method is disclosed for carrying out microwave assisted chemical reactions. The method includes the steps of placing reactants in a microwave-transparent vessel, placing the vessel and its contents into a microwave cavity, applying microwave radiation within the cavity and to the vessel and its contents while concurrently externally cooling the vessel conductively.

4. 发明授权

EP2845645B1 INFORMATION PROCESSING APPARATUS, INFORMATION PROCESSING METHOD, AND PROGRAM 有权转让
公开(公告)号：EP2845645B1
公开(公告)日：2018-09-05
申请号：EP13854874.8
申请日：2013-11-13
申请人： Microwave Chemical Co., Ltd.
发明人： TSUKAHARA, Yasunori , ISHIZUKA, Akinori , DEGUCHI, Yukari
IPC分类号： B01J19/12 , H05B6/68
CPC分类号： H05B6/666 , B01J8/001 , B01J8/0403 , B01J8/0496 , B01J19/0013 , B01J19/126 , B01J19/1862 , B01J2208/00442 , B01J2219/00063 , B01J2219/002 , B01J2219/00202 , B01J2219/00209 , B01J2219/00213 , B01J2219/00238 , B01J2219/0871 , B01J2219/0892 , B01J2219/1218 , B01J2219/1272 , B01J2219/1275 , B01J2219/1296 , G01R21/00 , H05B6/6447 , H05B6/705 , H05B6/80
摘要： Provided is an information processing apparatus that can detect occurrence of an abnormality in a microwave irradiation apparatus, including: a supplied electric power value accepting unit 13 that accepts a supplied electric power value, which is a difference between an electric power value of microwaves incident on a microwave irradiation apparatus 2 and an electric power value of microwaves reflected by the microwave irradiation apparatus 2; a temperature accepting unit 15 that accepts a temperature of a content; an electric energy calculating unit 14 that calculates an electric energy corresponding to a microwave irradiation time, using the supplied electric power value; a temperature change calculating unit 16 that calculates a temperature change corresponding to the microwave irradiation time, using the accepted temperature; a judging unit 20 that, using the electric energy, the temperature change, and a relational expression for associating the electric energy and the temperature change, judges whether or not the relational expression is satisfied within a tolerable range by the electric energy and the temperature change; and an output unit 21 that performs output regarding occurrence of an abnormality, in a case where it is judged that the relational expression is not satisfied within the tolerable range by the electric energy and the temperature change.

5. 发明公开

EP1625131A4 PROCESS AND APPARATUS FOR PREPARING METAL OR NONMETAL PHTHALOCYANINE 有权
标题翻译： VERFAHREN UND APPARAT ZUR HERSTELLUNG VON METALL- BZW. NICHTMETALLPHTHALOCYANIN
公开(公告)号：EP1625131A4
公开(公告)日：2006-12-20
申请号：EP04733202
申请日：2004-05-14
申请人： PHTHALOS CO LTD
发明人： KWON JONG HO , JUNG KI SUCK , SON WOO HO , PARK SEONG SOO
IPC分类号： C07D487/22 , B01J19/10 , B01J19/12
CPC分类号： C07D487/22 , B01J19/10 , B01J19/126 , B01J2219/00063 , B01J2219/089 , B01J2219/0892 , B01J2219/123 , B01J2219/1275
摘要： Disclosed herein is a process for preparing a metal or nonmetal phthalocyanine by using both microwave and ultrasonic wave energy in the presence of a solvent, or by using microwave energy in the absence of a solvent. Specifically, according to the process, anhydrous phthalic acid, phthalimide, 1,3-diiminoisoindoline, 1,2-dicyanobenzene, an halogen derivative thereof, an alkyl_ derivative thereof or an alkoxy derivative thereof is mixed with a metal chloride or an alkoxy metal at 130250°C for 0.2515 hours by using microwave at a frequency of 0.1-1000Hz and a power of 100-3,000W and ultrasonic wave at a frequency of 1-1,000GHz and a power of 100-5,000W in the presence of a solvent, or by using microwave at a frequency of 0.1-100GHz and a power of 100-4,000W in the absence of a solvent. Further disclosed is an apparatus for preparing a metal or nonmetal phthalocyanine in the absence or presence of solvent.
摘要翻译：本发明公开了一种通过在溶剂存在下使用微波和超声波能量，或者通过在不存在溶剂的情况下使用微波能量来制备金属或非金属酞菁的方法。具体而言，根据该方法，可以使用无水邻苯二甲酸，邻苯二甲酰亚胺，1,3-二亚氨基异吲哚满，1,2-二氰基苯，其卤素衍生物，衍生物或其烷氧基衍生物与金属氯化物或烷氧基金属在1302〜150℃下混合0.25〜15小时，使用频率为0.1〜1000Hz，功率为100〜3,000W的微波和频率为1的超声波 -1,000GHz，功率为100-5,000W，或者在溶剂不存在的情况下，使用频率为0.1-100GHz，功率为100-4,000W的微波。还公开了在溶剂不存在或存在下制备金属或非金属酞菁的设备。

6. 发明授权

EP1356710B1 MICROWAVE-ASSISTED CHEMICAL SYNTHESIS INSTRUMENT WITH FIXED TUNING 有权
标题翻译：带有计数器VOTE装仪的微波辅助化学合成
公开(公告)号：EP1356710B1
公开(公告)日：2004-09-22
申请号：EP02705941.9
申请日：2002-01-24
申请人： CEM Corporation
发明人： JENNINGS, William, Edward
IPC分类号： H05B6/70 , H05B6/64 , H05B6/74 , H05B6/80
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/00058 , B01J2219/00063 , B01J2219/00065 , B01J2219/00094 , B01J2219/002 , B01J2219/0024 , B01J2219/1209 , B01J2219/1233 , B01J2219/1269 , B01J2219/1275 , H01P7/06
摘要： An instrument is disclosed fro microwave-assisted chemical processes that avoids tuning discrepancies that otherwise result based upon the materials being heated. The instrument includes a source of microwave radiation, a waveguide in communication with the source, with at least a portion of the waveguide forming a cylindrical arc, a cylindrical cavity inmediately surrounded by the cylindrical arc portions of the waveguide, and at least three slotted openings in the circumference of the circular waveguide that provide microwave communication between the waveguide and the cavity.

7. 发明公开

EP1356710A2 MICROWAVE-ASSISTED CHEMICAL SYNTHESIS INSTRUMENT WITH FIXED TUNING 有权
标题翻译：带有计数器VOTE装仪的微波辅助化学合成
公开(公告)号：EP1356710A2
公开(公告)日：2003-10-29
申请号：EP02705941.9
申请日：2002-01-24
申请人： CEM Corporation
发明人： JENNINGS, William, Edward
IPC分类号： H05B6/70 , H05B6/64 , H05B6/74 , H05B6/80
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/00058 , B01J2219/00063 , B01J2219/00065 , B01J2219/00094 , B01J2219/002 , B01J2219/0024 , B01J2219/1209 , B01J2219/1233 , B01J2219/1269 , B01J2219/1275 , H01P7/06
摘要： An instrument is disclosed fro microwave-assisted chemical processes that avoids tuning discrepancies that otherwise result based upon the materials being heated. The instrument includes a source of microwave radiation, a waveguide in communication with the source, with at least a portion of the waveguide forming a cylindrical arc, a cylindrical cavity inmediately surrounded by the cylindrical arc portions of the waveguide, and at least three slotted openings in the circumference of the circular waveguide that provide microwave communication between the waveguide and the cavity.

8. 发明公开

EP1257356A1 MICROWAVE HEATING APPARATUS 有权
标题翻译：微波加热
公开(公告)号：EP1257356A1
公开(公告)日：2002-11-20
申请号：EP01906044.1
申请日：2001-02-26
申请人： Personal Chemistry i Uppsala AB
发明人： FAGRELL, Magnus , RISMAN, Per, Olov, G.
IPC分类号： B01J19/12 , H05B6/70
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/1248 , B01J2219/1266 , B01J2219/1269 , B01J2219/1272 , B01J2219/1275 , H05B6/701 , H05B6/705
摘要： The present invention relates to an apparatus for heating a sample, such as chemical reaction mixtures, whose dielectric properties varies during the heating process. In particular, the present invention relates to a microwave heating apparatus comprising a microwave generator, a waveguide for guiding the generated microwaves to an applicator, and a deflector formed by a closed loop defining a plane, said deflector having an inherent resonance frequency and a thickness in a direction normal to said plane, the deflector being rotatable around an axis being at least substantially parallel to said plane, the deflector being positioned in the waveguide so as to form a resonant cavity with the sample and the waveguide applicator. The resonance conditions of the resonant cavity and the coupling factor of radiation from the waveguide to the cavity are easily adjustable by rotation of the deflector. The resonance conditions and the coupling factor can be adjusted in response to the dielectric properties of the sample in order to optimise the amount of absorbed power and thereby obtain control of the sample heating process.

9. 发明公开

EP2845645A1 INFORMATION PROCESSING DEVICE, INFORMATION PROCESSING METHOD, AND PROGRAM 有权转让
标题翻译：信息管理系统，信息管理
公开(公告)号：EP2845645A1
公开(公告)日：2015-03-11
申请号：EP13854874.8
申请日：2013-11-13
申请人： Microwave Chemical Co., Ltd. , Osaka University
发明人： TSUKAHARA, Yasunori , ISHIZUKA, Akinori , DEGUCHI, Yukari
IPC分类号： B01J19/12 , H05B6/68
CPC分类号： H05B6/666 , B01J8/001 , B01J8/0403 , B01J8/0496 , B01J19/0013 , B01J19/126 , B01J19/1862 , B01J2208/00442 , B01J2219/00063 , B01J2219/002 , B01J2219/00202 , B01J2219/00209 , B01J2219/00213 , B01J2219/00238 , B01J2219/0871 , B01J2219/0892 , B01J2219/1218 , B01J2219/1272 , B01J2219/1275 , B01J2219/1296 , G01R21/00 , H05B6/6447 , H05B6/705 , H05B6/80
摘要： Provided is an information processing apparatus that can detect occurrence of an abnormality in a microwave irradiation apparatus, including: a supplied electric power value accepting unit 13 that accepts a supplied electric power value, which is a difference between an electric power value of microwaves incident on a microwave irradiation apparatus 2 and an electric power value of microwaves reflected by the microwave irradiation apparatus 2; a temperature accepting unit 15 that accepts a temperature of a content; an electric energy calculating unit 14 that calculates an electric energy corresponding to a microwave irradiation time, using the supplied electric power value; a temperature change calculating unit 16 that calculates a temperature change corresponding to the microwave irradiation time, using the accepted temperature; a judging unit 20 that, using the electric energy, the temperature change, and a relational expression for associating the electric energy and the temperature change, judges whether or not the relational expression is satisfied within a tolerable range by the electric energy and the temperature change; and an output unit 21 that performs output regarding occurrence of an abnormality, in a case where it is judged that the relational expression is not satisfied within the tolerable range by the electric energy and the temperature change.
摘要翻译：提供了一种能够检测微波照射装置中的异常发生的信息处理装置，包括：供给电力值接受单元13，其接受作为入射的微波的电功率值之间的差的供给电力值微波照射装置2和由微波照射装置2反射的微波的电功率值; 接受内容的温度的温度接受单元15; 使用所提供的电力值计算与微波照射时间相对应的电能的电能计算单元14; 使用所接受的温度来计算与微波照射时间对应的温度变化的温度变化计算部16; 使用电能，温度变化和关联电能与温度变化的关系表达式的判断单元20，通过电能和温度变化来判断关系表达式是否在容许范围内得到满足 ; 以及在通过电能和温度变化判断在容许范围内不满足关系表达式的情况下，执行关于异常发生的输出的输出单元21。

10. 发明公开

EP2777809A1 CHEMICAL REACTION DEVICE 有权转让
标题翻译：化学工业股份有限公司
公开(公告)号：EP2777809A1
公开(公告)日：2014-09-17
申请号：EP12848355.9
申请日：2012-11-09
申请人： Microwave Chemical Co., Ltd. , Osaka University
发明人： ISHIZUKA, Akinori , YOSHINO, Iwao , MOMOTA, Kunitaka , TSUKAHARA, Yasunori
IPC分类号： B01J19/12 , C07C67/03 , C07C67/08 , C07C69/22 , H05B6/80 , C07B61/00
CPC分类号： B01J19/126 , B01J8/20 , B01J8/36 , B01J19/18 , B01J19/1862 , B01J2208/00442 , B01J2208/00867 , B01J2219/00141 , B01J2219/0877 , B01J2219/0892 , B01J2219/1218 , B01J2219/1224 , B01J2219/1227 , B01J2219/1245 , B01J2219/1266 , B01J2219/1269 , B01J2219/1275 , B01J2219/1293 , B01J2219/1296 , B01J2219/182 , B01J2219/187 , C07C67/03 , C07C67/08 , H05B6/78 , H05B6/806 , C07C69/52
摘要： Provided is a chemical reaction apparatus capable of efficiently irradiating a content with microwaves even in a case where the amount of the content changes, including: a horizontal flow-type reactor 13 inside of which has been partitioned into multiple chambers by a partition plate, and a liquid content horizontally flows with an unfilled space being provided thereabove; a microwave generator 14 that generates microwaves; and at least one waveguide 15 that transmits the microwaves generated by the microwave generator 14 to the unfilled space in the reactor 13; wherein the reactor 13 has a shape in which an area of a liquid surface does not change even in a case where a height of the liquid surface changes according to a change in an amount of the content.
摘要翻译：本发明提供一种化学反应装置，即使在含量变化的情况下也能够高效地照射微波的内容物，其包括：其内部被分隔板分隔成多个室的水平流型反应器13，以及液体内容物水平地流动，在其上方设有未填充的空间; 产生微波的微波发生器14; 以及将由微波发生器14产生的微波传输到反应器13中未填充空间的至少一个波导15; 其中反应器13具有这样的形状，即使在液面的高度根据内容物的量的变化而变化的情况下，液面的面积也不变化。

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