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1. 发明公开

EP3102558A2 METHOD FOR PRODUCING CARBONATES 有权转让
标题翻译：生产碳酸盐的方法
公开(公告)号：EP3102558A2
公开(公告)日：2016-12-14
申请号：EP15704440.5
申请日：2015-02-04
申请人： SABIC Global Technologies B.V.
发明人： GAUTAM, Pankaj Singh , HOLLAR JR., William E. , FERRER NADAL, Sergio , ANDERSON, John Joseph
IPC分类号： C07C68/02 , C07C68/06 , C07C69/96
CPC分类号： C07C68/02 , B01J8/0285 , B01J8/0438 , B01J8/0442 , B01J8/067 , B01J19/245 , B01J2208/00185 , B01J2208/00194 , B01J2208/00221 , B01J2208/00238 , B01J2208/00513 , B01J2208/02 , B01J2208/065 , B01J2219/00015 , B01J2219/192 , B01J2219/1923 , B01J2219/194 , B01J2219/1943 , B01J2219/1944 , B01J2219/1946 , B01J2219/1947 , C01B32/80 , F28F1/025 , F28F1/08 , F28F1/10 , F28F1/16 , F28F1/24 , F28F1/34 , F28F1/38 , F28F1/40 , F28F1/426 , F28F13/08 , F28F2210/02 , C07C69/96
摘要： In an embodiment, a method of producing a carbonate comprises reacting carbon monoxide and chlorine in a phosgene reactor in the presence of a catalyst to produce a first product comprising phosgene; wherein carbon tetrachloride is present in the first product in an amount of 0 to 10 ppm by volume based on the total volume of phosgene; and reacting a monohydroxy compound with the phosgene to produce the carbonate; wherein the phosgene reactor comprises a tube, a shell, and a space located between the tube and the shell; wherein the tube comprises one or more of a mini-tube section and a second tube section; a first concentric tube concentrically located in the shell; a twisted tube; an internal scaffold; and an external scaffold.
摘要翻译：在一个实施方案中，生产碳酸盐的方法包括在催化剂存在下在光气反应器中使一氧化碳和氯气反应以产生包含光气的第一产物; 其中基于光气的总体积，四氯化碳以0至10体积ppm的量存在于第一产物中; 并使单羟基化合物与光气反应生成碳酸酯; 其中光气反应器包括管，壳和位于管和壳之间的空间; 其中所述管包括微型管部分和第二管部分中的一个或多个; 同心地位于壳体中的第一同心管; 扭曲的管子; 内部脚手架; 和一个外部脚手架。

2. 发明公开

EP1572582A1 VERFAHREN ZUR HERSTELLUNG VON CHLOR DURCH GASPHASENOXIDATION VON CHLORWASSERSTOFF 有权
公开(公告)号：EP1572582A1
公开(公告)日：2005-09-14
申请号：EP03789224.7
申请日：2003-12-11
申请人： BASF Aktiengesellschaft
发明人： OLBERT, Gerhard , WALSDORFF, Christian , HARTH, Klaus , STRÖFER, Eckhard , FIENE, Martin
IPC分类号： C01B7/04 , B01J8/06
CPC分类号： C01B7/04 , B01J8/008 , B01J8/067 , B01J19/0073 , B01J2208/00212 , B01J2208/00221 , B01J2208/0023 , B01J2208/00238 , B01J2208/00849 , B01J2219/0004 , Y02P20/149
摘要： Disclosed is a method for producing chlorine by means of gas phase oxidation of hydrogen chloride with a gas flow containing molecular oxygen in the presence of a fixed-bed catalyst. Said method is carried out in a reactor (1) comprising a nest of contact tubes (2) that are disposed parallel to each other in the longitudinal direction of the reactor and are fastened within tube bottoms (3) at the ends thereof, a hood (4) that is arranged at both ends of the reactor (1), and one or several deflecting metal sheets (6) which are disposed perpendicular to the longitudinal direction of the reactor in the intermediate space (5) between the contact tubes (2) and alternately release opposite passages (7) located on the inner wall of the reactor (1). The contact tubes (2) are filled with the fixed-bed catalyst, the hydrogen chloride and the gas flow containing molecular oxygen are directed from one end of the reactor through the contact tubes (2) via a hood (4) and are withdrawn from the opposite end of the reactor via the second hood (4), and a liquid heat-exchanging substance is directed through the intermediate space (5) around the contact tubes (2).
摘要翻译：本发明公开了一种在固定床催化剂存在下通过含有分子氧的气流气相氧化氯化氢来生产氯的方法。所述方法在反应器（1）中进行，所述反应器包括在反应器的纵向方向上彼此平行布置并且在管端部（3）的端部处固定在管底部（3）内的接触管（2）（1）的两端设置的一个或多个偏转金属板（6），以及一个或多个偏转金属板（6），所述偏转金属板垂直于反应器的纵向设置在接触管（2）之间的中间空间（5））并且交替地释放位于反应器（1）的内壁上的相对通道（7）。接触管（2）填充有固定床催化剂，氯化氢和含有分子氧的气流从反应器的一端经由罩（4）引导通过接触管（2），并从通过第二罩（4）的反应器的相对端和液体热交换物质被引导通过围绕接触管（2）的中间空间（5）。

3. 发明授权

EP2539420B1 PROCESS FOR PRODUCING SYNTHETIC LIQUID HYDROCARBONS AND REACTOR FOR FISCHER-TROPSCH SYNTHESIS 有权
标题翻译：生产合成液体烃的方法和用于费歇尔合成法的反应器
公开(公告)号：EP2539420B1
公开(公告)日：2017-09-06
申请号：EP11718526.4
申请日：2011-01-31
申请人： INFRA XTL TECHNOLOGY LIMITED
发明人： ERMOLAEV, Vadim Sergeevich , MORDKOVICH, Vladimir Zalmanovich , SOLOMONIK, Igor Grigorievich , DEREVICH, Igor Vladimirovich , SINEVA, Lilia Vadimovna , MITBERG, Eduard Borisovich
IPC分类号： C10G2/00 , C07C1/04 , B01J8/06 , B01J8/02
CPC分类号： B01J8/067 , B01J2208/00238 , B01J2219/1946 , C10G2/332 , C10G2/341 , C10G2300/1022 , C10G2300/4012

4. 发明公开

EP2539420A2 PROCESS FOR PRODUCING SYNTHETIC LIQUID HYDROCARBONS AND REACTOR FOR FISCHER-TROPSCH SYNTHESIS 有权
标题翻译：处理综合液态烃物质，核能等费托工艺的制备
公开(公告)号：EP2539420A2
公开(公告)日：2013-01-02
申请号：EP11718526.4
申请日：2011-01-31
申请人： Infra Technologies Ltd.
发明人： ERMOLAEV, Vadim Sergeevich , MORDKOVICH, Vladimir Zalmanovich , SOLOMONIK, Igor Grigorievich , DEREVICH, Igor Vladimirovich , SINEVA, Lilia Vadimovna , MITBERG, Eduard Borisovich
IPC分类号： C10G2/00 , B01J8/02
CPC分类号： B01J8/067 , B01J2208/00238 , B01J2219/1946 , C10G2/332 , C10G2/341 , C10G2300/1022 , C10G2300/4012
摘要： The present invention relates to petrochemistry, gas chemistry, coal chemistry, particularly to a synthesis of hydrocarbons C
5 and higher from CO and H
2 under the Fischer- Tropsch reaction; the invention relates to a process and a system for producing synthetic liquid hydrocarbons. A process for producing synthetic liquid hydrocarbons is provided by catalytic converting syngas under the Fischer-Tropsch reaction on a fixed catalyst bed in a vertical shell and tube reactor with coolant supply into shell wherein as soon as the syngas conversion degree achieves 60-80%, a pressure gradient along the tubes is reduced below 0.1 bar/m and this value is maintained during the whole process. A reactor for Fischer-Tropsch synthesis is provided comprising tubes with catalyst in a shell, the ratio of the tube diameter at the tube outlet to the diameter at the inlet is from 1.5/1 to 2.5/1. The invention gives a possibility to achieve the optimum temperature range in the catalyst bed; it improves heat and mass-transfer and shut out an accumulation of the liquid products in the bottom of the tubes.
摘要翻译：本发明涉及石油化学，气体化学物质，煤化学，特别是涉及烃C5的来自费 - 托反应在CO和H 2的合成和更高; 本发明涉及一种方法，以及用于生产合成液体烃的系统。一种用于生产合成液体烃的方法是通过费 - 托反应的催化下合成气转化中的垂直管壳式反应器与冷却剂供应到壳worin只要合成气转化度达到60-80％设置在固定催化剂床沿管的压力梯度减小到低于0.1巴/米，该值是在整个过程中保持。一种用于费 - 托合成反应器中的壳提供了一种包括管与催化剂，该管直径的在出口管的直径在入口的比例为1.5 / 1至2.5 /第一本发明提供了一种可能性，以实现在催化剂床中的最佳温度范围; 它改善了热和质量传递和拒之门外液体产品在管的底部积累。

5. 发明公开

EP3271062A1 BOILING WATER REACTOR 有权
标题翻译：沸水反应堆
公开(公告)号：EP3271062A1
公开(公告)日：2018-01-24
申请号：EP16710464.5
申请日：2016-03-18
申请人： Haldor Topsøe A/S
发明人： WIX, Christian , BOE, Michael
IPC分类号： B01J8/06
CPC分类号： B01J8/065 , B01J8/067 , B01J2208/00017 , B01J2208/00238
摘要： The invention relates to a boiling water reactor for an exothermal reaction. The reactor comprises reactant by-pass inserts arranged on top of the upper tube sheet to provide for a catalyst layer on top of the upper tube sheet and also a cooling stream of reactant by-passing the upper layer of catalyst and cooling the upper tube sheet from the temperature rise due to the exothermal reaction taking place in the upper layer of catalyst.

6. 发明公开

EP2917673A4 A FIXED BED REACTOR HEAT TRANSFER STRUCTURE 有权
标题翻译：传热装置用于硬床反应器
公开(公告)号：EP2917673A4
公开(公告)日：2016-08-17
申请号：EP13852712
申请日：2013-11-12
申请人： CERAMATEC INC
发明人： HARTVIGSEN JOSEPH J
IPC分类号： F28F1/10
CPC分类号： F28F7/00 , B01J8/067 , B01J2208/00115 , B01J2208/0015 , B01J2208/00168 , B01J2208/00212 , B01J2208/00238 , B01J2208/00513 , B01J2208/065 , B01J2219/30223 , B01J2219/30242 , B01J2219/30408 , B01J2219/30416 , F28D2021/0022 , F28F1/40
摘要： An apparatus includes a heat transfer structure configured to be disposed at least partially within an enclosure of a fixed bed reactor and operable to transfer heat from a heat source to a heat sink. The heat transfer structure includes a plurality of fins each fin including a first end and a second end, the first end contacting an inner surface of the enclosure of the fixed bed reactor, the second end at least partially enclosed within the enclosure of the fixed bed reactor. A path of at least one of the plurality of fins comprises the shortest possible length between the first end of the at least one of the plurality of fins and the second end of the at least one of the plurality of fins.

7. 发明公开

EP2917673A1 A FIXED BED REACTOR HEAT TRANSFER STRUCTURE 有权
标题翻译：传热装置用于硬床反应器
公开(公告)号：EP2917673A1
公开(公告)日：2015-09-16
申请号：EP13852712.2
申请日：2013-11-12
申请人： Ceramatec, Inc
发明人： HARTVIGSEN, Joseph J.
IPC分类号： F28F1/10
CPC分类号： F28F7/00 , B01J8/067 , B01J2208/00115 , B01J2208/0015 , B01J2208/00168 , B01J2208/00212 , B01J2208/00238 , B01J2208/00513 , B01J2208/065 , B01J2219/30223 , B01J2219/30242 , B01J2219/30408 , B01J2219/30416 , F28D2021/0022 , F28F1/40
摘要： An apparatus includes a heat transfer structure configured to be disposed at least partially within an enclosure of a fixed bed reactor and operable to transfer heat from a heat source to a heat sink. The heat transfer structure includes a plurality of fins each fin including a first end and a second end, the first end contacting an inner surface of the enclosure of the fixed bed reactor, the second end at least partially enclosed within the enclosure of the fixed bed reactor. A path of at least one of the plurality of fins comprises the shortest possible length between the first end of the at least one of the plurality of fins and the second end of the at least one of the plurality of fins.

8. 发明授权

EP1572582B1 VERFAHREN ZUR HERSTELLUNG VON CHLOR DURCH GASPHASENOXIDATION VON CHLORWASSERSTOFF 有权
公开(公告)号：EP1572582B1
公开(公告)日：2006-07-19
申请号：EP03789224.7
申请日：2003-12-11
申请人： BASF Aktiengesellschaft
发明人： OLBERT, Gerhard , WALSDORFF, Christian , HARTH, Klaus , STRÖFER, Eckhard , FIENE, Martin
IPC分类号： C01B7/04 , B01J8/06
CPC分类号： C01B7/04 , B01J8/008 , B01J8/067 , B01J19/0073 , B01J2208/00212 , B01J2208/00221 , B01J2208/0023 , B01J2208/00238 , B01J2208/00849 , B01J2219/0004 , Y02P20/149
摘要： Disclosed is a method for producing chlorine by means of gas phase oxidation of hydrogen chloride with a gas flow containing molecular oxygen in the presence of a fixed-bed catalyst. Said method is carried out in a reactor (1) comprising a nest of contact tubes (2) that are disposed parallel to each other in the longitudinal direction of the reactor and are fastened within tube bottoms (3) at the ends thereof, a hood (4) that is arranged at both ends of the reactor (1), and one or several deflecting metal sheets (6) which are disposed perpendicular to the longitudinal direction of the reactor in the intermediate space (5) between the contact tubes (2) and alternately release opposite passages (7) located on the inner wall of the reactor (1). The contact tubes (2) are filled with the fixed-bed catalyst, the hydrogen chloride and the gas flow containing molecular oxygen are directed from one end of the reactor through the contact tubes (2) via a hood (4) and are withdrawn from the opposite end of the reactor via the second hood (4), and a liquid heat-exchanging substance is directed through the intermediate space (5) around the contact tubes (2).

9. 发明公开

EP1621247A1 Durchführung von exothermen Gasphasenreaktionen 审中-公开
标题翻译： D ung。。。。。。。。
公开(公告)号：EP1621247A1
公开(公告)日：2006-02-01
申请号：EP05013934.4
申请日：2005-06-28
申请人： MAN DWE GmbH
发明人： Dachs, Josef, Dr. , Schuster, Wolfgang, Dr. , Bank, Rolf, Dr. , Lehr, Manfred
IPC分类号： B01J8/06 , B01J19/00
CPC分类号： F28F1/40 , B01J8/06 , B01J8/067 , B01J19/002 , B01J2208/00238 , B01J2208/0084 , B01J2208/00849 , B01J2219/00263
摘要： Bei einem Verfahren zum Betreiben eines Rohrbündelreaktors für exotherme Gasphasenreaktionen, der ein Rohrbündel mit katalysatorgefüllten Reaktionsrohren (2) aufweist, deren eine Enden von einer Gaseintrittshaube und deren andere Enden von einer Gasaustrittshaube überspannt und die zur Abführung der Reaktionswärme an der Außenseite von einem Wärmeträger umströmt werden, wobei ein explosionsfähiges Gasgemisch (G) über die Gaseintrittshaube in die Reaktionsrohre (2) eingeleitet und nach der Reaktion das gegebenenfalls immer noch explosionsfähige Gasgemisch (G) über die Gasaustrittshaube aus diesen abgeleitet wird, wird eine Grenztemperatur in den Reaktionsrohren (2) vorgegeben, die über den normalen Betriebstemperaturen der Reaktionsrohre (2) liegt, aber höchstens gleich der Entzündungstemperatur des explosionsfähigen Gasgemisches (G) ist und ein in Reaktionsrohren (2) sich jeweils ausbildender nicht betriebsmäßiger Hochtemperaturbereich (7), dessen Temperatur mindestens gleich der Grenztemperatur ist und der in dem jeweiligen Reaktionsrohr (2) in dessen Längsrichtung wandert, noch im Reaktionsrohr (2) gestoppt, so daß ein Durchschlagen des Hochtemperaturbereichs (7) in die Gaseintritts- bzw. die Gasaustrittshaube verhindert wird. Ferner werden noch Vorrichtungen, Reaktionsrohre und Rohrbündelreaktoren zur Durchführung des Verfahrens vorgeschlagen.
摘要翻译：一种用于操作用于放热气相反应的管束反应器的方法，其中将爆炸性气体混合物进料到管中和（可能仍然是爆炸性的）气体混合物排出，包括：（i）在管中提供极限温度（LT），高于正常条件下管道热区的最高温度，但不高于爆炸性气体混合物的着火温度; 和（ii）在管内停止非操作热区（7），其最大温度至少等于LT并且沿着管纵向迁移，使得这些热区渗入入口或出口罩被禁止。一种用于放出气相反应的管束反应器的方法，由一束催化剂填充的反应管（每个具有热区）组成，一端具有气体罩，另一端为气体出口罩，另一端为热载体在外部流动以抽出反应热，其中爆炸性气体混合物通过入口罩进入管中，并且（可能仍然是爆炸性的）气体混合物通过出口罩排出，包括：（1）提供极限温度 LT）在正常条件下，高于爆炸性气体混合物（G）的点火温度以上的热管道（2）内的最高温度; 和（2）在管内阻止非操作热区（7），其最大温度至少等于LT并且沿管纵向移动，使得这种热区渗入入口或出口罩被禁止。独立权利要求包括：（A）用于并入如上操作的反应器中的装置（1，300），其尺寸适于装配在反应管（2）中并形成用于获得预定LT的通流截面 ; （B）包括上述装置的用于放热气相反应的管束反应器的反应管; 和（C）用于放热气相反应的管束反应器，包括如上所述的反应管。

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