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    • 3. 发明公开
    • Method for fabricating and inspecting coatings
    • Verfahren zur Herstellung undÜberwachungvon Beschichtungen
    • EP1014079A2
    • 2000-06-28
    • EP99310020.5
    • 1999-12-13
    • United Technologies Corporation
    • Jaworowski, MarkWeston, Charles H.Janowsky, Glenn T.
    • G01N27/02
    • G01B7/105G01N27/025
    • A method of fabrication and inspection includes depositing a coating (20) and determining at least one physical property of the coating (20) using eddy current techniques. In a detailed embodiment an abradable coating (20) having a metal volume fraction in the range of from 0.3 to 0.5 is applied to an inner circumference of a stator (30) for a gas turbine engine compressor. An eddy current probe (56) is positioned by a manipulator (54). A distance separating the probe (56) and a surface (32) of the coating (20) is measured using a frequency above one megahertz (MHz). The thickness of the coating (20) is measured by determining the rolloff frequency for the coating's complex impedance. The coating density is determined by its complex impedance at a characteristic frequency below four MHz. The density can be used as an indication of the performance of the coating (20) with respect to abradability and the erosion resistance. The measurements may also be applied as a post-process quality control technique.
    • 制造和检查的方法包括使用涡流技术沉积涂层(20)并确定涂层(20)的至少一种物理性质。 在一个详细的实施例中,将金属体积分数在0.3至0.5范围内的可磨损涂层(20)施加到用于燃气涡轮发动机压缩机的定子(30)的内​​周。 涡流探针(56)由操纵器(54)定位。 使用高于1兆赫兹(MHz)的频率来测量分离探针(56)和涂层(20)的表面(32)的距离。 涂层(20)的厚度通过确定涂层复阻抗的滚降频率来测量。 涂层密度由其在低于4MHz的特征频率下的复阻抗来确定。 可以将密度用作涂层(20)相对于耐磨性和耐侵蚀性的性能的指示。 测量也可以作为后处理质量控制技术应用。
    • 8. 发明公开
    • Corrosion resistant, chromate-free conversion coating for magnesium alloys
    • Korrosionsbeständige,chromat-freie KonversionsbeschichtungfürMagnesium-Legierungen
    • EP1338678A2
    • 2003-08-27
    • EP03250845.9
    • 2003-02-11
    • UNITED TECHNOLOGIES CORPORATION
    • Jaworowski, MarkKryzman, Michael A.Tang, XaiBriles, Owen M.
    • C23C22/22C23C22/36
    • C23C22/78C23C22/36C23C22/44
    • The present invention relates to a process for forming a chromate-free, corrosion resistant coating on a product formed from magnesium or a magnesium alloy and to a solution used for forming the coating. The solution has phosphate and fluoride ions and contains from 1.0 g/l to 5.0 g/l of an active corrosion inhibitor selected from the group consisting potassium permanganate, sodium tungstate, sodium vanadate, and mixtures thereof. The solution may also contain from 0.1 to 1.0 vol% of a surfactant which reduces reaction time. The solution is maintained at a temperature of 120 to 200°F (49 to 93°C) and has a pH of 5 to 7. The process for forming the coating broadly comprises degreasing the magnesium or magnesium alloy product in a degreasing solution, cleaning the product in a highly alkaline cleaning solution, deoxidizing the product in a deoxidizing solution, and immersing the product in the coating solution for a time period of 15 minutes to 90 minutes.
    • 本发明涉及在由镁或镁合金形成的产品和用于形成涂层的溶液中形成无铬酸盐的耐腐蚀涂层的方法。 该溶液具有磷酸盐和氟离子,并且含有1.0g / l至5.0g / l的选自高锰酸钾,钨酸钠,钒酸钠及其混合物的活性腐蚀抑制剂。 该溶液还可含有0.1至1.0体积%的表面活性剂,其减少反应时间。 将溶液保持在120至200°F(49至93℃)的温度下并具有5至7的pH。形成涂层的方法广泛地包括在脱脂溶液中除去镁或镁合金产品,清洗 该产品在高碱性清洗溶液中,将脱氧溶液中的产物脱氧,并将产物浸入涂布溶液中15分钟至90分钟。