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1. 发明公开

EP3228386A1 COMPOSITE BODY, METHOD FOR PRODUCING COMPOSITE BODY, AMMONIA SYNTHESIS CATALYST, AND AMMONIA SYNTHESIS METHOD 有权
标题翻译：复合体，复合体生产方法，氨合成催化剂和氨合成方法
公开(公告)号：EP3228386A1
公开(公告)日：2017-10-11
申请号：EP15864436.9
申请日：2015-12-04
申请人： Japan Science and Technology Agency , Tokyo Institute of Technology
发明人： HOSONO Hideo , HARA Michikazu , KITANO Masaaki , YOKOYAMA Toshiharu , INOUE Yasunori
IPC分类号： B01J27/24 , C01B21/092 , C01C1/04
CPC分类号： C01C1/0411 , B01J21/18 , B01J23/462 , B01J23/58 , B01J23/63 , B01J23/648 , B01J27/24 , B01J35/0046 , B01J35/006 , B01J35/0066 , B01J35/1014 , B01J35/1019 , B01J37/0072 , B01J37/0205 , B01J37/0209 , B01J37/04 , B01J37/08 , B01J37/082 , B01J37/086 , C01B3/047 , C01B21/0923 , C01B21/0926 , C01P2004/04 , Y02E60/364 , Y02P20/52
摘要： An ammonia synthesis catalyst having high activity is obtained by having a two-dimensional electride compound having a lamellar crystal structure such as Ca 2 N support a transition metal. However, since the two-dimensional electride compound is unstable, the stability of the catalyst is low. In addition, in cases where a two-dimensional electride compound is used as a catalyst support, it is difficult to shape the catalyst depending on reactions since the two-dimensional electride compound has poor processability. A composite which includes a transition metal, a support and a metal amide compound, wherein the support is a metal oxide or a carbonaceous support; and the metal amide compound is a metal amide compound represented by general formula (1). M(NH 2 ) x ···(1) (In general formula (1), M represents at least one metal atom selected from the group consisting of Li, Na, K, Be, Mg, Ca, Sr, Ba and Eu; and x represents the valence of M.)
摘要翻译：具有高活性的氨合成催化剂是通过使具有层状晶体结构的二维电子化合物如Ca2N负载过渡金属而获得的。但是，由于二维电子化合物不稳定，所以催化剂的稳定性低。另外，在使用二维电子化合物作为催化剂载体的情况下，由于二维电子化合物的加工性差，因此难以根据反应对催化剂进行成形。一种包含过渡金属，载体和金属氨化合物的复合物，其中所述载体是金属氧化物或碳质载体; 该金属氨化合物是通式（1）所示的金属氨化合物。通式（1）中，M表示选自由Li，Na，K，Be，Mg，Ca，Sr，Ba和Eu组成的组中的至少一种金属原子; 并且x表示M的化合价）

2. 发明授权

EP3115339B1 MAYENITE-TYPE COMPOUND CONTAINING IMIDE ANION, AND METHOD FOR PRODUCING SAME 有权
公开(公告)号：EP3115339B1
公开(公告)日：2018-10-17
申请号：EP15758625.6
申请日：2015-02-12
申请人： Japan Science and Technology Agency , Tokyo Institute of Technology
发明人： HOSONO Hideo , HAYASHI Fumitaka , YOKOYAMA Toshiharu , KITANO Masaaki
IPC分类号： C01F7/16 , B01J20/04 , B01J20/08 , C01C1/00
CPC分类号： B01J20/041 , B01J20/08 , C01C1/006 , C01F7/164 , C01F7/166 , C01P2002/82 , C01P2002/86 , C01P2006/40
摘要： The invention related to a material that can stably hold an imide anion (NH 2 - ) therein even in the atmosphere or in a solvent, and a method for synthesizing the material and a use of the material. A mayenite-type compound into which imide anions are incorporated at a concentration of 1 × 10 18 cm -3 or more are provided. The mayenite-type compound can be produced by heating a mayenite-type compound including electrons or free oxygen ions in a cage thereof, in liquefied ammonia at 450 to 700°C and at a pressure of 30 to 100 MPa. The compound has properties such that active imide anions can be easily incorporated into the compound and the active imide anions can be easily released in the form of ammonia from the compound, and the compound has chemical stability.

3. 发明公开

EP2730542A1 PEROVSKITE OXIDE CONTAINING HYDRIDE ION, AND METHOD FOR MANUFACTURING SAME 有权转让
标题翻译： VERFAHREN ZU SEINER HERSTELLUNG的HYDRID-IONEN ENTHALTENDES PEROWSKITOXID
公开(公告)号：EP2730542A1
公开(公告)日：2014-05-14
申请号：EP12811931.0
申请日：2012-07-05
申请人： Tokyo Institute of Technology , Kyoto University
发明人： HOSONO Hideo , KAGEYAMA Hiroshi , KOBAYASHI Yoji , TAKANO Mikio , YAJIMA Takeshi
IPC分类号： C01G23/00
CPC分类号： B01J39/02 , B01J23/002 , B01J23/02 , C01B3/001 , C01B3/503 , C01G23/003 , C01G23/005 , C01G23/006 , C01P2002/34 , C01P2002/72 , C01P2004/52 , C01P2006/32 , C01P2006/40 , H01M4/9033 , Y02E60/324 , Y02E60/50
摘要： [Problem] Many oxide-ion conductors exhibit high functionality at high temperatures due to the large weight and charge of oxide ions, and it has been difficult to achieve the functionality at low temperatures.
[Solution] A perovskite oxide having hydride ion conductivity, at least 1 at% of the oxide ions (O 2- ) contained in a titanium-containing perovskite oxide being substituted with hydride ions (H - ). This oxide, in which negatively charged hydride ions (H - ) are used for the ionic conduction, has both hydride ion conductivity and electron conductivity. As a starting material, the titanium-containing perovskite oxide is kept together with a powder of an alkali metal or alkaline-earth metal hydride selected from LiH, CaH 2 , SrH 2 , and BaH 2 in a temperature range of 300°C or higher and lower than the melting point of the hydride in a vacuum or an inert gas atmosphere to substitute some of the oxide ions in the oxide with the hydride ions, resulting in the introduction of the hydride ions into oxygen sites.
摘要翻译： [问题]由于氧化离子的重量和电荷大，许多氧化物离子导体在高温下表现出高功能性，并且在低温下难以实现功能性。 [解决方案]具有氢离子导电性的钙钛矿氧化物，其含有钛酸钙的氧化钛中的氧化物离子（O 2-）的至少1at％被氢离子（H - ）取代。使用带负电荷的氢离子（H - ）作为离子传导的氧化物具有氢离子传导性和电子传导性。作为起始原料，将含钛的钙钛矿氧化物与选自LiH，CaH 2，SrH 2和BaH 2的碱金属或碱土金属氢化物的粉末在300℃以上的温度范围内保持并且在真空或惰性气体气氛中低于氢化物的熔点，以氢化物离子代替氧化物中的一些氧化物离子，导致氢离子引入氧位。

4. 发明公开

EP3514114A1 SHEET CONTAINING TWO-DIMENSIONAL BOROHYDRIDE AND PRODUCTION METHOD FOR SHEET CONTAINING TWO-DIMENSIONAL BORON COMPOUND 审中-公开
公开(公告)号：EP3514114A1
公开(公告)日：2019-07-24
申请号：EP17862010.0
申请日：2017-10-18
申请人： University of Tsukuba , Tokyo Institute of Technology
发明人： KONDO Takahiro , NAKAMURA Junji , NISHINO Hiroaki , FUJINO Asahi , FUJIMORI Tomohiro , HOSONO Hideo , MIYAUCHI Masahiro
IPC分类号： C01B35/04
摘要： A two-dimensional hydrogen boride-containing sheet of the present invention has a two-dimensional network that consists of (HB) n (n ≥ 4).

5. 发明公开

EP3489197A1 METHOD FOR MANUFACTURING ELECTRIDE-FORM MAYENITE COMPOUND 有权转让
公开(公告)号：EP3489197A1
公开(公告)日：2019-05-29
申请号：EP17834288.7
申请日：2017-07-25
申请人： Tokyo Institute of Technology , Hirosaki University
发明人： HOSONO Hideo , YOKOYAMA Toshiharu , TODA Yoshitake , ISHIYAMA Shintaro
IPC分类号： C01F7/16 , H01B13/00
摘要： Provided is a manufacturing method with which it is possible to convert a mayenite-type compound to an electride, wherein a reducing agent is not required, reaction conditions include a temperature that is lower than that in the related art, and the reaction is performed more quickly in a simple manner, and, additionally, by requiring a lower amount of energy. Provided is a method for manufacturing an electride of mayenite-type compounds, the method being characterized in that a mayenite-type compound is converted to an electride by making a current directly flow through the mayenite-type compound by applying a voltage to the mayenite-type compound in a heating state.

6. 发明公开

EP3597292A1 METAL SUPPORT, SUPPORTED METAL CATALYST, PRODUCTION METHOD FOR AMMONIA, PRODUCTION METHOD FOR HYDROGEN, AND PRODUCTION METHOD FOR CYANAMIDE COMPOUND 审中-实审转让
公开(公告)号：EP3597292A1
公开(公告)日：2020-01-22
申请号：EP18767282.9
申请日：2018-03-16
申请人： Japan Science and Technology Agency , Tokyo Institute of Technology
发明人： HOSONO Hideo , KISHIDA Kazuhisa , KITANO Masaaki , YOKOYAMA Toshiharu
IPC分类号： B01J27/24 , B01J37/08 , C01B3/04 , C01C1/04 , C01C3/18
摘要： Provided are a supported metal material showing high catalytic activity, a supported metal catalyst, a method of producing ammonia and a method of producing hydrogen using the supported metal catalyst, and a method of producing a cyanamide compound. The supported metal material of the present invention is a supported metal material in which a transition metal is supported on a support, and the support is a cyanamide compound represented by the following general formula (1):MCN 2 (1), wherein M represents a group II element of the periodic table, and the specific surface area of the cyanamide compound is 1 m 2 g -1 or more.

7. 发明公开

EP3375521A1 SUPPORTED-METAL ARTICLE, SUPPORTED METAL CATALYST, AND AMMONIA SYNTHESIZING METHOD IN WHICH SAID CATALYST IS USED 审中-公开
公开(公告)号：EP3375521A1
公开(公告)日：2018-09-19
申请号：EP16864226.2
申请日：2016-11-09
申请人： Japan Science and Technology Agency , Tokyo Institute of Technology
发明人： HOSONO Hideo , HARA Michikazu , KITANO Masaaki , MIZOGUCHI Hiroshi , YOKOYAMA Toshiharu , YAMAGATA Kyosuke
IPC分类号： B01J23/78 , B01J23/58 , B01J23/63 , B01J37/04 , C01C1/04
CPC分类号： C01C1/0411 , B01J23/462 , B01J23/58 , B01J23/63 , B01J23/78 , B01J37/04 , C01C1/04 , C01G55/008 , C01P2002/70 , Y02P20/52
摘要： The present invention provides a supported metal catalyst, a method for synthesizing ammonia using said catalyst, and a supported metal material in which a transition metal is supported on a support, wherein the support is a metal hydride represented by general formula (1): XH n ... (1); and in general formula (1), X represents at least one selected from the group consisting of atoms from Groups 2 and 3, and lanthanoid atoms, and n is in a range of 2≦n≦3.

8. 发明公开

EP3156126A1 SUPPORT METAL CATALYST AND METHOD FOR SYNTHESIZING AMMONIA USING SAME CATALYST 审中-公开
标题翻译： VERFAHREN ZUR SYNTHETISIERUNG VON AMMONIAK MITHILFE DES KATALYSATORSTRÄGERMETALLKATALYSATOR
公开(公告)号：EP3156126A1
公开(公告)日：2017-04-19
申请号：EP15755657.2
申请日：2015-02-12
申请人： Japan Science and Technology Agency , Tokyo Institute of Technology
发明人： HOSONO Hideo , HARA Michikazu , KITANO Masaaki , YOKOYAMA Toshiharu , INOUE Yasunori , KAMBARA Shinji
IPC分类号： B01J27/24 , B01J27/22 , C01B21/06 , C01B32/90 , C01C1/04
CPC分类号： B01J27/24 , B01J23/462 , B01J23/745 , B01J23/75 , B01J27/22 , B01J35/0006 , B01J35/1009 , C01B21/0612 , C01C1/0411 , C01P2006/12 , Y02P20/52
摘要： A catalyst is provided which is used for continuously synthesizing ammonia using a gas containing hydrogen and nitrogen as a raw material, wherein a transition metal which exhibits catalytic activity is supported by a support, and the support is a two-dimensional electride or a precursor thereof. The two-dimensional electride or the precursor thereof is a metal nitride represented by MxNyHz (M represents one or two or more of Group II metals selected from the group consisting of Mg, Ca, Sr and Ba, and x, y and z are in ranges of 1 ≤ x ≤ 11, 1 ≤ y ≤ 8, and 0 ≤ z ≤ 4 respectively, in which x is an integer, and y and z are not limited to an integer) or M 3 N 2 (M is the same as above), or a metal carbide selected from the group consisting of Y 2 C, Sc 2 C, Gd 2 C, Tb 2 C, Dy 2 C, Ho 2 C and Er 2 C. These catalysts are used for continuously reacting nitrogen with hydrogen, which are raw materials, on the catalyst, wherein the reaction is performed in an ammonia synthesis reaction system under the preferable conditions of a reaction temperature which is equal to or higher than 100°C and equal to or lower than 600°C, and a reaction pressure which is equal to or higher than 10 kPa and lower than 20 MPa.
摘要翻译：提供了一种催化剂，其用于使用含有氢和氮作为原料的气体连续合成氨，其中具有催化活性的过渡金属由载体负载，并且载体是二维电子或其前体。二维电子或其前体是以M x N y H z表示的金属氮化物（M表示选自Mg，Ca，Sr和Ba的第II族金属中的一种或两种以上，x，y和z在分别为1‰¤x‰¤11，1‰¤y‰¤8和0‰¤z‰4，其中x为整数，y和z不限于整数）或M 3 N 2（M与上述相同），或选自Y 2 C，Sc 2 C，Gd 2 C，Tb 2 C，Dy 2 C，Ho 2 C和Er 2 C的金属碳化物。这些催化剂用于将氮气与作为原料的氢气连续反应在催化剂上，其中反应在氨合成反应体系中在优选的条件下进行，反应温度等于或高于100℃等于或低于600℃，反应压力等于或高于10kPa并低于20MPa。

9. 发明公开

EP2891627A1 METHOD FOR PRODUCING CONDUCTIVE MAYENITE COMPOUND POWDER 审中-实审转让
标题翻译： VERFAHREN ZUR HERSTELLUNG EINESLEITFÄHIGENMAYENIT-VERBINDUNGSPULVERS
公开(公告)号：EP2891627A1
公开(公告)日：2015-07-08
申请号：EP13833435.4
申请日：2013-08-20
申请人： Tokyo Institute of Technology
发明人： HOSONO Hideo , HARA Michikazu , INOUE Yasunori , KITANO Masaaki , HAYASHI Fumitaka , YOKOYAMA Toshiharu , MATSUISHI Satoru , TODA Yoshitake
IPC分类号： C01F7/16 , B01J23/58 , B01J37/02 , C01C1/04 , H01B13/00
CPC分类号： B01J21/16 , B01J23/02 , B01J23/462 , B01J23/58 , B01J35/0006 , B01J35/0033 , B01J35/026 , B01J35/1009 , B01J35/1014 , B01J37/0201 , B01J37/04 , B01J37/08 , B01J37/082 , B01J37/10 , B01J37/16 , B01J37/18 , B01J37/347 , C01B33/26 , C01C1/0411 , C01F7/02 , C01F7/164 , C01P2006/12 , C01P2006/40 , Y02P20/52 , Y10T428/2982
摘要： [Problem] A conductive mayenite compound is expected to be applied to cold electron emitters, conductors, organic EL electron injection electrodes, thermoelectric conversion materials, thermoelectric power generation materials, reducing agents, oxidants, catalysts and the like. If a conductive mayenite compound having a large specific surface area is obtained, the usefulness thereof in respective applications is remarkably increased. [Solution] A conductive mayenite compound powder having a conduction electron density of 10 15 cm -3 or more and a specific surface area of 5 m 2 g -1 or more is produced by: (1) a step for forming a precursor powder by subjecting a mixture of a starting material powder and water to a hydrothermal treatment; (2) a step for forming a mayenite compound powder by heating and dehydrating the precursor powder; (3) a step for forming an activated mayenite compound powder by heating the compound powder in an inert gas atmosphere or in a vacuum; and (4) a step for injecting electrons into the mayenite compound through a reduction treatment by mixing the activated mayenite compound powder with a reducing agent.
摘要翻译： [问题]预期导电的钙铝石化合物被应用于冷电子发射体，导体，有机EL电子注入电极，热电转换材料，热电发电材料，还原剂，氧化剂，催化剂等。如果获得具有大的比表面积的导电的钙铝石化合物，其在各种应用中的用途显着增加。 [溶液]导电电子密度为10 15 cm -3以上，比表面积为5m 2 g -1以上的导电的钙铝石类化合物粉末通过以下方法制造：（1）通过以下步骤形成前体粉末的步骤：将原料粉末和水的混合物进行水热处理; （2）通过加热和脱水前体粉末形成钙铝石化合物粉末的步骤; （3）通过在惰性气体气氛或真空中加热化合物粉末来形成活化的钙铝石化合物粉末的步骤; 和（4）通过将活化的钙铝石化合物粉末与还原剂混合，通过还原处理将电子注入钙铝石化合物的步骤。

10. 发明公开

EP3351509A1 LAVES PHASE INTERMETALLIC COMPOUND, CATALYST USING INTERMETALLIC COMPOUND, AND METHOD FOR PRODUCING AMMONIA 有权
公开(公告)号：EP3351509A1
公开(公告)日：2018-07-25
申请号：EP16846580.5
申请日：2016-09-15
申请人： Tokyo Institute of Technology , Japan Science and Technology Agency
发明人： HOSONO Hideo , YOKOYAMA Toshiharu , KITANO Masaaki , MIZOGUCHI Hiroshi , OGAWA Takaya
IPC分类号： C01C1/04 , B01J23/63
CPC分类号： B01J23/63 , C01C1/04 , C01C1/0411 , Y02P20/52
摘要： The invention provides a Laves phase intermetallic compound having a composition represented by general formula ARu 2 (A is Y, Sc, or at least one element selected from lanthanoid elements excluding Ce), the crystallite size thereof being 1 nm to 100 nm; a catalyst including the intermetallic compound as an active ingredient; and a method for producing ammonia using the same.

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