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    • 6. 发明公开
    • Apparatus for fractional distillation under vacuum
    • Vorrichtungfürdie fraktionierte Destillation unter Vakuum。
    • EP0120508A2
    • 1984-10-03
    • EP84200114.1
    • 1984-01-30
    • SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
    • Kanbier, DirkVan Kleef, Alfred Louis
    • B01D3/12
    • B01D3/04Y10S159/16Y10S159/41Y10S203/11
    • Apparatus for fractional distillation under vacuum, comprising an evacuable vessel (1), enclosing a first zone (11) for liquid to be distilled, a second zone (12) for distillate and a third zone (13) for residue, the vessel being provided with a plurality of vertical hollow elements (17) having sidewalls (18) forming evaporator surfaces and being provided with inlet means (20) at their upper ends for directing liquid to be distilled from the first zone (11) towards the evaporator surfaces, each hollow element (17) surrounding at least partly a vertical cooling surface (21) to cause condensation of vaporized liquid to form distillate, each hollow element (17) being further provided with mean's (26) for separately withdrawing distillate and residue from its interior into the second zone (12) and third zone (13), respectively. The vessel (1) preferably consists of detachably interconnected wall portions.
    • 用于在真空下分馏的装置,包括可抽空的容器(1),其包围用于待蒸馏的液体的第一区(11),用于馏出物的第二区(12)和用于残渣的第三区(13),所述容器设置 具有多个垂直中空元件(17),其具有形成蒸发器表面的侧壁(18),并且在其上端处设置有入口装置(20),用于将从第一区域(11)蒸馏的液体引向蒸发器表面,每个 中空元件(17)至少部分地围绕垂直冷却表面(21),以使蒸发的液体冷凝以形成馏出物,每个中空元件(17)还设置有用于将馏出物和残余物从其内部分别取出的装置(26) 第二区域(12)和第三区域(13)。 容器(1)优选地由可拆卸地连接的壁部分组成。