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1. 发明公开

EP3153533A1 METHOD FOR PRODUCING DIMETHYL POLYVINYLPHOSPHONATE AND POLYVINYLPHOSPHONIC ACID 审中-公开
标题翻译：多烯基磷杂环戊二烯基二苯乙烯磷酸酯
公开(公告)号：EP3153533A1
公开(公告)日：2017-04-12
申请号：EP15803277.1
申请日：2015-06-01
申请人： Maruzen Petrochemical Co., Ltd.
发明人： TAKAHASHI Takashi , MATSUSHITA Keisuke , SUGIYAMA Masaki , YOSHIDA Norihiro , IKAWA Eiichi , MITA Takahito , ENDO Masahiro
IPC分类号： C08F130/02 , C08F2/06 , C08F2/38 , C08F8/12
CPC分类号： C08F130/02 , C08F2/06 , C08F2/38 , C08F8/12
摘要： A method for producing poly(dimethyl vinylphosphonate) from a monomer component mainly containing dimethyl vinylphosphonate by anionic polymerization in the presence of an anionic polymerization initiator, the method being characterized in that an aliphatic ether is used as a polymerization solvent, and a method for producing poly (vinylphosphonic acid) characterized in that the poly(dimethyl vinylphosphonate) obtained by the former method is hydrolyzed in the presence of an acid are provided. The methods make it possible to easily produce a poly(dimethyl vinylphosphonate) which has a high molecular weight and in which the molecular weight is controlled, and make it possible to produce a poly (vinylphosphonic acid) which has a high molecular weight and in which the molecular weight is controlled corresponding to the poly(dimethyl vinylphosphonate).
摘要翻译：在阴离子聚合引发剂存在下，通过阴离子聚合从主要含有乙烯基膦酸二甲酯的单体组分制备聚（二甲基乙烯基膦酸酯）的方法，其特征在于使用脂肪族醚作为聚合溶剂，聚（乙烯基膦酸），其特征在于，通过前述方法获得的聚（二甲基乙烯基膦酸酯）在酸的存在下水解。该方法使得可以容易地制备具有高分子量并且其分子量被控制的聚（二甲基乙烯基膦酸酯），并且可以制备具有高分子量的聚（乙烯基膦酸），其中对应于聚（二甲基乙烯基膦酸酯）控制分子量。

2. 发明公开

EP3318583A1 IMPROVED METHOD FOR PRODUCING HYDROXY GROUP-CONTAINING VINYL ETHER POLYMER 有权
标题翻译：生产含羟基乙烯基醚聚合物的改进方法
公开(公告)号：EP3318583A1
公开(公告)日：2018-05-09
申请号：EP16821286.8
申请日：2016-06-29
申请人： Maruzen Petrochemical Co., Ltd.
发明人： SUGIHARA Shinji , YOSHIDA Norihiro
IPC分类号： C08F16/26 , C08F4/04 , C08K3/18 , C08L29/10 , C09D11/00 , C09D129/10 , C09J129/10
CPC分类号： C08F16/26 , C08F4/04 , C08K3/18 , C08L29/10 , C09D11/00 , C09D129/10 , C09J129/10
摘要： [Object]
To provide a simple and efficient method for producing a hydroxyl group-containing vinyl ether polymer, without the need of a removal step of low boiling point impurities such as residual monomers and initiator residues and polyacetal, or the like, by improving the monomer conversion rate while reducing the amount of a polymerization initiator to be used, and suppressing generation of polyacetal.
[Means for solving problem]
A method for producing a hydroxyl group-containing vinyl ether polymer according to the present invention comprises:
a step of radical polymerizing at least one vinyl ether selected from vinyl ether having a hydroxyl group represented by the following formula (2):

wherein R 7 represents an alkylene group which is straight-chained, branched or comprises an alicyclic structure, and p is 1, 2, or 3,
in the presence of water as a polymerization solvent and an azo compound represented by the following formula (1) as a polymerization initiator:

wherein R 1 to R 4 each independently represent a hydrogen atom or an alkyl group and R 5 and R 6 each independently represent an alkoxy group optionally having a substituent group or an alkyl amino group optionally having a substituent group.
摘要翻译：本发明提供一种简单且有效的含羟基乙烯基醚聚合物的制造方法，不需要除去残留单体，引发剂残渣，聚缩醛等低沸点杂质的工序，单体转化率，同时减少使用的聚合引发剂的量，并抑制聚缩醛的产生。 [解决问题的手段]本发明的含羟基乙烯基醚聚合物的制造方法包括：将选自下述式（2）所示的具有羟基的乙烯基醚中的至少一种乙烯基醚自由基聚合的工序）表示的偶氮化合物：其中R7表示在作为聚合溶剂的水存在下直链，支化或包含脂环结构且p为1,2或3的亚烷基和由下式 1）作为聚合引发剂：其中R 1至R 4各自独立地表示氢原子或烷基，并且R 5和R 6各自独立地表示任选具有取代基的烷氧基或任选具有取代基的烷基氨基。

3. 发明公开

EP2465885A1 VINYL ETHER-BASED STAR POLYMER AND PROCESS FOR PRODUCTION THEREOF 审中-公开
标题翻译： STERNPOLYMER AUF VINYLETHYLENBASIS UND HERSTELLUNGSVERFAHRENDAFÜR
公开(公告)号：EP2465885A1
公开(公告)日：2012-06-20
申请号：EP10808108.4
申请日：2010-07-01
申请人： Maruzen Petrochemical Co., Ltd.
发明人： YOSHIDA Norihiro
IPC分类号： C08F297/00 , C08F4/52
CPC分类号： C08F297/00 , C08F4/52
摘要： Provided is a vinyl ether-based star polymer that has arms containing a copolymer of a vinyl ether-based polymer and a oxystyrene-based polymer, and a process for production of the star polymer that is capable of being carried out continuously in a series of steps. The process includes a vinyl ether-based star polymer having arms containing a copolymer of a vinyl ether-based polymer and an oxystyrene-based polymer, and a process for production of the vinyl ether-based star polymer, containing: subjecting a vinyl ether-based monomer to living cationic polymerization in the presence of an initiating species, a Lewis acid that is suitable for cationic polymerization of the vinyl ether-based monomer, and a solvent; then subjecting an oxystyrene-based monomer to living cationic polymerization with a Lewis acid that is suitable for cationic polymerization of the oxystyrene-based monomer added thereto; adding a divinyl compound to introduce a vinyl group to a side chain; and forming a core through intermolecular crosslinking with the vinyl group.
摘要翻译：本发明提供一种具有乙烯基醚类聚合物和氧苯乙烯类聚合物的共聚物的臂的乙烯基醚系星形聚合物以及能够连续地进行一系列的聚合物的星形聚合物的制造方法脚步。该方法包括具有包含乙烯基醚类聚合物和氧苯乙烯类聚合物的共聚物的臂的乙烯基醚类星形聚合物，以及乙烯基醚系星形聚合物的制造方法，其特征在于，在起始物质存在下，使用阳离子聚合反应，适用于乙烯基醚类单体的阳离子聚合的路易斯酸和溶剂; 然后用与适用于添加氧基苯乙烯类单体的阳离子聚合的路易斯酸进行氧苯乙烯类单体的活性阳离子聚合; 加入二乙烯基化合物以将乙烯基引入侧链; 并通过与乙烯基的分子间交联形成芯。

4. 发明公开

EP3424964A1 COPOLYMER, ANTITHROMBOTIC COATING AGENT USING SAME AND MEDICAL DEVICE 有权
公开(公告)号：EP3424964A1
公开(公告)日：2019-01-09
申请号：EP17759472.8
申请日：2017-01-24
申请人： Maruzen Petrochemical Co., Ltd. , National University Corporation Yamagata University
发明人： TANAKA Masaru , YOSHIDA Norihiro
IPC分类号： C08F216/18 , A61L33/06
摘要： The present invention has an object to find a biocompatible material that has excellent film formation properties and resistance to water dissolution, and can be easily applied on various bases as a coating, while having excellent antithrombotic properties, and to provide an antithrombotic coating agent and an antithrombotic coating film produced by using the biocompatible material, and a medical device provided with the antithrombotic coating film. Means for achieving the object are a copolymer containing at least one repeating unit (A) represented by formula (1) (wherein, n represents an integer of 2 to 10 and R 1 represents a methyl group or an ethyl group), and at least one repeating unit (B) represented by formula (2) (wherein R 2 represents an aliphatic hydrocarbon group); an antithrombotic coating agent containing the copolymer and an organic solvent; an antithrombotic coating film formed of the copolymer; and a medical device provided with the coating film.

5. 发明公开

EP3395842A1 PROCESS FOR PRODUCING VINYL ETHER POLYMER HAVING HYDROXY GROUPS IN SIDE CHAINS, AND TEMPERATURE-RESPONSIVE POLYMER MIXTURE 有权
公开(公告)号：EP3395842A1
公开(公告)日：2018-10-31
申请号：EP16878525.1
申请日：2016-12-14
申请人： Maruzen Petrochemical Co., Ltd.
发明人： YOSHIDA Norihiro , SUGIHARA Shinji
IPC分类号： C08F116/12 , C08F2/16 , C08F4/04
CPC分类号： C08F2/16 , C08F4/04 , C08F116/12
摘要： [Object] To provide a method for producing a vinyl ether polymer having a hydroxyl group on the side chain, wherein the vinyl ether polymer having a low viscosity and excellent workability and processability is produced in a simple and efficient method.
[Means for solving problem] The present invention relates to a method for producing a vinyl ether polymer having a hydroxyl group on the side chain, characterized in that vinyl ether comprising a hydroxyl group is subjected to radical polymerization by using an oil-soluble azo polymerization initiator, in the presence of a mixed solvent comprising water and an organic solvent selected from alcohol or cyclic ether radical polymerization.

6. 发明公开

EP2412737A1 VINYL ETHER-BASED STAR POLYMER AND PROCESS FOR PRODUCTION THEREOF 审中-公开
标题翻译：基于乙烯基醚的星形聚合物及其生产方法
公开(公告)号：EP2412737A1
公开(公告)日：2012-02-01
申请号：EP10755729.0
申请日：2010-01-08
申请人： Maruzen Petrochemical CO., LTD.
发明人： YOSHIDA Norihiro
IPC分类号： C08F293/00
CPC分类号： C08F297/00 , G03F7/038
摘要： Provided is a vinyl ether-based star polymer which has an arm including a vinyl ether polymer and an arm including an oxystyrene polymer. Also provided is a process for producing the star polymer, which can be continuously carried out in a series of steps. Said vinyl ether-based star polymer and process for producing the same are such that the polymer includes a core and polymer-chain arm portions extending from the core, in which an arm portion including vinyl ether repeating units and an arm portion including oxystyrene repeating units are provided.
摘要翻译：提供一种乙烯基醚系星形聚合物，其具有包含乙烯基醚聚合物的臂和包含氧化苯乙烯聚合物的臂。还提供了生产星形聚合物的方法，其可以连续地在一系列步骤中进行。所述基于乙烯基醚的星形聚合物及其制造方法使得聚合物包含芯和从芯延伸的聚合物链臂部分，其中包含乙烯基醚重复单元的臂部分和包含氧苯乙烯重复单元的臂部分被提供。

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