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1. 发明公开

EP0398620A3 Poly(oxyalkylene) modified phthalocyanine colorants 失效
标题翻译：聚（氧化烯）改性的酞菁着色剂
公开(公告)号：EP0398620A3
公开(公告)日：1991-02-27
申请号：EP90305187.8
申请日：1990-05-15
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Rekers, John William , Moody, David Jesse , Weaver, Max Allen
IPC分类号： C09B47/04 , C08K5/3415 , C08K5/42
CPC分类号： C09B47/20 , C08K5/43 , C09B47/18 , C09B47/22 , C09B47/26 , C09B69/00
摘要： Colorants and polymeric or resinous compositions containing the same, including polymeric substrates, especially polyurethane foams which are tinted or deeply colored with one or a mixture of the colorants which have the general formulae
A 1 -[SO 2 -N(R 3 )-Y] 1-4 , A 2 -[D-Z-SO 2 -N(R 2 )-Y] 1-16 , or
wherein: R 2 is selected from hydrogen or unsubstituted or substituted alkyl, cycloalkyl, aryl or Y; each of A 1 , A 2 , and A3 is a nonionic metallophthalocyanine chromophore which can be substituted or unsubstituted; Z is an arylene moiety; each D or D is selected from a covalent bond or a linking group consisting of or containing at least one of -0-, -S-, -N(R 3 )-, or -N(SO 2 R 4 )-as the linking moiety, wherein R4 is unsubstituted or substituted alkyl, cycloaliphatic or aryl, and R 3 is R 4 or hydrogen; or D in combination with Z can also be a covalent bond; Y is a poly(oxyalkylene) moiety having an average molecular weight of from 150 to about 10,000 and containing at least about 50 mole percent of monomeric units or mixture thereof of the formula (-RO-) wherein each R is substituted or unsubstituted straight or branched alkylene of 2-4 carbons or mixtures thereof, and containing at least three -RO- units; wherein ring P can be unsubstituted or substituted in addition to the -(D -Y) moieties; and wherein each aliphatic hydrocarbon portion or moiety of the groups, moieties or substituents recited above contains from 1-20 carbons and wherein n is 1-16, except when -D-Z- is a covalent bond then n is equal to 1-4.
摘要翻译：着色剂和含有该着色剂的聚合物或树脂组合物，包括聚合物基材，尤其是用一种或多种具有通式A1- [SO2-N（R3）-Y] 1- 4，A2- [DZ-SO2-N（R2）-Y] 1-16，或其中：R2选自氢或未取代或取代的烷基，环烷基，芳基或Y; A1，A2和A3中的每一个是可以被取代或未被取代的非离子型金属酞菁发色团; Z是亚芳基部分; 各D或D选自共价键或由-O-，-S - ， - N（R 3） - 或-N（SO 2 R 4） - 中的至少一个组成或包含其中的至少一个的连接基团作为连接部分，其中 R4是未取代的或取代的烷基，脂环族基或芳基，并且R3是R4或氢; 或D与Z结合也可以是共价键; Y是平均分子量为150-约10,000的聚（氧化烯）部分，并含有至少约50％（摩尔）式（-RO-）的单体单元或其混合物，其中每个R是取代或未取代的直链或支链具有2-4个碳原子的支链亚烷基或其混合物，并且含有至少三个-RO-单元; 其中环P可以是未取代的或除了 - （D-Y）部分以外还被取代; 并且其中上述基团，部分或取代基的每个脂族烃部分或部分含有1至20个碳，并且其中n为1至16，除非-D-Z-为共价键时，则n等于1至4。

2. 发明公开

EP0529162A1 Colorants and intermediates therefor having branched poly(oxyalkylene)moieties, and their manufacture 失效
标题翻译： Farbstoffe und Zwischenprodukte mit verzweigten Poly（oxykylen）-Resten sowie ihre Herstellung。
公开(公告)号：EP0529162A1
公开(公告)日：1993-03-03
申请号：EP91307834.1
申请日：1991-08-28
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Hines, John Bery , Moody, David Jesse , Kluger, Edward William
IPC分类号： C09B69/10 , D06P5/13 , C08G65/28
CPC分类号： C08G65/334 , C08G65/2627 , C08G65/333 , C09B69/00 , D06P5/138
摘要： Colorants and compositions useful as a fugitive or permanent colorant for a variety of substrates, or as intermediates for their manufacture, and having one or more improved properties of enhanced aqueous washability, compatibility with and non-extractibility from thermoplastic resins, or reactivity with resins having reactive functionality, said composition having the formula C(Z)₁₋₈ wherein:
C is the residue of a reactant having from 1-8 nucleophilic site residues to which the Z moieties are attached; said Z moieties containing at least about 60 weight percent of poly(oxyalkylene) which is comprised of

(a) at least one glycidol residue segment of 2-6 glycidol residues attached to a nucleophilic site of C, wherein said poly(oxyalkylene) contains a total of from 2-20 glycidol residues,
(b) and wherein said poly(oxyalkylene) further contains the residues of one or more other epoxide reactants of ethylene oxide (EO), propylene oxide (PO), or butylene oxide (BO), or mixtures thereof, wherein said poly(oxyalkylene) contains a total of from about 10 to about 600 of said EO, PO or BO residues, or mixtures thereof, at least about 75 mole percent of which are EO residues,
(c) and with the provisions that the ratio of the total of - O-PO- and -O-BO- linkages of all glycidol residues to the total of all functional oxy linkages of said glycidol residues is less than one, and the molar ratio of EO residues to glycidol residues is from 4 to 75.
摘要翻译：可用作各种底物的挥发性或永久性着色剂的着色剂和组合物，或作为其制造的中间体，并且具有一种或多种改进的水性洗涤性，与热塑性树脂的相容性和不可萃取性的改进性能，或与具有所述组合物具有式C（Z）1-8，其中：C是具有与Z部分连接的1-8个亲核位点残基的反应物的残基; 所述Z部分含有至少约60重量％的聚（氧化烯），其由（a）至少一个连接到C的亲核位点的2-6个缩水甘油残基的缩水甘油残基部分组成，其中所述聚（氧化烯）含有总共2-20个缩水甘油残基，（b），其中所述聚（氧化烯）还包含环氧乙烷（EO），环氧丙烷（PO）或环氧丁烷（BO））的一种或多种其它环氧化物反应物的残基，或其混合物，其中所述聚（氧化烯）含有总共约10至约600的所述EO，PO或BO残基或其混合物，其至少约75摩尔％为EO残基，（c）和所有缩水甘油残基的-O-PO-和-O-BO-键的总量与所述缩水甘油残基的所有功能性氧键的总和的比例小于1，EO残基与缩水甘油残基为4-75

3. 发明公开

EP0166566A3 Resin colorants and resin coloration 失效
标题翻译：树脂色素和树脂色彩
公开(公告)号：EP0166566A3
公开(公告)日：1986-11-20
申请号：EP85304352
申请日：1985-06-18
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Moore, Patrick David
IPC分类号： C09B29/033 , C08K05/23 , C09B69/10
CPC分类号： C09B69/106 , C08G18/38 , C08G18/50 , C08K5/45 , C09B29/0059 , C08L75/04
摘要： A polyurethane resin is colored by incorporating, during production, a reactive coloring agent of the formula

wherein R 1 , R 2 and R 3 are each hydrogen or a substituent, e.g. a carbonyl-containing group, and A is an organic dyestuff coupler. The agents are novel when A is 4-aminophenyl and the amine carries two substituents independently selected from polyalkylene oxide radicals, radicals of copolymers of polyalkylene oxides, and radicals of hydroxyalkylenes.

4. 发明公开

EP0074707A3 Polyamines and their use as curing agents 失效
标题翻译：聚氨酯及其作为固化剂使用
公开(公告)号：EP0074707A3
公开(公告)日：1983-09-14
申请号：EP82303881
申请日：1982-07-22
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Iyer, Venketa Subramanian
IPC分类号： C07C87/22 , C07C87/20 , C07C93/02 , C07C87/38 , C07C87/28 , C07C87/50 , C07C87/36 , C07C147/12 , C08G59/50
CPC分类号： C08G59/504 , C08G59/50 , C08G65/322 , C08G65/33379
摘要： A polyamine of the formula
wherein R, is H or C 1-\12 alkyl;
R 2 and R 3 are independently selected from H and C 1-8 alkyl; R 4 is H or
R s is a radical having a valency of n and which is the radical of a C 5-30 alkane, a C 12-30 aromatic compound or C 5-60 cycloalkane or is derived from an amine-terminated polygycol having a molecular weight of from 100 to 6,000 and from 2 to 100 ether linkages; and n is an integer of from 2 to 15. These compounds can be used as curing agents for epoxy resins. They can be prepared by reduction of novel nitro analogues, themselves prepared from a nitroalkane, an aldehyde and a polyamine.

5. 发明授权

EP0445926B1 Organic materials having sulfonamido linked poly(oxyalkylene) moieties and their preparation 失效
标题翻译：穿其中sulfonamidogebundene聚（氧化烯）的有机材料基团和它们的制备
公开(公告)号：EP0445926B1
公开(公告)日：1996-08-21
申请号：EP91301134.2
申请日：1991-02-12
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Harris, Jeffery Reed , Weaver, Max Allen , Moody, David Jesse
IPC分类号： C09B69/10 , C08G65/32
CPC分类号： C07D209/48 , C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/3348 , C09B69/00

6. 发明授权

EP0398620B1 Poly(oxyalkylene) modified phthalocyanine colorants 失效
标题翻译：聚（氧化烯） - 改性酞菁酞菁
公开(公告)号：EP0398620B1
公开(公告)日：1996-04-17
申请号：EP90305187.8
申请日：1990-05-15
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Rekers, John William , Moody, David Jesse , Weaver, Max Allen
IPC分类号： C09B47/04 , C08K5/3415 , C08K5/42
CPC分类号： C09B47/20 , C08K5/43 , C09B47/18 , C09B47/22 , C09B47/26 , C09B69/00

7. 发明授权

EP0166566B1 Resin colorants and resin coloration 失效
标题翻译：树脂颜料和树脂色彩
公开(公告)号：EP0166566B1
公开(公告)日：1992-10-07
申请号：EP85304352.9
申请日：1985-06-18
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Moore, Patrick David
IPC分类号： C09B29/033 , C08K5/23 , C09B69/10
CPC分类号： C09B69/106 , C08G18/38 , C08G18/50 , C08K5/45 , C09B29/0059 , C08L75/04

8. 发明公开

EP0445926A2 Organic materials having sulfonamido linked poly(oxyalkylene) moieties and their preparation 失效
标题翻译： Organische Materialien，die sulfamidogebundene Poly（oxenylen）gruppen tragen und ihre Herstellung。
公开(公告)号：EP0445926A2
公开(公告)日：1991-09-11
申请号：EP91301134.2
申请日：1991-02-12
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Harris, Jeffery Reed , Weaver, Max Allen , Moody, David Jesse
IPC分类号： C09B69/10 , C08G65/32
CPC分类号： C07D209/48 , C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/3348 , C09B69/00
摘要： The process for chemically modifying metal-free, organic material for improving one or more properties thereof such as water dispersibility, compatibility with other organics, or increased chemical reactivity, wherein the process includes providing material with from 1-6 sulfonylhalide groups or sulfonate ester groups or mixtures thereof, and contacting the material under sulfonamido forming conditions with one or more reactants containing one or more poly(oxyalkylene) moieties, each of the reactants having from 1 to 4 functional amine groups, and each of the poly(oxyalkylene) moieties being comprised of from about 4 to about 200 epoxide reactant residues at least about 50 mole percent of which residues contain 2-4 carbons.
摘要翻译：化学改性无机有机材料以改进其一种或多种性质如水分散性，与其它有机物的相容性或增加的化学反应性的方法，其中该方法包括提供具有1-6个磺酰卤基团或磺酸酯基团的材料或其混合物，并且在亚磺酰氨基形成条件下使材料与一种或多种含有一个或多个聚（氧化烯）部分的反应物接触，每个反应物具有1至4个官能胺基团，并且每个聚（氧化烯）部分为由约4至约200个环氧化物反应物残余物组成，其残留物的至少约50摩尔％含有2-4个碳。

9. 发明公开

EP0398620A2 Poly(oxyalkylene) modified phthalocyanine colorants 失效
标题翻译：聚（氧化烯） - 改性酞菁酞菁。
公开(公告)号：EP0398620A2
公开(公告)日：1990-11-22
申请号：EP90305187.8
申请日：1990-05-15
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Rekers, John William , Moody, David Jesse , Weaver, Max Allen
IPC分类号： C09B47/04 , C08K5/3415 , C08K5/42
CPC分类号： C09B47/20 , C08K5/43 , C09B47/18 , C09B47/22 , C09B47/26 , C09B69/00
摘要： Colorants and polymeric or resinous compositions containing the same, including polymeric substrates, especially polyurethane foams which are tinted or deeply colored with one or a mixture of the colorants which have the general formulae
A 1 -[SO 2 -N(R 3 )-Y] 1-4 , A 2 -[D-Z-SO 2 -N(R 2 )-Y] 1-16 , or
wherein: R 2 is selected from hydrogen or unsubstituted or substituted alkyl, cycloalkyl, aryl or Y; each of A 1 , A 2 , and A3 is a nonionic metallophthalocyanine chromophore which can be substituted or unsubstituted; Z is an arylene moiety; each D or D is selected from a covalent bond or a linking group consisting of or containing at least one of -0-, -S-, -N(R 3 )-, or -N(SO 2 R 4 )-as the linking moiety, wherein R4 is unsubstituted or substituted alkyl, cycloaliphatic or aryl, and R 3 is R 4 or hydrogen; or D in combination with Z can also be a covalent bond; Y is a poly(oxyalkylene) moiety having an average molecular weight of from 150 to about 10,000 and containing at least about 50 mole percent of monomeric units or mixture thereof of the formula (-RO-) wherein each R is substituted or unsubstituted straight or branched alkylene of 2-4 carbons or mixtures thereof, and containing at least three -RO- units; wherein ring P can be unsubstituted or substituted in addition to the -(D -Y) moieties; and wherein each aliphatic hydrocarbon portion or moiety of the groups, moieties or substituents recited above contains from 1-20 carbons and wherein n is 1-16, except when -D-Z- is a covalent bond then n is equal to 1-4.
摘要翻译：着色剂和含有它们的聚合物或树脂组合物，包括聚合物基材，特别是聚氨酯泡沫，其具有通式A1- [SO2-N（R2）-Y] 1- 4，A2- [DZ-SO2-N（R2）-Y] 1-16或其中：R2选自氢或未取代或取代的烷基，环烷基，芳基或Y; A1，A2和A3中的每一个是可以被取代或未取代的非离子金属酞菁发色团; Z是亚芳基; 每个D或D min选自共价键或由-O，-S-，-N（R 3） - 或-N（SO 2 R 4） - 中的至少一个组成或含有的连接基团作为连接部分，其中R4是未取代或取代的烷基，脂环族或芳基，R3是R4或氢; 或D与Z组合也可以是共价键; Y是平均分子量为150至约10,000并含有至少约50摩尔％的式（-RO-）的单体单元或其混合物的聚（氧化烯）部分，其中每个R是取代或未取代的直链或 2-4个碳的支链亚烷基或其混合物，并含有至少三个-RO-单元; 其中除了 - （D min -Y）部分之外，环P可以是未取代的或取代的; 并且其中上述基团，部分或取代基的每个脂族烃部分或部分含有1-20个碳，并且其中n为1-16，除非当-D-Z-为共价键时，则n等于1-4。

10. 发明授权

EP0437105B1 Intermediates and colorants having primary hydroxyl enriched poly(oxyalkylene) moieties and their preparation 失效
标题翻译：中间体和染料具有提高的伯羟基基团的聚（氧化烯）基团和它们的制备
公开(公告)号：EP0437105B1
公开(公告)日：1996-11-13
申请号：EP90314335.2
申请日：1990-12-28
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Moody, David Jesse , Kluger, Edward William , Rekers, John William
IPC分类号： C09B69/10 , C08G65/28
CPC分类号： C08G65/2627 , C09B69/00

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