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1. 发明公开

EP0529162A1 Colorants and intermediates therefor having branched poly(oxyalkylene)moieties, and their manufacture 失效
标题翻译： Farbstoffe und Zwischenprodukte mit verzweigten Poly（oxykylen）-Resten sowie ihre Herstellung。
公开(公告)号：EP0529162A1
公开(公告)日：1993-03-03
申请号：EP91307834.1
申请日：1991-08-28
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Hines, John Bery , Moody, David Jesse , Kluger, Edward William
IPC分类号： C09B69/10 , D06P5/13 , C08G65/28
CPC分类号： C08G65/334 , C08G65/2627 , C08G65/333 , C09B69/00 , D06P5/138
摘要： Colorants and compositions useful as a fugitive or permanent colorant for a variety of substrates, or as intermediates for their manufacture, and having one or more improved properties of enhanced aqueous washability, compatibility with and non-extractibility from thermoplastic resins, or reactivity with resins having reactive functionality, said composition having the formula C(Z)₁₋₈ wherein:
C is the residue of a reactant having from 1-8 nucleophilic site residues to which the Z moieties are attached; said Z moieties containing at least about 60 weight percent of poly(oxyalkylene) which is comprised of

(a) at least one glycidol residue segment of 2-6 glycidol residues attached to a nucleophilic site of C, wherein said poly(oxyalkylene) contains a total of from 2-20 glycidol residues,
(b) and wherein said poly(oxyalkylene) further contains the residues of one or more other epoxide reactants of ethylene oxide (EO), propylene oxide (PO), or butylene oxide (BO), or mixtures thereof, wherein said poly(oxyalkylene) contains a total of from about 10 to about 600 of said EO, PO or BO residues, or mixtures thereof, at least about 75 mole percent of which are EO residues,
(c) and with the provisions that the ratio of the total of - O-PO- and -O-BO- linkages of all glycidol residues to the total of all functional oxy linkages of said glycidol residues is less than one, and the molar ratio of EO residues to glycidol residues is from 4 to 75.
摘要翻译：可用作各种底物的挥发性或永久性着色剂的着色剂和组合物，或作为其制造的中间体，并且具有一种或多种改进的水性洗涤性，与热塑性树脂的相容性和不可萃取性的改进性能，或与具有所述组合物具有式C（Z）1-8，其中：C是具有与Z部分连接的1-8个亲核位点残基的反应物的残基; 所述Z部分含有至少约60重量％的聚（氧化烯），其由（a）至少一个连接到C的亲核位点的2-6个缩水甘油残基的缩水甘油残基部分组成，其中所述聚（氧化烯）含有总共2-20个缩水甘油残基，（b），其中所述聚（氧化烯）还包含环氧乙烷（EO），环氧丙烷（PO）或环氧丁烷（BO））的一种或多种其它环氧化物反应物的残基，或其混合物，其中所述聚（氧化烯）含有总共约10至约600的所述EO，PO或BO残基或其混合物，其至少约75摩尔％为EO残基，（c）和所有缩水甘油残基的-O-PO-和-O-BO-键的总量与所述缩水甘油残基的所有功能性氧键的总和的比例小于1，EO残基与缩水甘油残基为4-75

2. 发明公开

EP0398620A3 Poly(oxyalkylene) modified phthalocyanine colorants 失效
标题翻译：聚（氧化烯）改性的酞菁着色剂
公开(公告)号：EP0398620A3
公开(公告)日：1991-02-27
申请号：EP90305187.8
申请日：1990-05-15
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Rekers, John William , Moody, David Jesse , Weaver, Max Allen
IPC分类号： C09B47/04 , C08K5/3415 , C08K5/42
CPC分类号： C09B47/20 , C08K5/43 , C09B47/18 , C09B47/22 , C09B47/26 , C09B69/00
摘要： Colorants and polymeric or resinous compositions containing the same, including polymeric substrates, especially polyurethane foams which are tinted or deeply colored with one or a mixture of the colorants which have the general formulae
A 1 -[SO 2 -N(R 3 )-Y] 1-4 , A 2 -[D-Z-SO 2 -N(R 2 )-Y] 1-16 , or
wherein: R 2 is selected from hydrogen or unsubstituted or substituted alkyl, cycloalkyl, aryl or Y; each of A 1 , A 2 , and A3 is a nonionic metallophthalocyanine chromophore which can be substituted or unsubstituted; Z is an arylene moiety; each D or D is selected from a covalent bond or a linking group consisting of or containing at least one of -0-, -S-, -N(R 3 )-, or -N(SO 2 R 4 )-as the linking moiety, wherein R4 is unsubstituted or substituted alkyl, cycloaliphatic or aryl, and R 3 is R 4 or hydrogen; or D in combination with Z can also be a covalent bond; Y is a poly(oxyalkylene) moiety having an average molecular weight of from 150 to about 10,000 and containing at least about 50 mole percent of monomeric units or mixture thereof of the formula (-RO-) wherein each R is substituted or unsubstituted straight or branched alkylene of 2-4 carbons or mixtures thereof, and containing at least three -RO- units; wherein ring P can be unsubstituted or substituted in addition to the -(D -Y) moieties; and wherein each aliphatic hydrocarbon portion or moiety of the groups, moieties or substituents recited above contains from 1-20 carbons and wherein n is 1-16, except when -D-Z- is a covalent bond then n is equal to 1-4.
摘要翻译：着色剂和含有该着色剂的聚合物或树脂组合物，包括聚合物基材，尤其是用一种或多种具有通式A1- [SO2-N（R3）-Y] 1- 4，A2- [DZ-SO2-N（R2）-Y] 1-16，或其中：R2选自氢或未取代或取代的烷基，环烷基，芳基或Y; A1，A2和A3中的每一个是可以被取代或未被取代的非离子型金属酞菁发色团; Z是亚芳基部分; 各D或D选自共价键或由-O-，-S - ， - N（R 3） - 或-N（SO 2 R 4） - 中的至少一个组成或包含其中的至少一个的连接基团作为连接部分，其中 R4是未取代的或取代的烷基，脂环族基或芳基，并且R3是R4或氢; 或D与Z结合也可以是共价键; Y是平均分子量为150-约10,000的聚（氧化烯）部分，并含有至少约50％（摩尔）式（-RO-）的单体单元或其混合物，其中每个R是取代或未取代的直链或支链具有2-4个碳原子的支链亚烷基或其混合物，并且含有至少三个-RO-单元; 其中环P可以是未取代的或除了 - （D-Y）部分以外还被取代; 并且其中上述基团，部分或取代基的每个脂族烃部分或部分含有1至20个碳，并且其中n为1至16，除非-D-Z-为共价键时，则n等于1至4。

3. 发明公开

EP0166566A3 Resin colorants and resin coloration 失效
标题翻译：树脂色素和树脂色彩
公开(公告)号：EP0166566A3
公开(公告)日：1986-11-20
申请号：EP85304352
申请日：1985-06-18
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Moore, Patrick David
IPC分类号： C09B29/033 , C08K05/23 , C09B69/10
CPC分类号： C09B69/106 , C08G18/38 , C08G18/50 , C08K5/45 , C09B29/0059 , C08L75/04
摘要： A polyurethane resin is colored by incorporating, during production, a reactive coloring agent of the formula

wherein R 1 , R 2 and R 3 are each hydrogen or a substituent, e.g. a carbonyl-containing group, and A is an organic dyestuff coupler. The agents are novel when A is 4-aminophenyl and the amine carries two substituents independently selected from polyalkylene oxide radicals, radicals of copolymers of polyalkylene oxides, and radicals of hydroxyalkylenes.

4. 发明公开

EP0074707A3 Polyamines and their use as curing agents 失效
标题翻译：聚氨酯及其作为固化剂使用
公开(公告)号：EP0074707A3
公开(公告)日：1983-09-14
申请号：EP82303881
申请日：1982-07-22
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Iyer, Venketa Subramanian
IPC分类号： C07C87/22 , C07C87/20 , C07C93/02 , C07C87/38 , C07C87/28 , C07C87/50 , C07C87/36 , C07C147/12 , C08G59/50
CPC分类号： C08G59/504 , C08G59/50 , C08G65/322 , C08G65/33379
摘要： A polyamine of the formula
wherein R, is H or C 1-\12 alkyl;
R 2 and R 3 are independently selected from H and C 1-8 alkyl; R 4 is H or
R s is a radical having a valency of n and which is the radical of a C 5-30 alkane, a C 12-30 aromatic compound or C 5-60 cycloalkane or is derived from an amine-terminated polygycol having a molecular weight of from 100 to 6,000 and from 2 to 100 ether linkages; and n is an integer of from 2 to 15. These compounds can be used as curing agents for epoxy resins. They can be prepared by reduction of novel nitro analogues, themselves prepared from a nitroalkane, an aldehyde and a polyamine.

5. 发明授权

EP0437105B1 Intermediates and colorants having primary hydroxyl enriched poly(oxyalkylene) moieties and their preparation 失效
标题翻译：中间体和染料具有提高的伯羟基基团的聚（氧化烯）基团和它们的制备
公开(公告)号：EP0437105B1
公开(公告)日：1996-11-13
申请号：EP90314335.2
申请日：1990-12-28
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Moody, David Jesse , Kluger, Edward William , Rekers, John William
IPC分类号： C09B69/10 , C08G65/28
CPC分类号： C08G65/2627 , C09B69/00

6. 发明公开

EP0445926A3 Organic materials having sulfonamido linked poly(oxyalkylene) moieties and their preparation 失效
标题翻译：具有磺酰胺连接的聚（氧亚氨基）体系的有机材料及其制备
公开(公告)号：EP0445926A3
公开(公告)日：1991-11-06
申请号：EP91301134.2
申请日：1991-02-12
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Harris, Jeffery Reed , Weaver, Max Allen , Moody, David Jesse
IPC分类号： C09B69/10 , C08G65/32
CPC分类号： C07D209/48 , C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/3348 , C09B69/00
摘要： The process for chemically modifying metal-free, organic material for improving one or more properties thereof such as water dispersibility, compatibility with other organics, or increased chemical reactivity, wherein the process includes providing material with from 1-6 sulfonylhalide groups or sulfonate ester groups or mixtures thereof, and contacting the material under sulfonamido forming conditions with one or more reactants containing one or more poly(oxyalkylene) moieties, each of the reactants having from 1 to 4 functional amine groups, and each of the poly(oxyalkylene) moieties being comprised of from about 4 to about 200 epoxide reactant residues at least about 50 mole percent of which residues contain 2-4 carbons.

7. 发明公开

EP0437105A1 Intermediates and colorants having primary hydroxyl enriched poly(oxyalkylene) moieties and their preparation 失效
标题翻译： Zwischenproduckte和具有增加的伯羟基基团的聚（氧化烯）基团和其制备的染料。
公开(公告)号：EP0437105A1
公开(公告)日：1991-07-17
申请号：EP90314335.2
申请日：1990-12-28
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Moody, David Jesse , Kluger, Edward William , Rekers, John William
IPC分类号： C09B69/10 , C08G65/28
CPC分类号： C08G65/2627 , C09B69/00
摘要： Enhanced branched chain hydroxyl compounds are provided of formula
wherein Y is the residue of an organic nucleophile, preferably an organic chromophore or an organic chromophore intermediate, and each Z is a poly(oxyalkylene) moiety having a molecular weight of from about 400-10,000 and containing at least one glycidol residue, wherein at least one of the primary oxy sites of said glycidol residue is linked preferably directly to a first epoxide residue of three or more carbons, and wherein said first epoxide residue is linked through a secondary oxy site preferably directly to a second epoxide residue having a primary terminal hydroxyl.
摘要翻译：提供增强的支链羟基化合物式Y-（Z）1-6 worin的Y是有机亲核残基，优选中间的有机发色团或有机生色的，和每个Z是具有分子聚（氧化烯）结构部分重量为约400至10.000的并含有至少一个缩水甘油残基，氧的主站点worin至少一个所述缩水甘油残基优选直接连接到三个或更多个碳原子的第一环氧化物残基，和worin所述第一环氧化物的残基是通过二次氧位点连接优选地直接到具有伯羟基端的第二环氧化物的残基。

8. 发明公开

EP0166566A2 Resin colorants and resin coloration 失效
标题翻译： Harzfarbstoffe undHarzfärbung。
公开(公告)号：EP0166566A2
公开(公告)日：1986-01-02
申请号：EP85304352.9
申请日：1985-06-18
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Moore, Patrick David
IPC分类号： C09B29/033 , C08K5/23 , C09B69/10
CPC分类号： C09B69/106 , C08G18/38 , C08G18/50 , C08K5/45 , C09B29/0059 , C08L75/04
摘要： A polyurethane resin is colored by incorporating, during production, a reactive coloring agent of the formula

wherein R 1 , R 2 and R 3 are each hydrogen or a substituent, e.g. a carbonyl-containing group, and A is an organic dyestuff coupler. The agents are novel when A is 4-aminophenyl and the amine carries two substituents independently selected from polyalkylene oxide radicals, radicals of copolymers of polyalkylene oxides, and radicals of hydroxyalkylenes.
摘要翻译：聚氨酯树脂通过在制备过程中引入式（CHEM）的反应性着色剂而着色，其中R 1，R 2和R 3各自为氢或取代基。含羰基，A是有机染料偶合剂。当A是4-氨基苯基时，这些试剂是新的，并且胺载有独立地选自聚环氧烷基，聚环氧烷共聚物的基团和羟基亚烷基的两个取代基。

9. 发明公开

EP0074707A2 Polyamines and their use as curing agents 失效
标题翻译：多胺和德文Verwendung alsHärter。
公开(公告)号：EP0074707A2
公开(公告)日：1983-03-23
申请号：EP82303881.5
申请日：1982-07-22
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Iyer, Venketa Subramanian
IPC分类号： C07C87/22 , C07C87/20 , C07C93/02 , C07C87/38 , C07C87/28 , C07C87/50 , C07C87/36 , C07C147/12 , C08G59/50
CPC分类号： C08G59/504 , C08G59/50 , C08G65/322 , C08G65/33379
摘要： A polyamine of the formula
wherein R, is H or C 1-\12 alkyl;

R 2 and R 3 are independently selected from H and C 1-8 alkyl;
R 4 is H or

R s is a radical having a valency of n and which is the radical of a C 5-30 alkane, a C 12-30 aromatic compound or C 5-60 cycloalkane or is derived from an amine-terminated polygycol having a molecular weight of from 100 to 6,000 and from 2 to 100 ether linkages; and
n is an integer of from 2 to 15.
These compounds can be used as curing agents for epoxy resins. They can be prepared by reduction of novel nitro analogues, themselves prepared from a nitroalkane, an aldehyde and a polyamine.
摘要翻译：一种式...的多胺...其中R 1是H或C 1-12烷基; R 2和R 3独立地选自H和C 1-8烷基; R 4是H或...。 n价的化合价，其为C5-30烷烃，C12-30芳族化合物或C5-60环烷烃的基团，或衍生自分子量为100至6000和2至100的胺封端的多羟基化合物醚键; 和... n是2〜15的整数。这些化合物可以用作环氧树脂的固化剂。它们可以通过还原由硝基烷烃，醛和多胺制备的新型硝基类似物来制备。

10. 发明授权

EP0445926B1 Organic materials having sulfonamido linked poly(oxyalkylene) moieties and their preparation 失效
标题翻译：穿其中sulfonamidogebundene聚（氧化烯）的有机材料基团和它们的制备
公开(公告)号：EP0445926B1
公开(公告)日：1996-08-21
申请号：EP91301134.2
申请日：1991-02-12
申请人： MILLIKEN RESEARCH CORPORATION
发明人： Kluger, Edward William , Harris, Jeffery Reed , Weaver, Max Allen , Moody, David Jesse
IPC分类号： C09B69/10 , C08G65/32
CPC分类号： C07D209/48 , C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/3348 , C09B69/00

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