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1. 发明公开

EP1296894A1 ULTRASTABLE POROUS ALUMINOSILICATE STRUCTURES 审中-公开
标题翻译：超稳定的多孔铝硅酸盐结构
公开(公告)号：EP1296894A1
公开(公告)日：2003-04-02
申请号：EP01926443.1
申请日：2001-03-27
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , ZHANG, Wenzhong , LIU, Yu
IPC分类号： C01B33/26
CPC分类号： B01J29/005 , B01J29/0308 , B01J29/041 , B01J29/084 , B01J29/40 , B01J29/7007 , B01J2229/36 , B01J2229/62 , C01B33/38 , C01B39/04 , C01B39/48 , C10G11/05 , C10G47/16
摘要： Mesoporous hexagonal, cubic, lamellar, wormhole, or cellular foam aluminosilicates, gallosilicates and titanosilicates derived from protozeolitic seeds using an ionic structure directing agent are described. The silicon and aluminum, gallium or titanium centers in the structures are stable so that the framework of the structure does not collapse when heated in the presence of water or water vapor (steam). The steam stable compositions can be used as catalysts for hydrocarbon conversions, including the fluidized bed catalytic cracking and the hydrocracking of petroleum oils, and other reactions of organic compounds.

2. 发明授权

EP0484495B1 POLYOXOMETALATE INTERCALATED LAYERED DOUBLE HYDROXIDES 失效
标题翻译： LAYERS形双氢氧化物具有中间多金属氧酸盐
公开(公告)号：EP0484495B1
公开(公告)日：1997-07-09
申请号：EP91910073.5
申请日：1991-05-06
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , KWON, Taehyun , DIMOTAKIS, Emmanuel, D. , AMARASEKERA, Jayantha
IPC分类号： C01B13/14 , C01F7/00 , B01J29/04 , C01G9/00 , B01J20/02 , B01J21/16
CPC分类号： B01D53/864 , B01J20/12 , B01J23/007 , B01J29/049 , C01B13/14 , C01B13/145 , C01F7/00 , C01F7/002 , C01G9/006 , C01P2002/22 , C01P2002/72 , C01P2002/78
摘要： This disclosure describes the synthesis of layered double hydroxide compositions interlayered by polyoxometalate anions with Keggin-type structures and having the formula [M1-x''Mx'''(OH)2]Ax/nn-.yH2O, wherein, M'' is a divalent metal and M''' is a trivalent metal, A is an anionic polyoxometalate of negative charge n, x range between 0.12 to 0.8, and y is a positive number. The products exhibit well-defined XRD peaks corresponding to uniformly crystalline layered products with basal spacing values » 14 Å.

3. 发明授权

EP0486676B1 PROCESS USING SORBENTS FOR THE REMOVAL OF SOx FROM FLUE GAS AND OTHER GAS STREAMS 失效
标题翻译：除去方法SOX OFF烟气等气体的数据流通过吸附剂
公开(公告)号：EP0486676B1
公开(公告)日：1996-10-09
申请号：EP91912279.6
申请日：1991-05-28
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , AMARASEKERA, Jayantha , POLANSKY, Christine, A.
IPC分类号： B01D53/34 , B01J20/06
CPC分类号： B82Y30/00 , B01D53/508 , B01J20/06 , C01F7/002 , C01G1/00 , C01G49/009 , C01P2002/22 , C01P2002/78
摘要： A process of removing noxious sulfur oxides from gas streams using heated layered double hydroxide (LDH) sorbents is described. The sorbent compositions contain metal components incorporated into the galleries of the LDH structures in the form of metal-containing oxo-anions, to promote the oxidation of sulfur dioxide.

4. 发明授权

EP2115055B1 COMPOSITES COMPRISING POLYMER AND MESOPOROUS SILICATE 有权
标题翻译：复合有聚合物和介孔SILIKAT
公开(公告)号：EP2115055B1
公开(公告)日：2015-03-18
申请号：EP08724423.2
申请日：2008-01-07
申请人： Board of Trustees of Michigan State University
发明人： PINNAVAIA, Thomas, J. , PARK, In , XUE, Siqi
IPC分类号： C08K3/00 , C08K3/34 , C08K3/36 , C08K7/26
CPC分类号： C08K7/26 , C08K3/013 , C08K3/34 , C08K3/346 , C08K3/36
摘要： Surfactant-templated mesoporous silicates and mesoporous layered silicate clays having certain porosity parameters are used as reinforcing agents for polymers to make composites. The combination of porosity parameters that allows mesoporous silicates to be competitive with organoclays for the reinforcement of engineering polymers include an average mesopore size of at least 4 nm for surfactant-templated mesoporous silicates and least 2 nm for mesoporous layered silicate clays.

5. 发明公开

EP1159345A1 HOMOSTRUCTURED MIXED ORGANIC AND INORGANIC CATION EXCHANGED TAPERED COMPOSITIONS 审中-公开
标题翻译：混合有机，无机阳离子交换稀释HOMO结构组成
公开(公告)号：EP1159345A1
公开(公告)日：2001-12-05
申请号：EP99904475.3
申请日：1999-01-29
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , SHI, Heng-Zhen , LAN, Tie
IPC分类号： C08K7/22
摘要： Homostructured, cation exchanged, layered compositions containing mixed onium and alkali metal, alkaline earth metal, protonated hydronium ions and mixtures thereof are described. Particulate concentrates formed by intercalation of a polymer component into the galleries of the layered inorganic and organic homostructured layered cation exchange composition and to the use of the particulate concentrates for the preparation of cured polymer-inorganic nanolayer hybrid composite compositions are described. In the most preferred embodiment of the invention the layered inorganic composition is selected from the family of 2:1 layered silicate clays.

6. 发明授权

EP0491931B1 COMPOSITE CLAY MATERIALS FOR REMOVAL OF SOx FROM GAS STREAMS 失效
标题翻译：合成音脱除硫氧化物从气流中
公开(公告)号：EP0491931B1
公开(公告)日：1995-12-13
申请号：EP91913738.0
申请日：1991-05-28
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , POLANSKY, Christine, A. , AMARASEKERA, Jayantha
IPC分类号： B01J8/00 , C01B17/00 , B01J20/12 , B01D53/34 , B01J20/04
CPC分类号： B01J21/16 , B01D53/508 , B01J20/12 , B01J37/0207 , B01J37/031 , C01B33/44
摘要： A method for preparing and using compositions including a smectite clay and a base or base precursor which reacts with SOx in a hot flue gas is described. The base or base precursor is preferably the dispersed phase in the bulk phase of the clay. The compositions are heated to form the base which reacts with SOx in the flue gas.

7. 发明公开

EP2115055A2 COMPOSITES COMPRISING POLYMER AND MESOPOROUS SILICATE 有权
标题翻译：复合有聚合物和介孔SILIKAT
公开(公告)号：EP2115055A2
公开(公告)日：2009-11-11
申请号：EP08724423.2
申请日：2008-01-07
申请人： Board of Trustees of Michigan State University
发明人： PINNAVAIA, Thomas, J. , PARK, In , XUE, Siqi
IPC分类号： C08K3/00 , C08K3/34 , C08K3/36 , C08K7/26
CPC分类号： C08K7/26 , C08K3/013 , C08K3/34 , C08K3/346 , C08K3/36
摘要： Surfactant-templated mesoporous silicates and mesoporous layered silicate clays having certain porosity parameters are used as reinforcing agents for polymers to make composites. The combination of porosity parameters that allows mesoporous silicates to be competitive with organoclays for the reinforcement of engineering polymers include an average mesopore size of at least 4 nm for surfactant-templated mesoporous silicates and least 2 nm for mesoporous layered silicate clays.

8. 发明授权

EP0830314B1 POROUS INORGANIC OXIDE MATERIALS PREPARED BY NON-IONIC SURFACTANT TEMPLATING ROUTE 失效
标题翻译：制造的NOT离子TENSIDTEMPLATS多孔无机氧化物材料
公开(公告)号：EP0830314B1
公开(公告)日：2002-12-18
申请号：EP96916589.3
申请日：1996-05-24
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , BAGSHAW, Stephen A.
IPC分类号： C01B39/00
CPC分类号： C01B37/02 , C01B37/00 , C01B37/005 , C01F7/36 , C01P2002/04 , C01P2002/72 , C01P2004/62 , C01P2006/12 , C01P2006/16
摘要： A method for the preparation of new quasi-crystalline, porous inorganic oxide materials possessing uniform framework-confined mesopores in the range 2.0-10.0 nm and large elementary particle size of more than 500.0 nm. The method uses an interaction between various non-ionic polyethylene oxide based surfactants (N DEG ) and neutral inorganic oxide precursors (I DEG ) at ambient reaction temperatures. The materials formed exhibit semi-ordered arrays of well defined pores owing to the specific mechanism of self-assembly, large pore wall thicknesses of at least 2.0 nm producing highly stable materials and large particle sizes incorporating large numbers of pores. This (N DEG I DEG ) templating approach introduces several new concepts to mesostructure synthesis. The application of the low-cost, non-toxic and biodegradable surfactants and ambient reaction temperatures, introduces environmentally clean synthetic techniques to the formation of mesostructures. Recovery of the template can be achieved through solvent extraction where the solvent may be water or ethanol.

9. 发明公开

EP0484495A1 POLYOXOMETALATE INTERCALATED LAYERED DOUBLE HYDROXIDES 失效
标题翻译： LAYERS形双氢氧化物具有中间多金属氧酸盐。
公开(公告)号：EP0484495A1
公开(公告)日：1992-05-13
申请号：EP91910073.0
申请日：1991-05-06
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , KWON, Taehyun , DIMOTAKIS, Emmanuel, D. , AMARASEKERA, Jayantha
IPC分类号： B01D53 , B01J20 , B01J23 , B01J29 , C01B13 , C01F7 , C01G9
CPC分类号： B01D53/864 , B01J20/12 , B01J23/007 , B01J29/049 , C01B13/14 , C01B13/145 , C01F7/00 , C01F7/002 , C01G9/006 , C01P2002/22 , C01P2002/72 , C01P2002/78
摘要： Cette invention se rapporte à la synthèse de compositions de doubles hydroxydes en couches, dans lesquelles sont intercalés des anions de polyoxométalate présentant des structures du type Keggin et ayant la formule [M1-x''Mx'''(OH)2]Ax/nn-.yH2O, où M'' représente un métal bivalent et M''' un métal trivalent. A représente un polyoxométalate de charge négative n, x se situe entre 0,12 et 0,8, et y représente un nombre positif. Les produits présentent des crêtes XRD bien définies correspondant à des produits en couches uniformément cristallins et comprenant des valeurs d'espacement de base 14 Å.

10. 发明公开

EP0830314A1 POROUS INORGANIC OXIDE MATERIALS PREPARED BY NON-IONIC SURFACTANT TEMPLATING ROUTE 失效
标题翻译：非离子表面活性剂模板制备多孔无机氧化物材料
公开(公告)号：EP0830314A1
公开(公告)日：1998-03-25
申请号：EP96916589.0
申请日：1996-05-24
申请人： MICHIGAN STATE UNIVERSITY
发明人： PINNAVAIA, Thomas, J. , BAGSHAW, Stephen A, 801, les Hauts de Saint-Priest
IPC分类号： C01B37 , C01F7
CPC分类号： C01B37/02 , C01B37/00 , C01B37/005 , C01F7/36 , C01P2002/04 , C01P2002/72 , C01P2004/62 , C01P2006/12 , C01P2006/16
摘要： A method for the preparation of new quasi-crystalline, porous inorganic oxide materials possessing uniform framework-confined mesopores in the range 2.0-10.0 nm and large elementary particle size of more than 500.0 nm. The method uses an interaction between various non-ionic polyethylene oxide based surfactants (N°) and neutral inorganic oxide precursors (I°) at ambient reaction temperatures. The materials formed exhibit semi-ordered arrays of well defined pores owing to the specific mechanism of self-assembly, large pore wall thicknesses of at least 2.0 nm producing highly stable materials and large particle sizes incorporating large numbers of pores. This (N° I°) templating approach introduces several new concepts to mesostructure synthesis. The application of the low-cost, non-toxic and biodegradable surfactants and ambient reaction temperatures, introduces environmentally clean synthetic techniques to the formation of mesostructures. Recovery of the template can be achieved through solvent extraction where the solvent may be water or ethanol.
摘要翻译：一种制备新型准晶体多孔无机氧化物材料的方法，该材料具有2.0-10.0nm范围的均匀骨架介孔和大于500.0nm的大基本粒度。该方法在环境反应温度下使用各种基于非离子聚环氧乙烷的表面活性剂（N°）和中性无机氧化物前体（I°）之间的相互作用。由于自组装的特殊机制，形成的材料具有半有序的阵列，具有至少2.0nm的大孔壁厚度，产生高度稳定的材料和具有大量孔隙的大粒径。这种（N°I°）模板方法为介观结构合成引入了几个新概念。低成本，无毒且可生物降解的表面活性剂和环境反应温度的应用，引入了环境清洁的合成技术来形成中间结构。通过溶剂萃取可以实现模板的回收，其中溶剂可以是水或乙醇。

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