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1. 发明授权

EP0488356B1 Processes for producing graphite blocks from graphitizable organic polymers and process for carbonizing graphitizable polymer films 失效
标题翻译：一种用于生产由石墨化的有机聚合物和方法石墨块进行碳化石墨化的聚合物膜的过程
公开(公告)号：EP0488356B1
公开(公告)日：1997-03-05
申请号：EP91120496.4
申请日：1991-11-29
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , Research Development Corporation of Japan , MATSUSHITA ELECTRONIC COMPONENTS CO., LTD.
发明人： Murakami, Mutsuaki , Hoshi, Toshiharu , Watanabe, Kazuhiro , Nishiki, Naomi , Nakamura, Katsuyuki , Okada, Hisashi
IPC分类号： C04B35/524
CPC分类号： C04B35/524

2. 发明公开

EP0488356A1 Processes for producing graphite blocks from graphitizable organic polymers and process for carbonizing graphitizable polymer films 失效
标题翻译：一种用于从石墨化的有机聚合物和碳化石墨化的聚合物膜的方法生产石墨块的过程。
公开(公告)号：EP0488356A1
公开(公告)日：1992-06-03
申请号：EP91120496.4
申请日：1991-11-29
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , Research Development Corporation of Japan , MATSUSHITA ELECTRONIC COMPONENTS CO., LTD.
发明人： Murakami, Mutsuaki , Hoshi, Toshiharu , Watanabe, Kazuhiro , Nishiki, Naomi , Nakamura, Katsuyuki , Okada, Hisashi
IPC分类号： C04B35/54
CPC分类号： C04B35/524
摘要： A process for producing a graphite block from a plurality of graphitizable polymer films or a plurality of carbonaceous films separately obtained from graphitizable polymer films is described. The method comprises superposing the plurality of the graphitizable polymer films or the plurality of the carbonaceous films, and thermally treating the plurality of the graphitizable polymer films or the plurality of the carbonaceous films in a substantially compression pressure-free condition when the treating temperature is in thermal decomposition temperature range and the graphitization temperature range and under compression pressures in temperature ranges between the thermal decomposition temperature and the graphitization temperature ranges and over the graphitization temperature range. The compression pressure over the graphitization temperature range should be higher than that in the range between the thermal decomposition and graphitization temperature ranges. By this, a wrinkle-free graphite block with a good rocking characteristic is obtained.
摘要翻译：描述了一种用于制造由石墨化的聚合物薄膜或碳质薄膜从石墨化聚合物膜单独获得的多个的多个石墨块的过程。该方法包括叠加石墨的聚合物膜的多元性或碳质薄膜的多个，并且热处理该石墨化的聚合物膜在基本上压缩无压力的条件下的多个或一碳质薄膜的多元性当处理温度是在热分解温度范围和石墨化温度范围和下在热分解温度和石墨化温度范围之间以及在石墨化温度范围的温度范围内压缩压力。在石墨化的温度范围内压缩压力应比在热分解和石墨化温度范围之间的范围高。通过这种方式，具有良好的摇摆特征防皱石墨块获得。

3. 发明授权

EP0331375B1 Optical elements for radiation comprising graphite films 失效
标题翻译：射线与石墨层的光学元件。
公开(公告)号：EP0331375B1
公开(公告)日：1995-08-23
申请号：EP89301868.9
申请日：1989-02-24
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , Research Development Corporation of Japan
发明人： Watanabe, Kazuhiro , Murakami, Mutsuaki , Yoshimura, Susumu
IPC分类号： G02B1/10 , G02B1/02
CPC分类号： B82Y10/00 , G21K1/062 , G21K2201/061 , G21K2201/064 , G21K2201/067 , G21K2201/068

4. 发明授权

EP0223047B1 Graphite intercalation compound film and method of preparing the same 失效
标题翻译：石墨介质复合膜及其制备方法
公开(公告)号：EP0223047B1
公开(公告)日：1991-01-23
申请号：EP86114008.5
申请日：1986-10-09
申请人： Research Development Corporation of Japan , MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD.
发明人： Murakami, Mutsuaki , Watanabe, Kazuhiro , Yoshimura, Susumu
IPC分类号： C01B31/00
CPC分类号： C01B32/22 , Y10T428/30

5. 发明授权

EP0305197B1 Method for making a graphite film or sheet and radiation optical elements using the graphite sheet 失效
标题翻译：使用石墨片制造石墨薄膜或薄片和辐射光学元件的方法
公开(公告)号：EP0305197B1
公开(公告)日：1992-06-03
申请号：EP88307924.6
申请日：1988-08-26
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , RESEARCH DEVELOPMENT CORPORATION OF JAPAN
发明人： Murakami, Mutsuaki , Nishiki, Naomi , Yoshimura, Yokohama , Watanabe, Kazuhiro
IPC分类号： C04B35/54 , B32B27/08 , C01B31/04 , G02B1/10
CPC分类号： C04B35/524

6. 发明公开

EP0223047A2 Graphite intercalation compound film and method of preparing the same 失效
标题翻译：其制备石墨层间化合物和方法的膜。
公开(公告)号：EP0223047A2
公开(公告)日：1987-05-27
申请号：EP86114008.5
申请日：1986-10-09
申请人： Research Development Corporation of Japan , MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD.
发明人： Murakami, Mutsuaki , Watanabe, Kazuhiro , Yoshimura, Susumu
IPC分类号： C01B31/00
CPC分类号： C01B32/22 , Y10T428/30
摘要： This invention relates to a graphite intercalation compound in the form of a film, which is obtained by intercalating a donor type, an acceptor type or a covalent type material between the layers of graphite film obtained by thermal treatment of poly(phenylene oxadiazole). The obtained intercalated graphite film has a large scale area and has an extremely improved stability compared with known graphite intercalation compounds.

7. 发明公开

EP0331375A2 Optical elements for radiation comprising graphite films 失效
标题翻译： Strahlenoptische Elemente mit Graphit-Schichten。
公开(公告)号：EP0331375A2
公开(公告)日：1989-09-06
申请号：EP89301868.9
申请日：1989-02-24
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , Research Development Corporation of Japan
发明人： Watanabe, Kazuhiro , Murakami, Mutsuaki , Yoshimura, Susumu
IPC分类号： G02B1/10 , G02B1/02
CPC分类号： B82Y10/00 , G21K1/062 , G21K2201/061 , G21K2201/064 , G21K2201/067 , G21K2201/068
摘要： This invention relates to optical elements for radiation which comprises a graphite film obtained from a film of a polymer such as polyphenylene oxadiazole, polybenzothiazole, polybenzobisthiazole, polybenzooxazole, polybenzobisoxazole, polypyromellitimide, polyphenylene isophthalamide, polyphenylene benzoimidazole, polyphenylene benzobisimidazole, polythiazole or poly-p-phenylene-vinylene The graphite film is obtained by pyrolysis of the polymer film at 2800°C or higher at a pressure of not lower than 4 kg/cm² in vacuum or in an inert gas. Alternatively, the element may be made of a graphite film obtained from the polymers mentioned above and intercalated with a metal halide. The intercalated films are readily bonded by pressing in the form of a thick sheet or block. Still alternatively, the graphite films and the intercalated films may be superposed alternately and bonded by pressing, or the intercalated films may be sandwiched between the graphite films and bonded together to form a thick sheet or block. The optical element has application as a lens, monochromater, filter or analyzer for radiations
摘要翻译：本发明涉及用于辐射的光学元件，其包括由聚苯乙烯恶二唑，聚苯并噻唑，聚苯并双噻唑，聚苯并恶唑，聚苯并双恶唑，聚吡喃单酰亚胺，聚苯撑间苯二甲酰胺，聚苯并咪唑，聚苯撑苯并咪唑，聚噻唑或聚对苯二甲酸，亚苯基亚乙烯通过聚合物膜在2800℃或更高的压力下在真空或惰性气体中以4kg / cm 2以上的压力进行热分解，得到石墨膜。或者，元件可以由由上述聚合物获得的石墨膜制成，并插入金属卤化物。嵌入的膜通过以厚片或块的形式压制而容易地粘合。或者，石墨膜和嵌入的膜可以交替叠置并通过压制结合，或者插入的膜可以夹在石墨膜之间并结合在一起以形成厚的片或块。光学元件作为透镜，单色仪，过滤器或辐射分析仪具有应用

8. 发明公开

EP0305197A2 Method for making a graphite film or sheet and radiation optical elements using the graphite sheet 失效
标题翻译：一种用于生产石墨膜或片材和在其中使用的石墨片的辐射的光学装置的过程。
公开(公告)号：EP0305197A2
公开(公告)日：1989-03-01
申请号：EP88307924.6
申请日：1988-08-26
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , RESEARCH DEVELOPMENT CORPORATION OF JAPAN
发明人： Murakami, Mutsuaki , Nishiki, Naomi , Yoshimura, Yokohama , Watanabe, Kazuhiro
IPC分类号： C04B35/54 , B32B27/08 , C01B31/04 , G02B1/10
CPC分类号： C04B35/524
摘要： This invention relates to a method for making a graphite sheet or block which comprises hot pressing at least two films of a polymer selected from a polyoxadiazole, an aromatic polyamide and an aromatic polyimide at a pressure not lower than 0.4 MPa (4 kg/cm²) at temperatures not lower than 2200°C. Alternatively, the at least two films may be thermally treated at temperatures of not lower than 2200°C and subsequently hot pressed at a pressure of not lower than 0.4 MPa (4 kg/cm²) at a temperature of not lower than 2000°C when the at least two films are made of the polyoxidiazole or aromatic polyamide or at a temperature of not lower than 1600°C when the at least two films are made of the aromatic polyimide.
摘要翻译：本发明涉及的方法用于制造石墨片或块，其包括热在不低于0.4兆帕的压力下压制从聚恶二唑上的芳族聚酰胺和芳族聚酰亚胺中选择的聚合物的至少两个膜（4千克/厘米< 2>）在温度不低于2200℃或者，所述至少两个膜可被热在不低于2200℃的温度下处理，随后热压在不低于0.4兆帕的压力下（4千克/平方厘米 <2>在不低于2000℃的温度）当所述至少两个膜由在不低于1600℃的温度下polyoxidiazole或芳族聚酰胺的或当所述至少两个膜由芳族化合物的聚酰亚胺。

9. 发明公开

EP0331375A3 Optical elements for radiation comprising graphite films 失效
标题翻译：用于辐射包含石墨膜的光学元件
公开(公告)号：EP0331375A3
公开(公告)日：1991-04-03
申请号：EP89301868.9
申请日：1989-02-24
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , Research Development Corporation of Japan
发明人： Watanabe, Kazuhiro , Murakami, Mutsuaki , Yoshimura, Susumu
IPC分类号： G02B1/10 , G02B1/02
CPC分类号： B82Y10/00 , G21K1/062 , G21K2201/061 , G21K2201/064 , G21K2201/067 , G21K2201/068
摘要： This invention relates to optical elements for radiation which comprises a graphite film obtained from a film of a polymer such as polyphenylene oxadiazole, polybenzothiazole, polybenzobisthiazole, polybenzooxazole, polybenzobisoxazole, polypyromellitimide, polyphenylene isophthalamide, polyphenylene benzoimidazole, polyphenylene benzobisimidazole, polythiazole or poly-p-phenylene-vinylene The graphite film is obtained by pyrolysis of the polymer film at 2800°C or higher at a pressure of not lower than 4 kg/cm² in vacuum or in an inert gas. Alternatively, the element may be made of a graphite film obtained from the polymers mentioned above and intercalated with a metal halide. The intercalated films are readily bonded by pressing in the form of a thick sheet or block. Still alternatively, the graphite films and the intercalated films may be superposed alternately and bonded by pressing, or the intercalated films may be sandwiched between the graphite films and bonded together to form a thick sheet or block. The optical element has application as a lens, monochromater, filter or analyzer for radiations

10. 发明公开

EP0305197A3 Method for making a graphite film or sheet and radiation optical elements using the graphite sheet 失效
标题翻译：使用石墨片制造石墨薄膜或薄片和辐射光学元件的方法
公开(公告)号：EP0305197A3
公开(公告)日：1990-07-11
申请号：EP88307924.6
申请日：1988-08-26
申请人： MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD. , RESEARCH DEVELOPMENT CORPORATION OF JAPAN
发明人： Murakami, Mutsuaki , Nishiki, Naomi , Yoshimura, Yokohama , Watanabe, Kazuhiro
IPC分类号： C04B35/54 , B32B27/08 , C01B31/04 , G02B1/10
CPC分类号： C04B35/524
摘要： This invention relates to a method for making a graphite sheet or block which comprises hot pressing at least two films of a polymer selected from a polyoxadiazole, an aromatic polyamide and an aromatic polyimide at a pressure not lower than 0.4 MPa (4 kg/cm²) at temperatures not lower than 2200°C. Alternatively, the at least two films may be thermally treated at temperatures of not lower than 2200°C and subsequently hot pressed at a pressure of not lower than 0.4 MPa (4 kg/cm²) at a temperature of not lower than 2000°C when the at least two films are made of the polyoxidiazole or aromatic polyamide or at a temperature of not lower than 1600°C when the at least two films are made of the aromatic polyimide.

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