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1. 发明公开

EP0337103A2 Biocidal composition 失效
标题翻译： Biozide Zusammensetzung。
公开(公告)号：EP0337103A2
公开(公告)日：1989-10-18
申请号：EP89103887.9
申请日：1989-03-06
申请人： ISHIHARA SANGYO KAISHA, Ltd.
发明人： Nasu, Rikuo , Komyoji, Terumasa , Nakajima, Toshio , Suzuki, Kazumi , Ito, Keiichiro , Ohshima, Takeshi , Yoshimura, Hideshi
IPC分类号： A01N43/50 , A01N59/20 , A01N57/12 , A01N55/00 , A01N53/00 , A01N47/38 , A01N47/34 , A01N47/14 , A01N47/04 , A01N43/90 , A01N43/80
CPC分类号： C07D233/90 , A01N43/50 , A01N63/04 , A01N59/20 , A01N57/12 , A01N55/00 , A01N53/00 , A01N47/38 , A01N47/34 , A01N47/14 , A01N47/04 , A01N43/90 , A01N43/80 , A01N43/653 , A01N43/40 , A01N37/36 , A01N37/34 , A01N37/24 , A01N2300/00
摘要： A biocidal composition containing, as active ingredients, at least one imidazole compound represented by formula (I):
wherein R¹ represents a phenyl group, a halogen-substituted phenyl group, an alkyl group, or a halogen-substituted alkyl group; and R² represents a halogen atom,
and at least one other specific compound. The combination of the compound represented by formula (I) and other specific compound can produce an unexpected effect in amount required and biocidal spectrum.
摘要翻译：一种杀生物组合物，其含有作为活性成分的至少一种由式（I）表示的咪唑化合物：其中R 1表示苯基，卤素取代的苯基，烷基或卤素取代的烷基; 和R 2表示卤素原子，和至少一种其它特定化合物。由式（I）表示的化合物与其他特定化合物的组合可以产生预期的效果，并且具有杀菌谱。

2. 发明公开

EP0009212A1 Process for producing 2-chloro-5-trichloromethylpyridine 失效
标题翻译：一种用于2-氯-5-三氯甲基吡啶的制备方法。
公开(公告)号：EP0009212A1
公开(公告)日：1980-04-02
申请号：EP79103431.7
申请日：1979-09-13
申请人： ISHIHARA SANGYO KAISHA LTD.
发明人： Nishiyama, Ryuzo , Fujikawa, Kanichi , Yokomichi, Isao , Nasu, Rikuo , Awazu, Takao , Kawashima, Junichi
IPC分类号： C07D213/61 , C07B9/00
CPC分类号： C07D213/61
摘要： 2-Chloro-5-trichloromethylpyridine of the formula (I):
is produced in high yield by reacting β-picoline of the formula (II):
with chlorine in a gaseous phase at 300 to 500°C, e.g. 330 to 470°C, in a residence time of 0,5 to 60 seconds, in the presence of an inert diluent of nitrogen, a halogenated methane, a halogenated ethane, a halogenated ethylene or a mixture thereof.
2-Chloro-5-trichlormonomethylpyridine is useful as an intermediate for medicines, agricultural chemicals, dyes, especially herbicides.

3. 发明公开

EP0137424A3 Process for producing 2,4-dichlorobenzotrifluoride 失效
标题翻译：生产2,4-二氯苯并呋喃的方法
公开(公告)号：EP0137424A3
公开(公告)日：1985-06-12
申请号：EP84111575
申请日：1984-09-27
申请人： ISHIHARA SANGYO KAISHA, LTD.
发明人： Nasu, Rikuo , Shigehara, Itaru , Kawashima, Junichi , Maeda, Masaru
IPC分类号： C07C25/13 , C07C17/32
CPC分类号： C07C17/32 , C07C25/13
摘要： A process for producing 2,4-dichlorobenzotrifluoride, which comprises reacting m-dichlorobenzene with a halogenated methane of the formula CF x Cl 4-x where x is 0, 1 or 2, and hydrogen fluoride at a temperature of from 80 to 180°C in the presence of a catalyst of at least one member selected from the group consisting of fluorides of antimony, boron, titanium, tantalum and niobium.
摘要翻译：一种2,4-二氯三氟甲苯的制备方法，其包括使间二氯苯与式为CF xCl 4-x的卤代甲烷（其中x为0,1或2）和氟化氢在80-180℃的温度下反应存在选自锑，硼，钛，钽和铌的氟化物中的至少一种的催化剂。

4. 发明公开

EP0137424A2 Process for producing 2,4-dichlorobenzotrifluoride 失效
标题翻译： Verfahren zur Herstellung von 2,4-二氯苯氟。
公开(公告)号：EP0137424A2
公开(公告)日：1985-04-17
申请号：EP84111575.1
申请日：1984-09-27
申请人： ISHIHARA SANGYO KAISHA, LTD.
发明人： Nasu, Rikuo , Shigehara, Itaru , Kawashima, Junichi , Maeda, Masaru
IPC分类号： C07C25/13 , C07C17/32
CPC分类号： C07C17/32 , C07C25/13
摘要： A process for producing 2,4-dichlorobenzotrifluoride, which comprises reacting m-dichlorobenzene with a halogenated methane of the formula CF x Cl 4-x where x is 0, 1 or 2, and hydrogen fluoride at a temperature of from 80 to 180°C in the presence of a catalyst of at least one member selected from the group consisting of fluorides of antimony, boron, titanium, tantalum and niobium.
摘要翻译：一种2,4-二氯三氟甲苯的制备方法，其包括使间二氯苯与式为CF xCl 4-x的卤代甲烷（其中x为0,1或2）和氟化氢在80-180℃的温度下反应存在选自锑，硼，钛，钽和铌的氟化物中的至少一种的催化剂。

5. 发明授权

EP0009212B1 Process for producing 2-chloro-5-trichloromethylpyridine 失效
标题翻译：二氯-5-三氯甲基吡啶的制备方法
公开(公告)号：EP0009212B1
公开(公告)日：1984-02-08
申请号：EP79103431.7
申请日：1979-09-13
申请人： ISHIHARA SANGYO KAISHA LTD.
发明人： Nishiyama, Ryuzo , Fujikawa, Kanichi , Yokomichi, Isao , Nasu, Rikuo , Awazu, Takao , Kawashima, Junichi
IPC分类号： C07D213/61 , C07B9/00
CPC分类号： C07D213/61

6. 发明授权

EP0497213B1 Process for producing 3,5-difluoroaniline 失效
标题翻译：一种用于3,5-二氟苯胺的制备方法。
公开(公告)号：EP0497213B1
公开(公告)日：1995-09-27
申请号：EP92101099.7
申请日：1992-01-23
申请人： ISHIHARA SANGYO KAISHA, LTD.
发明人： Nasu, Rikuo , Hamaguchi, Motohiko
IPC分类号： C07C209/68 , C07C209/74 , C07C211/52
CPC分类号： C07C209/74 , C07C209/68

7. 发明授权

EP0337103B1 Biocidal composition 失效
标题翻译：生物组成
公开(公告)号：EP0337103B1
公开(公告)日：1993-02-10
申请号：EP89103887.9
申请日：1989-03-06
申请人： ISHIHARA SANGYO KAISHA, Ltd.
发明人： Nasu, Rikuo , Komyoji, Terumasa , Nakajima, Toshio , Suzuki, Kazumi , Ito, Keiichiro , Ohshima, Takeshi , Yoshimura, Hideshi
IPC分类号： A01N43/50 , A01N59/20 , A01N57/12 , A01N55/00 , A01N53/00 , A01N47/38 , A01N47/34 , A01N47/14 , A01N47/04 , A01N43/90 , A01N43/80
CPC分类号： C07D233/90 , A01N43/50 , A01N63/04 , A01N59/20 , A01N57/12 , A01N55/00 , A01N53/00 , A01N47/38 , A01N47/34 , A01N47/14 , A01N47/04 , A01N43/90 , A01N43/80 , A01N43/653 , A01N43/40 , A01N37/36 , A01N37/34 , A01N37/24 , A01N2300/00

8. 发明公开

EP0497213A3 Process for producing 3,5-difluoroaniline 失效
标题翻译：生产3,5-二氟苯胺的方法
公开(公告)号：EP0497213A3
公开(公告)日：1993-01-20
申请号：EP92101099.7
申请日：1992-01-23
申请人： ISHIHARA SANGYO KAISHA, LTD.
发明人： Nasu, Rikuo , Hamaguchi, Motohiko
IPC分类号： C07C209/68 , C07C209/74 , C07C211/52
CPC分类号： C07C209/74 , C07C209/68
摘要： A process for producing 3,5-difluoroaniline, which comprises reacting a benzonitrile compound of the formula (I):

wherein each of Xi, X 2 and X 3 is hydrogen, chlorine, bromine or a cyano group, provided that at least one of X 1 to X 3 is a cyano group, with a mineral acid for hydrolysis and decarboxylation to obtain an aniline compound of the formula (II):
wherein each of X 4 , X 5 and X 6 is hydrogen, chlorine or bromine, provided that at least one of X 4 to X 6 is hydrogen, and in the case of a compound of the formula (II) wherein X 4 , X 5 and X 6 are not simultaneously hydrogen, reacting such a compound with hydrogen in a presence of a catalyst for reduction to obtain 3,5-difluoroaniline.

9. 发明公开

EP0497213A2 Process for producing 3,5-difluoroaniline 失效
标题翻译： Verfahren zur Herstellung von 3,5-difluoro Anilin。
公开(公告)号：EP0497213A2
公开(公告)日：1992-08-05
申请号：EP92101099.7
申请日：1992-01-23
申请人： ISHIHARA SANGYO KAISHA, LTD.
发明人： Nasu, Rikuo , Hamaguchi, Motohiko
IPC分类号： C07C209/68 , C07C209/74 , C07C211/52
CPC分类号： C07C209/74 , C07C209/68
摘要： A process for producing 3,5-difluoroaniline, which comprises reacting a benzonitrile compound of the formula (I):

wherein each of Xi, X 2 and X 3 is hydrogen, chlorine, bromine or a cyano group, provided that at least one of X 1 to X 3 is a cyano group, with a mineral acid for hydrolysis and decarboxylation to obtain an aniline compound of the formula (II):

wherein each of X 4 , X 5 and X 6 is hydrogen, chlorine or bromine, provided that at least one of X 4 to X 6 is hydrogen, and in the case of a compound of the formula (II) wherein X 4 , X 5 and X 6 are not simultaneously hydrogen, reacting such a compound with hydrogen in a presence of a catalyst for reduction to obtain 3,5-difluoroaniline.
摘要翻译：一种制备3,5-二氟苯胺的方法，其包括使式（I）的苄腈化合物：其中X1，X2和X3各自为氢，氯，溴或氰基，其中至少一个 X 1〜X 3为氰基，与无机酸进行水解和脱羧反应，得到式（II）的苯胺化合物：其中X 4，X 5和X 6各自为氢，氯或溴，条件是在 X 4〜X 6中的至少一个为氢，在X 4，X 5，X 6不同时为氢的式（II）化合物的情况下，在还原用催化剂的存在下使该化合物与氢反应，得到3 ，5-二氟苯胺。

10. 发明公开

EP0337103A3 Biocidal composition 失效
标题翻译：生物组成
公开(公告)号：EP0337103A3
公开(公告)日：1990-01-17
申请号：EP89103887.9
申请日：1989-03-06
申请人： ISHIHARA SANGYO KAISHA, Ltd.
发明人： Nasu, Rikuo , Komyoji, Terumasa , Nakajima, Toshio , Suzuki, Kazumi , Ito, Keiichiro , Ohshima, Takeshi , Yoshimura, Hideshi
IPC分类号： A01N43/50 , A01N59/20 , A01N57/12 , A01N55/00 , A01N53/00 , A01N47/38 , A01N47/34 , A01N47/14 , A01N47/04 , A01N43/90 , A01N43/80
CPC分类号： C07D233/90 , A01N43/50 , A01N63/04 , A01N59/20 , A01N57/12 , A01N55/00 , A01N53/00 , A01N47/38 , A01N47/34 , A01N47/14 , A01N47/04 , A01N43/90 , A01N43/80 , A01N43/653 , A01N43/40 , A01N37/36 , A01N37/34 , A01N37/24 , A01N2300/00
摘要： A biocidal composition containing, as active ingredients, at least one imidazole compound represented by formula (I):
wherein R¹ represents a phenyl group, a halogen-substituted phenyl group, an alkyl group, or a halogen-substituted alkyl group; and R² represents a halogen atom,
and at least one other specific compound. The combination of the compound represented by formula (I) and other specific compound can produce an unexpected effect in amount required and biocidal spectrum.

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