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1. 发明公开

EP3294697A1 PROCESS FOR MAKING HCFO-1233zd 有权
公开(公告)号：EP3294697A1
公开(公告)日：2018-03-21
申请号：EP16793142
申请日：2016-04-25
申请人： HONEYWELL INT INC
发明人： WANG HAIYOU , TUNG HSUEH SUNG , COTTRELL STEPHEN A
IPC分类号： C07C17/25 , C07C17/42 , C07C19/10
CPC分类号： C07C17/25 , C07C21/18
摘要： Disclosed is a process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) which includes reacting a propane feedstock comprising tetrachlorofluoropropanes, trichlorodifluoropropanes, dichlorotrifluoropropanes, or a mixture thereof, in the presence of a solid catalyst. The process generally comprises the following four steps: (i) providing a propane feedstock comprising trichlorodifluoropropanes and dichlorotrifluoropropanes, (ii) reacting the feedstock in a vapor phase reactor in the presence of HF and in the presence of a solid catalyst under conditions effective to form a product stream comprising HCFO-1233zd and unconverted starting materials, (iii) recovering or removing HCl and HF, and (iv) isolating HCFO-1233zd(E), HCFO-1233zd(Z), or both.

2. 发明公开

EP2970741A4 AZEOTROPIC COMPOSITIONS OF 1,3,3-TRICHLORO-1,1-DIFLUOROPROPANE AND HYDROGEN FLUORIDE 审中-实审
标题翻译：作者：1,3,3四氯-1,1- FLUOR丙烷和氢氟酸的共沸混合物
公开(公告)号：EP2970741A4
公开(公告)日：2016-11-02
申请号：EP14778275
申请日：2014-03-05
申请人： HONEYWELL INT INC
发明人： MERKEL DANIEL C , POKROVSKI KONSTANTIN A , TUNG HSUEH SUNG , WANG HAIYOU , COTTRELL STEPHEN A , PHAM HANG T
IPC分类号： C09K5/04 , C07C19/08 , C11D7/08 , C11D7/50 , C23G5/028
CPC分类号： C07C19/10 , C09K5/044 , C11D7/08 , C11D7/5036 , C23G5/02809
摘要： Provided are azeotropic or azeotrope-like mixtures of 1,3,3-trichloro-1,1-difluoro-propane (HCFC-242fa) and hydrogen fluoride. Such compositions are useful as a feed stock or intermediate in the production of HFC-245fa and HCFO-1233zd.

3. 发明公开

EP2709970A4 INTEGRATED PROCESS FOR THE PRODUCTION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE 审中-公开
标题翻译：集成方法1-氯-3,3,3-三氟丙烯
公开(公告)号：EP2709970A4
公开(公告)日：2014-10-29
申请号：EP12786229
申请日：2012-05-17
申请人： HONEYWELL INT INC
发明人： COTTRELL STEPHEN A , TUNG HSUEH SUNG , POKROVSKI KONSTANTIN A
IPC分类号： C07C17/25 , C07C17/383 , C07C21/18
CPC分类号： C07C17/383 , C07C17/206 , C07C17/25 , C07C17/38 , C07C21/18 , Y02P20/125

4. 发明公开

EP2440318A4 MULTI-STAGE MULTI-TUBE SHELL-AND-TUBE REACTOR 审中-公开
标题翻译：多级更多PIPE管式反应器
公开(公告)号：EP2440318A4
公开(公告)日：2016-10-05
申请号：EP10786590
申请日：2010-06-03
申请人： HONEYWELL INT INC
发明人： CHIU YUON , COTTRELL STEPHEN A , HORWATH RICHARD DURICK , KOPKALLI HALUK
IPC分类号： B01J8/06 , F28D7/16 , F28F9/02
CPC分类号： F28D7/1638 , B01J8/067 , B01J2208/00221 , B01J2208/0023 , F28F9/0202 , F28F9/0265 , F28F2009/226 , F28F2210/08
摘要： A multi-stage, multi-tube, shell-and-tube reactor which contains reaction zones and interstage temperature control (cooling/heating) zones in series. The reactor has at least two types of zones which both contribute to removing or supplying heat to the system depending on the system's need. The reactor will have a group of reaction zones which contain tubes packed with catalyst to progress the reaction and remove or supply heat simultaneously. There are also a number of interstage temperature control (cooling/heating) zones which are designed to supply or remove heat to or from the system. The positioning, number, and design of the zones will depend on the amount of temperature control desired and exothermic or endothermic nature of the processes to be conducted in the reactor.

5. 发明公开

EP2892644A4 REACTOR AND AGITATOR USEFUL IN A PROCESS FOR MAKING 1-CHLORO-3,3,3-TRIFLUOROPROPENE 审中-公开
标题翻译：反应器和混频器FOR USE IN一种生产1-氯3,3,3-三氟丙烯
公开(公告)号：EP2892644A4
公开(公告)日：2016-07-20
申请号：EP13834867
申请日：2013-08-29
申请人： HONEYWELL INT INC
发明人： COTTRELL STEPHEN A
IPC分类号： B01J19/18 , C07C17/20 , C07C21/18 , F16J15/00 , F16J15/32 , F16J15/3212 , F16J15/3284
CPC分类号： B01J19/02 , B01F7/00033 , B01J3/08 , B01J19/006 , B01J19/0066 , B01J19/0073 , B01J19/18 , B01J19/26 , B01J2219/00006 , B01J2219/0004 , B01J2219/00094 , B01J2219/00123 , B01J2219/00162 , B01J2219/0218 , B01J2219/0263 , B01J2219/0277 , C07C17/093 , C07C17/25 , C07C17/38 , C07C17/383 , C07C21/185 , Y02P20/149 , C07C21/18
摘要： Disclosed is a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.

6. 发明公开

EP2814795A4 PROCESS FOR THE PRODUCTION OF HCFC-1233zd 有权转让
标题翻译： VERFAHREN ZUR HERSTELLUNG VON HCFC-1233ZD
公开(公告)号：EP2814795A4
公开(公告)日：2015-09-30
申请号：EP13748643
申请日：2013-02-11
申请人： HONEYWELL INT INC
发明人： COTTRELL STEPHEN A , TUNG HSUEH SUNG , POKROVSKI KONSTANTIN A , WANG HAIYOU , MERKEL DANIEL C
IPC分类号： C07C17/20 , C07B61/00 , C07C21/18
CPC分类号： C07C17/23 , C07C17/20 , C07C17/206 , C07C17/25 , C07C17/38 , C07C17/383 , C07C21/18
摘要： A process for the manufacture of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) at commercial scale from the reaction of HCC-240 and HF is disclosed. In one embodiment, HCC-240fa and HF are fed to a reactor operating at high pressure. Several different reactor designs useful in this process include; a stirred-tank reactor (batch and/or continuous flow); a plug flow reactor; a static mixer used as a reactor; at least one of the above reactors operating at high pressure; optionally combined with a distillation column running at a lower pressure; and combinations of the above; and/or with a distillation column. The resulting product stream consisting of 1233zd, HCl, HF, and other byproducts is partially condensed to recover HF by phase separation. The recovered HF phase is recycled to the reactor. The HCl is scrubbed from the vapor stream and recovered as an aqueous solution. The remaining organic components including the desired HCFC-1233zd are scrubbed, dried and distilled to meet commercial product specifications.
摘要翻译：公开了从HCC-240和HF的反应制备商业规模的1-氯-3,3,3-三氟丙烯（HCFC-1233zd）的方法。在一个实施方案中，将HCC-240fa和HF加入到在高压下操作的反应器中。在这个过程中有用的几种不同的反应器设计包括：搅拌釜反应器（批次和/或连续流动）; 活塞流反应器; 用作反应器的静态混合器; 上述反应器中的至少一个在高压下运行; 任选地与在较低压力下运行的蒸馏塔组合; 和上述的组合; 和/或用蒸馏塔。由1233zd，HCl，HF和其他副产物组成的产物流部分冷凝，通过相分离回收HF。将回收的HF相再循环到反应器中。将HCl从蒸汽流中洗涤并作为水溶液回收。将包含所需HCFC-1233zd的剩余有机组分进行洗涤，干燥和蒸馏以满足商业产品规格。

7. 发明公开

EP2406177A4 METHODS AND REACTOR DESIGNS FOR PRODUCING PHOSPHORUS PENTAFLUORIDE 审中-公开
标题翻译：方法和反应器设计用于生产磷五氟化
公开(公告)号：EP2406177A4
公开(公告)日：2013-05-08
申请号：EP10751458
申请日：2010-03-12
申请人： HONEYWELL INT INC
发明人： LULY MATTHEW H , SMITH ROBERT A , NAIR HARIDASAN K , DEPRATO PHILIP , POKROVSKI KONSTANTIN A , MERKEL DANIEL C , UHRICH KEVIN , COTTRELL STEPHEN A , BRENNER DANIEL J
IPC分类号： C01B25/10 , B01J12/00 , B01J19/26 , C01B9/08 , C01B25/455
CPC分类号： C01B25/10 , B01J4/002 , B01J12/00 , B01J19/24 , C01B25/455

8. 发明公开

EP3294698A1 INTEGRATED PROCESS FOR MAKING HCFO-1233zd AND HFC-245fa 审中-公开
公开(公告)号：EP3294698A1
公开(公告)日：2018-03-21
申请号：EP16793144
申请日：2016-04-25
申请人： HONEYWELL INT INC
发明人： COTTRELL STEPHEN A , CERRI GUSTAVO , CHIU YUON , MCCLAINE JENNIFER W
IPC分类号： C07C17/42 , C07C17/25 , C07C19/10
CPC分类号： C07C17/21 , C07C17/208 , Y02P20/125 , C07C19/08
摘要： A process is described wherein otherwise unusable by-products from a process for the manufacture of trans HCFO-1233zd(E) are converted to a valuable product by introducing them into a process for the production of HFC-245fa. The process includes the catalytic hydrofluorination of a reaction mixture comprising the HCFO-1233zd production by-products.

9. 发明公开

EP2951140A4 PROCESS FOR THE PREPARATION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE USING A PHASE TRANSFER CATALYST 有权转让
标题翻译：工艺生产1-氯3,3,3-三氟使用相转移催化剂
公开(公告)号：EP2951140A4
公开(公告)日：2016-09-28
申请号：EP14746002
申请日：2014-02-03
申请人： HONEYWELL INT INC
发明人： TUNG HSUEH SUNG , WANG HAIYOU , MERKEL DANIEL C , COTTRELL STEPHEN A , POKROVSKI KONSTANTIN A , SHANKLAND IAN
IPC分类号： C07C17/25 , C07C17/35 , C07C21/18
CPC分类号： C07C17/204 , C07C17/206 , C07C17/21 , C07C17/25 , C07C21/18
摘要： Disclosed is a process in which the fluorination of an organic reactant comprising 1,1,1,3,3-pentachloropropane (240fa) with anhydrous HF is conducted in the presence of an effective amount of a phase-transfer catalyst which facilitates the reaction between these incompatible reaction components to produce 1-chloro-3,3,3-trifluoro-propene (1233zd). Other organic reactant materials include 1,1,3,3-tetrachloropropene (HCO-1230za), 1,3,3,3-tetrachloropropene (HCO-1230zd), and various mixtures with or without 240fa.

10. 发明公开

EP2665696A4 METHODS OF MAKING 2,3,3,3-TETRAFLUORO-2-PROPENE 有权
标题翻译：用于生产2,3,3,3-四氟-2-丙烯
公开(公告)号：EP2665696A4
公开(公告)日：2015-12-23
申请号：EP12737145
申请日：2012-01-13
申请人： HONEYWELL INT INC
发明人： COTTRELL STEPHEN A , CHIU YUON , TUNG HSUEH SUNG , UHRICH KEVIN D , SCHEIDLE PETER , KOPKALLI HALUK
IPC分类号： C07C17/25 , B01J23/18 , C07C17/087 , C07C17/21 , C07C17/38 , C07C21/18
CPC分类号： C07C17/21 , C07C17/087 , C07C17/206 , C07C17/25 , C07C17/38 , C07C17/383 , C07C19/10 , C07C21/18
摘要： wherein the HC1 generated during these steps is scrubbed with water to form an acid solution and the organic components are scrubbed with a caustic solution and then dried before further processing.

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