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1. 发明授权

EP3303530B1 A PROCESS FOR REFINING GLYCERIDE OIL COMPRISING A BASIC QUATERNARY AMMONIUM SALT TREATMENT 有权
公开(公告)号：EP3303530B1
公开(公告)日：2019-03-06
申请号：EP16727382.0
申请日：2016-05-27
申请人： Evonik Degussa GmbH
发明人： FEDOR, Gabriela , ATKINS, Martin Philip , GOODRICH, Peter , KLATT HAMER, Christopher , WITTHAUT, Daniel , BOES, Ulrich
IPC分类号： C11B3/00 , C11B3/04 , C11B3/10 , C11B3/12

2. 发明授权

EP3303531B1 A PROCESS FOR REMOVING METAL FROM A METAL-CONTAINING GLYCERIDE OIL COMPRISING A BASIC QUATERNARY AMMONIUM SALT TREATMENT 失效转让
公开(公告)号：EP3303531B1
公开(公告)日：2019-03-20
申请号：EP16727383.8
申请日：2016-05-27
申请人： Evonik Degussa GmbH
发明人： FEDOR, Gabriela , ATKINS, Martin Philip , GOODRICH, Peter , KLATT HAMER, Christopher , WITTHAUT, Daniel , BOES, Ulrich
IPC分类号： C11B3/06 , C11B3/14 , C11B3/00 , C11B3/12 , C11B3/02

3. 发明公开

EP3098293A1 A PROCESS FOR REMOVING METAL FROM A METAL-CONTAINING GLYCERIDE OIL COMPRISING A BASIC QUATERNARY AMMONIUM SALT TREATMENT 审中-公开
标题翻译： PROCESS FOR金属从含金属甘油酯WITH碱性季胺盐的治疗REMOVAL
公开(公告)号：EP3098293A1
公开(公告)日：2016-11-30
申请号：EP15169317.3
申请日：2015-05-27
申请人： Evonik Degussa GmbH
发明人： FEDOR, Gabriela , ATKINS, Martin Philip , GOODRICH, Peter , KLATT HAMER, Christopher , WITTHAUT, Daniel , BOES, Ulrich
IPC分类号： C11B3/06 , C11B3/14 , C11B3/00 , C11B3/12 , C11B3/02
CPC分类号： C11B3/06 , C11B3/001 , C11B3/006 , C11B3/02 , C11B3/04 , C11B3/14
摘要： The present invention relates to a process for removing metal from metal-containing glyceride oil comprising the steps of:
(i) contacting a glyceride oil, comprising chromium, manganese, iron, cobalt, nickel and/or copper in a total amount of from 10 mg/kg to 10,000 mg/kg, with a liquid comprising a basic quaternary ammonium salt to form a treated glyceride oil; wherein the basic quaternary ammonium salt comprises a basic anion selected from hydroxide, alkoxide, alkylcarbonate, hydrogen carbonate, carbonate, serinate, prolinate, histidinate, threoninate, valinate, asparaginate, taurinate and lysinate; and
(ii) separating the treated glyceride oil from a salt comprising the quaternary ammonium cation, providing a treated glyceride oil containing a reduced amount of metals.
摘要翻译：本发明涉及一种用于从含有金属的甘油酯油中除去金属，包括以下步骤：（i）使甘油酯油，包括铬，锰，铁，钴，镍和/或铜在10的总量毫克/千克至10,000毫克/千克，与包括基本季铵盐以形成处理过的甘油酯油的液体; worin基本季铵盐包括选自氢氧化物，醇盐，烷基碳酸盐，碳酸氢盐，碳酸盐，丝氨酸，脯氨酸，组氨酸，苏氨酸，缬氨酸，天冬氨酸，牛磺酸和赖氨酸盐中的碱性阴离子; 和（ii）分离盐包括季铵阳离子处理过的油的甘油酯，提供了治疗甘油酯油含有金属的量减少。

4. 发明公开

EP3098292A1 A PROCESS FOR REFINING GLYCERIDE OIL COMPRISING A BASIC QUATERNARY AMMONIUM SALT TREATMENT 审中-公开
标题翻译： VERFAHREN ZUM RAFFINIENEN VONGLYCERIDÖLMIT EINER BEHANDLUNG MIT BASISCHEMQUATERNÄREMAMMONIUMSALZ
公开(公告)号：EP3098292A1
公开(公告)日：2016-11-30
申请号：EP15169311.6
申请日：2015-05-27
申请人： Evonik Degussa GmbH
发明人： FEDOR, Gabriela , ATKINS, Martin Philip , GOODRICH, Peter , KLATT HAMER, Christopher , WITTHAUT, Daniel , BOES, Ulrich
IPC分类号： C11B3/00 , C11B3/04 , C11B3/10 , C11B3/12
CPC分类号： C11B3/06 , C11B3/001 , C11B3/04 , C11B3/10 , C11B3/12 , C11B3/14
摘要： The present invention relates to a process for refining glyceride oil comprising the steps of:
(i) contacting glyceride oil with a liquid comprising a basic quaternary ammonium salt to form a treated glyceride oil; wherein the quaternary ammonium salt comprises a basic anion selected from hydroxide, alkoxide, alkylcarbonate, hydrogen carbonate, carbonate, serinate, prolinate, histidinate, threoninate, valinate, asparaginate, taurinate and lysinate; and a quaternary ammonium cation;
(ii) separating the treated glyceride oil from a salt comprising the quaternary ammonium cation; and
(iii) subjecting the treated glyceride oil after the separation step to at least one further refining step;
and to the use of contacting a glyceride oil with the basic quaternary ammonium salt for preventing or reducing the formation of fatty acid esters of chloropropanols and/or glycidol upon heating of the glyceride oil.
摘要翻译：本发明涉及一种精制甘油酯油的方法，包括以下步骤：（i）使甘油酯油与包含碱性季铵盐的液体接触以形成经处理的甘油酯油; 其中季铵盐包括选自氢氧化物，醇盐，烷基碳酸盐，碳酸氢盐，碳酸盐，丝氨酸盐，脯氨酸盐，组氨酸盐，苏氨酸盐，缬氨酸盐，天冬酰胺酸盐，牛磺酸盐和赖氨酸盐的碱性阴离子; 和季铵阳离子; （ii）从包含季铵阳离子的盐分离经处理的甘油酯油; 和（iii）在分离步骤之后对经处理的甘油酯油进行至少一个进一步的精制步骤; 并且使用甘油酯油与碱性季铵盐接触，以防止或减少加热甘油酯油时氯丙醇和/或缩水甘油的脂肪酸酯的形成。

5. 发明公开

EP3303531A1 A PROCESS FOR REMOVING METAL FROM A METAL-CONTAINING GLYCERIDE OIL COMPRISING A BASIC QUATERNARY AMMONIUM SALT TREATMENT 失效转让
标题翻译：一种从含有金属的甘油酯油中去除金属的方法，该甘油酯油包含碱性季铵盐处理剂
公开(公告)号：EP3303531A1
公开(公告)日：2018-04-11
申请号：EP16727383.8
申请日：2016-05-27
申请人： Evonik Degussa GmbH
发明人： FEDOR, Gabriela , ATKINS, Martin Philip , GOODRICH, Peter , KLATT HAMER, Christopher , WITTHAUT, Daniel , BOES, Ulrich
IPC分类号： C11B3/06 , C11B3/14 , C11B3/00 , C11B3/12 , C11B3/02
CPC分类号： C11B3/06 , C11B3/001 , C11B3/006 , C11B3/02 , C11B3/04 , C11B3/14
摘要： The present invention relates to a process for removing metal from metal-containing glyceride oil comprising the steps of: (i) contacting a glyceride oil, comprising chromium, manganese, iron, cobalt, nickel and/or copper in a total amount of from 10 mg/kg to 10,000 mg/kg, with a liquid comprising a basic quaternary ammonium salt to form a treated glyceride oil; wherein the basic quaternary ammonium salt comprises a basic anion selected from hydroxide, alkoxide, alkylcarbonate, hydrogen carbonate, carbonate, serinate, prolinate, histidinate, threoninate, valinate, asparaginate, taurinate and lysinate; and (ii) separating the treated glyceride oil from a salt comprising the quaternary ammonium cation, providing a treated glyceride oil containing a reduced amount of metals.

6. 发明公开

EP3303530A1 A PROCESS FOR REFINING GLYCERIDE OIL COMPRISING A BASIC QUATERNARY AMMONIUM SALT TREATMENT 审中-公开
标题翻译：精制包含碱性季铵盐处理的甘油酯的方法
公开(公告)号：EP3303530A1
公开(公告)日：2018-04-11
申请号：EP16727382.0
申请日：2016-05-27
申请人： Evonik Degussa GmbH
发明人： FEDOR, Gabriela , ATKINS, Martin Philip , GOODRICH, Peter , KLATT HAMER, Christopher , WITTHAUT, Daniel , BOES, Ulrich
IPC分类号： C11B3/00 , C11B3/04 , C11B3/10 , C11B3/12
CPC分类号： C11B3/06 , C11B3/001 , C11B3/04 , C11B3/10 , C11B3/12 , C11B3/14
摘要： The present invention relates to a process for refining glyceride oil comprising the steps of: (i) contacting glyceride oil with a liquid comprising a basic quaternary ammonium salt to form a treated glyceride oil; wherein the quaternary ammonium salt comprises a basic anion selected from hydroxide, alkoxide, alkylcarbonate, hydrogen carbonate, carbonate, serinate, prolinate, histidinate, threoninate, valinate, asparaginate, taurinate and lysinate; and a quaternary ammonium cation; (ii) separating the treated glyceride oil from a salt comprising the quaternary ammonium cation; and (iii) subjecting the treated glyceride oil after the separation step to at least one further refining step; and to the use of contacting a glyceride oil with the basic quaternary ammonium salt for preventing or reducing the formation of fatty acid esters of chloropropanols and/or glycidol upon heating of the glyceride oil.

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