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    • 3. 发明公开
    • Polymer dye particles and process for making polymer dye particles
    • Polymer-Farbstoff Partikel sowie Verfahren zu deren Herstellung
    • EP1319671A1
    • 2003-06-18
    • EP02079964.9
    • 2002-11-28
    • EASTMAN KODAK COMPANY
    • Wang, Xiaoru, c/o Eastman Kodak CompanyChen, Huijuan D., c/o Eastman Kodak Company
    • C08F2/44
    • C09D11/30C08F2/44
    • This invention relates to a process for making polymer-dye particles comprising, in order:

      I) forming a colorant mixture comprising a water insoluble dye and an organic medium containing at least one ethylenically-unsaturated monomer;
      II) combining the colorant mixture with an aqueous mixture comprising a surfactant and a co-stabilizer to form a colorant mixture/aqueous mixture;
      III) causing the colorant mixture/aqueous mixture to form a stable aqueous droplet mixture via strong agitation; and
      IV) initiating polymerization to form composite polymer-dye particles comprising a colorant phase and a polymer phase;
         wherein an addition polymerization initiator is added prior to initiating polymerization.
      It further relates to composite polymer dye particles prepared by the above process and to composite polymer dye particles comprising a colorant phase containing a water insoluble dye, and a polymer phase, said particles being associated with a co-stabilizer.
    • 本发明涉及一种制备聚合物染料颗粒的方法,其包括以下顺序:I)形成包含水不溶性染料和含有至少一种烯属不饱和单体的有机介质的着色剂混合物; II)将着色剂混合物与包含表面活性剂和共稳定剂的水性混合物组合以形成着色剂混合物/含水混合物; III)使着色剂混合物/含水混合物通过强烈搅动形成稳定的水滴混合物; 和IV)引发聚合以形成包含着色剂相和聚合物相的复合聚合物 - 染料颗粒; 其中在引发聚合之前加入加成聚合引发剂。 它还涉及通过上述方法制备的复合聚合物染料颗粒和包含含有水不溶性染料的着色相和聚合物相的复合聚合物染料颗粒,所述颗粒与共稳定剂缔合。