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    • 4. 发明公开
    • METHOD FOR MANUFACTURING HIGH-PURITY ORGANOSILICON COMPOUND
    • VERFAHREN ZUR HERSTELLUNG EINER HOCHREINEN ORGANOSILICIUMVERBINDUNG
    • EP2940062A1
    • 2015-11-04
    • EP13868759.5
    • 2013-12-26
    • Dow Corning Toray Co., Ltd.
    • TAMURA SeikiSOUDA TatsuoSAWAYAMA SayuriHORI Seiji
    • C08G77/34C08G77/38C07F7/20A61K8/89
    • C08G77/46A61K8/894A61K2800/10A61Q19/00C07F7/20C08G77/34C08G77/38C08L83/12C08L71/00
    • The present invention relates to a production method for a liquid high-purity organosilicon compound, the method comprising the steps of:
      adding, to a mixture containing an organosilicon compound selected from a group consisting of organomodified silcones and organomodified silanes and impurities, an organic wax having affinity with the impurities and having a higher melting point than the organosilicon compound, melting and mixing while heating, and introducing the impurities into the melted organic wax;
      obtaining a solidified product of the organic wax by cooling the organic wax; and
      performing solid/liquid phase separation on the organosilicon compound and the solidified product of the organic wax.
      With the present invention, it is possible to provide a useful method for producing a high-purity organosilicon compound stably and on a commercial scale.
    • 液体高纯度有机硅化合物的制造方法技术领域本发明涉及一种液体高纯度有机硅化合物的制造方法,该方法包括以下步骤:向含有有机硅化合物的有机硅化合物和有机改性硅烷和杂质的混合物中加入有机蜡 与杂质具有亲和性,并且具有比有机硅化合物更高的熔点,在加热时熔融和混合,并将杂质引入熔融的有机蜡中; 通过冷却有机蜡获得有机蜡的固化产物; 并在有机硅化合物和有机蜡的固化产物上进行固相/液相分离。 通过本发明,可以提供稳定且商业规模生产高纯度有机硅化合物的有用方法。