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1. 发明公开

EP1114023A1 PROCESS FOR PREPARING CARBOXYLIC ACIDS 有权
标题翻译：用于生产碳氢酸
公开(公告)号：EP1114023A1
公开(公告)日：2001-07-11
申请号：EP99948206.0
申请日：1999-09-14
申请人： Dow AgroSciences LLC
发明人： RINGER, James, William , MOLZAHN, David, Craig , HUCUL, Dennis, Alexander
IPC分类号： C07C227/02 , C07C51/16 , C07F9/38
CPC分类号： C07F9/3813 , C07C51/16 , C07C227/02 , C07C59/08 , C07C53/08 , C07C59/06 , C07C229/12 , C07C229/16 , C07C229/22
摘要： Aliphatic primary alcohols, including aliphatic primary alcohols possessing one or more oxygen, nitrogen and/or phosphorus heteroatoms that may be atoms substituting for carbon atoms in the alkyl group or component atoms of substituents on the alkyl group, were converted into salts of carboxylic acids by contacting an alkaline aqueous solution of the primary alcohol with a catalyst comprising cobalt, copper, and at least one of cerium, iron, zinc, and zirconium. Diethanolamine, for example, was converted to sodium iminodiacetate by treatment in an aqueous medium containing sodium hydroxyde with a catalyst that was obtained by reducing a mixture of cobalt, copper, and zirconium oxides with hydrogen.

2. 发明公开

EP0888297A1 N-ARYLSULFILIMINE COMPOUNDS AND THEIR USE AS CATALYSTS IN THE PREPARATION OF N-ARYLARYLSULFONAMIDE COMPOUNDS 失效
标题翻译： N-芳基磺酰胺类化合物及其在制备N-芳基磺酰胺化合物中的催化剂
公开(公告)号：EP0888297A1
公开(公告)日：1999-01-07
申请号：EP97947582.0
申请日：1997-11-13
申请人： Dow AgroSciences LLC
发明人： RINGER, James, William , PEARSON, Douglas, Lee , SCOTT, Carmen, A. , WALLIN, Anne, Parson
IPC分类号： B01J31 , C07C303 , C07C381 , C07D213 , C07D231 , C07D239 , C07D487 , C07C311
CPC分类号： C07D213/76 , B01J31/0222 , B01J31/0224 , B01J31/0229 , B01J31/0232 , B01J31/0235 , B01J31/0237 , B01J31/0244 , B01J31/0271 , C07C303/38 , C07C381/10 , C07D231/38 , C07D239/42 , C07D487/04 , C07C311/21
摘要： N-arylsulfilimine compounds, such as S,S-dimethyl-N-(2,6-dichlorophenyl)sulfilimine, were prepared and found to catalyze the reaction of aromatic sulfonyl chloride compounds, such as 2-chlorosulfonyl-7-fluoro-5-ethoxy[1,2,4]-triazolo[1,5-c]pyrimidine, with aromatic amine compounds, such as 2,6-dichloroaniline, to form N-arylarylsulfonamide compounds, such as N-(2,6-dichlorophenyl)-7-fluoro-5-ethoxy-[1,2,4]triazolo[1,5-c]pyrimidine-2-sulfonamide. The aryl moiety of the N-arylsulfilimine catalyst and the aryl moiety of the aromatic amine compound were generally chosen to be identical.
摘要翻译： N-芳基硫亚胺化合物，如S，S-二甲基-N-（2,6-二氯苯基）硫亚胺，被发现催化芳族磺酰氯化合物如2-氯磺酰基-7-氟-5- 乙氧基[1,2,4] - 三唑并[1,5-c]嘧啶与芳香族胺化合物如2,6-二氯苯胺反应生成N-芳基芳基磺酰胺化合物，例如N-（2,6-二氯苯基） -7-氟-5-乙氧基 - [1,2,4]三唑并[1,5-c]嘧啶-2-磺酰胺。 N-芳基硫亚胺催化剂的芳基部分和芳香胺化合物的芳基部分通常选择为相同的。

3. 发明授权

EP1114023B1 PROCESS FOR PREPARING CARBOXYLIC ACIDS 有权
标题翻译：用于生产碳氢酸
公开(公告)号：EP1114023B1
公开(公告)日：2004-05-26
申请号：EP99948206.0
申请日：1999-09-14
申请人： Dow AgroSciences LLC
发明人： RINGER, James, William , MOLZAHN, David, Craig , HUCUL, Dennis, Alexander
IPC分类号： C07C227/02 , C07C51/16 , C07F9/38
CPC分类号： C07F9/3813 , C07C51/16 , C07C227/02 , C07C59/08 , C07C53/08 , C07C59/06 , C07C229/12 , C07C229/16 , C07C229/22

4. 发明公开

EP1042303A1 CHLOROPYRIMIDINE PROCESS 有权
标题翻译：氯化嘧啶工艺
公开(公告)号：EP1042303A1
公开(公告)日：2000-10-11
申请号：EP98964168.3
申请日：1998-12-18
申请人： Dow AgroSciences LLC
发明人： LENG, Ronald, Bruce , RINGER, James, William , MAURER, Julie, Lynn
IPC分类号： C07D239/34 , C07D239/30
CPC分类号： C07D239/30 , C07D239/34 , Y02P20/582
摘要： Chloropyrimidine compounds, such as 4,6-dichloro-2-ethoxypyrimidine, were prepared in good yield and good purity from the corresponding hydroxypyrimidine compounds in the absence of organic solvents and with a reduced amount of phosphorus oxychloride by carrying out the reaction in the presence of a trialkylamine compound and phosphorus trichloride. The additions of hydroxypyrimidine compound and trialkylamine compound could be made in segments. The chloropyrimidine compounds produced were recovered in an improved manner by adding chlorine to convert the chlorophosphoric acid by-products and phosphorus trichloride to phosphorus oxychloride, diluting the mixture with additional chloropyrimidine compound and removing the phosphorus oxychloride by distillation, combining the residue with water and a base, distilling the trialkylamine compound from the resulting mixture, and removing the aqueous phase.
摘要翻译：在不存在有机溶剂的条件下，通过在相应的羟基嘧啶化合物存在下以良好的产率和高纯度制备氯嘧啶化合物，例如4,6-二氯-2-乙氧基嘧啶，其中通过在存在的情况下进行反应来减少量的三氯氧化磷的三烷基胺化合物和三氯化磷。可以分段加入羟基嘧啶化合物和三烷基胺化合物。通过加入氯将氯代磷酸副产物和三氯化磷转化成三氯氧化磷，用另外的氯嘧啶化合物稀释混合物并通过蒸馏除去三氯氧化磷，将残余物与水和甲醇混合，以改进的方式回收所产生的氯嘧啶化合物从所得混合物中蒸馏出三烷基胺化合物，并除去水相。

5. 发明授权

EP1756127B1 PURIFICATION OF N-(PHOSPHONOMETHYL)GLYCINE 有权
标题翻译：纯化的N-（膦酰基甲基）甘氨酸
公开(公告)号：EP1756127B1
公开(公告)日：2008-12-17
申请号：EP05753118.8
申请日：2005-05-20
申请人： Dow AgroSciences LLC
发明人： TAI, Jimmy, Jui , PRAAY, Herbert, Nathan , RINGER, James, William , EMONDS, Mark, Victor, Michael
IPC分类号： C07F9/38
CPC分类号： C07F9/025 , C07F9/3813
摘要： The present invention is a process for the purification of glyphosate (PMG) comprising: 1) dissolving or suspending a material comprising PMG in water, in the presence of a base, to produce a composition comprising a PMG salt in an aqueous base, contacting the composition with an acid, such that the PMG salt is neutralized, forming a precipitate of PMG, and 3) isolating the precipitate of PMG. with the proviso that the composition of step 1) is not concentrated or filtered using a nanofiltration membrane.

6. 发明公开

EP1756127A1 PURIFICATION OF N-(PHOSPHONOMETHYL)GLYCINE 有权
标题翻译：纯化的N-（膦酰基甲基）甘氨酸
公开(公告)号：EP1756127A1
公开(公告)日：2007-02-28
申请号：EP05753118.8
申请日：2005-05-20
申请人： Dow AgroSciences LLC
发明人： TAI, Jimmy, Jui , PRAAY, Herbert, Nathan , RINGER, James, William , EMONDS, Mark, Victor, Michael
IPC分类号： C07F9/38
CPC分类号： C07F9/025 , C07F9/3813
摘要： The present invention is a process for the purification of glyphosate (PMG) comprising: 1) dissolving or suspending a material comprising PMG in water, in the presence of a base, to produce a composition comprising a PMG salt in an aqueous base, contacting the composition with an acid, such that the PMG salt is neutralized, forming a precipitate of PMG, and 3) isolating the precipitate of PMG. with the proviso that the composition of step 1) is not concentrated or filtered using a nanofiltration membrane.

7. 发明授权

EP1042303B1 CHLOROPYRIMIDINE PROCESS 有权
标题翻译：氯化嘧啶工艺
公开(公告)号：EP1042303B1
公开(公告)日：2003-02-05
申请号：EP98964168.3
申请日：1998-12-18
申请人： Dow AgroSciences LLC
发明人： LENG, Ronald, Bruce , RINGER, James, William , MAURER, Julie, Lynn
IPC分类号： C07D239/34 , C07D239/30
CPC分类号： C07D239/30 , C07D239/34 , Y02P20/582

8. 发明授权

EP0888297B1 N-ARYLSULFILIMINE COMPOUNDS AND THEIR USE AS CATALYSTS IN THE PREPARATION OF N-ARYLARYLSULFONAMIDE COMPOUNDS 失效
标题翻译： N-芳基磺酰胺类化合物及其在制备N-芳基磺酰胺化合物中的催化剂
公开(公告)号：EP0888297B1
公开(公告)日：2000-08-30
申请号：EP97947582.9
申请日：1997-11-13
申请人： Dow AgroSciences LLC
发明人： RINGER, James, William , PEARSON, Douglas, Lee , SCOTT, Carmen, A. , WALLIN, Anne, Parson
IPC分类号： C07C381/10 , C07D333/46 , C07D231/38 , C07D213/76 , C07D487/04 , C07C303/38
CPC分类号： C07D213/76 , B01J31/0222 , B01J31/0224 , B01J31/0229 , B01J31/0232 , B01J31/0235 , B01J31/0237 , B01J31/0244 , B01J31/0271 , C07C303/38 , C07C381/10 , C07D231/38 , C07D239/42 , C07D487/04 , C07C311/21

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