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1. 发明授权

EP0892762B1 METHOD OF PREPARATION OF LITHIUM MANGANESE OXIDE SPINEL 失效
标题翻译： VERFAHREN ZUR HERSTELLUNG EINES LITHIUMMANGANOXIDSPINELLES
公开(公告)号：EP0892762B1
公开(公告)日：2001-05-30
申请号：EP97920053.2
申请日：1997-04-02
申请人： DURACELL INC.
发明人： WANG, Enoch, I. , BOWDEN, William, L. , GIONET, Paul
IPC分类号： C01G45/00 , H01M4/50
CPC分类号： H01M4/505 , C01G45/1221 , C01P2002/32 , C01P2006/40 , H01M10/0525
摘要： A method of making lithium manganese oxide of spinel structure is disclosed. The method involves the step of prelithiating a manganese oxide by reacting it with lithium hydroxide or lithium salt and then reacting the prelithiated manganese oxide in a second step at elevated temperature to form a lithium manganese oxide spinel. In a specific embodiment manganese dioxide powder is reacted with lithium hydroxide to prelithiate the manganese dioxide and the prelithiated manganese dioxide is separated from the reaction mixture and heated and reacted with lithium carbonate at elevated temperature to convert it to lithium manganese oxide spinel. The spinel product may be used advantageously in secondary (rechargeable) batteries.
摘要翻译：公开了制备尖晶石结构的锂锰氧化物的方法。该方法包括通过使其与氢氧化锂或锂盐反应来预氧化锰氧化物，然后在升高的温度下在第二步骤中使预氧化的氧化锰反应形成锰酸锂尖晶石。在具体实施方案中，将二氧化锰粉末与氢氧化锂反应以预氧化二氧化锰，并将预锂化的二氧化锰与反应混合物分离，并在升高的温度下加热并与碳酸锂反应以将其转化为锰酸锂尖晶石。尖晶石产品可以有利地用于二次（可充电）电池中。

2. 发明公开

EP0842120A1 AN IMPROVED PROCESS FOR MAKING A LITHIATED LITHIUM MANGANESE OXIDE SPINEL 失效
标题翻译：一种改进的锂锰氧化物锂锰尖晶石的制备方法
公开(公告)号：EP0842120A1
公开(公告)日：1998-05-20
申请号：EP96918315.0
申请日：1996-06-05
申请人： DURACELL INC.
发明人： BOWDEN, William, L. , WANG, Enoch , KALLMES, Andrew
IPC分类号： C01G45 , C01D15 , H01M4
CPC分类号： H01M4/505 , C01G45/1242 , C01G45/1257 , C01P2002/32
摘要： Disclosed is a process for making a lithiated lithium manganese oxide spinel of the formula: Li(1+x)Mn2O4 comprising contacting a lithium manganese oxide spinel of the formula: LiMn2O4 with a lithium carboxylate compound, at a temperature and for a time sufficient to decompose the carboxylate compound and free the lithium to form said lithiated spinel.
摘要翻译：本发明公开了一种制备式Li（1 + x）Mn2O4的锂化锰酸锂尖晶石的方法，包括使式LiMn2O4的锂锰氧化物尖晶石与羧酸锂化合物在一定温度下接触足够的时间分解羧酸盐化合物并释放锂以形成所述锂化尖晶石。

3. 发明公开

EP0423117A1 ELECTROCHEMICAL CELLS 失效
标题翻译：电化学电池。
公开(公告)号：EP0423117A1
公开(公告)日：1991-04-24
申请号：EP89900737.0
申请日：1988-11-23
申请人： DURACELL INC. (a Delaware corporation)
发明人： WHITNEY, Thomas, A. , BOWDEN, William, L. , DEY, Arabinda, N.
IPC分类号： H01M , H01M4 , H01M6
CPC分类号： H01M4/58 , H01M4/48 , H01M6/00 , H01M6/16
摘要： Cellules électrochimiques dans lesquelles la cathode comprend des céramiques contenant des oxydes de cuivre caractérisés comme étant des perovskites.

4. 发明公开

EP1084515A1 LITHIATED MANGANESE OXIDE 审中-公开
标题翻译： LITHIIERTES MANGANOXID
公开(公告)号：EP1084515A1
公开(公告)日：2001-03-21
申请号：EP99922890.1
申请日：1999-05-10
申请人： DURACELL INC.
发明人： MOSES, Peter, R. , BOWDEN, William, L. , ILTCHEV, Nikolay , BRANDT, Klaus
IPC分类号： H01M4/50 , C01G45/02 , H01M6/14
CPC分类号： C01G45/1228 , C01G45/02 , C01P2002/32 , C01P2002/54 , C01P2002/72 , C01P2006/40 , H01M4/50 , H01M4/505 , H01M6/16
摘要： A lithiated manganese oxide for use in primary lithium cells is described. The lithiated manganese oxide can be prepared by exposure to a lithium source under conditions that result in the formation of a modified manganese oxide phase. When the modified phase is used in a primary lithium cell, the operating voltage of an electrochemical cell containing the lithiated manganese oxide increases relative to the operating voltage of a cell containing a manganese dioxide that is not exposed to the lithium source.

5. 发明授权

EP0842118B1 AN IMPROVED MANGANESE DIOXIDE FOR LITHIUM BATTERIES 失效
标题翻译：改进二氧化锰锂电池
公开(公告)号：EP0842118B1
公开(公告)日：2004-05-26
申请号：EP96917156.0
申请日：1996-06-05
申请人： DURACELL INC.
发明人： BOWDEN, William, L. , CAPPARELLA, Mark , FOOKSA, Radek
IPC分类号： C01G45/02 , H01M4/50
CPC分类号： C01G45/02 , C01G45/1228 , C01P2002/54 , C01P2006/40 , H01M4/50 , H01M4/502 , H01M2300/0014
摘要： Disclosed is a process for treating manganese dioxide containing ion-exchangeable cations by replacing the ion-exchangeable cations present in the manganese dioxide with lithium by a process comprising first replacing ion-exchangeable cations present in the manganese dioxide with hydrogen. This readily is accomplished by slurrying the manganese dioxide in an aqueous acid solution. The resulting acidic manganese dioxide then is neutralized with a basic solution of a lithium containing compound, such as lithium hydroxide. This neutralization step serves to accomplish replacement of the previously introduced hydrogen, by ion-exchange, with lithium. The manganese dioxide then is washed with water, dried, and heat-treated at an elevated temperature, in conventional manner, to convert the gamma manganese dioxide to a mixture of the gamma and beta forms, which then is used as the active cathodic component in an electrochemical cell.

6. 发明授权

EP0664768B1 PROCESS FOR PRODUCING MANGANESE DIOXIDE 失效
标题翻译：用于生产二氧化锰
公开(公告)号：EP0664768B1
公开(公告)日：1998-12-23
申请号：EP93919880.0
申请日：1993-08-04
申请人： DURACELL INC.
发明人： WANG, Enoch, I. , LIN, Lifun , BOWDEN, William, L.
IPC分类号： C01G45/02 , H01M4/50
CPC分类号： H01M4/502 , C01G45/02 , C01P2004/03 , C01P2004/10 , C01P2006/10 , C01P2006/40 , C01P2006/60 , H01M4/50

7. 发明授权

EP0842120B1 AN IMPROVED PROCESS FOR MAKING A LITHIATED LITHIUM MANGANESE OXIDE SPINEL 失效
标题翻译：改进方法制造锂锂化的氧化锰尖晶石
公开(公告)号：EP0842120B1
公开(公告)日：2003-01-29
申请号：EP96918315.1
申请日：1996-06-05
申请人： DURACELL INC.
发明人： BOWDEN, William, L. , WANG, Enoch , KALLMES, Andrew
IPC分类号： C01G45/12 , C01G45/00 , H01M4/50
CPC分类号： H01M4/505 , C01G45/1242 , C01G45/1257 , C01P2002/32
摘要： Disclosed is a process for making a lithiated lithium manganese oxide spinel of the formula: Li(1+x)Mn2O4 comprising contacting a lithium manganese oxide spinel of the formula: LiMn2O4 with a lithium carboxylate compound, at a temperature and for a time sufficient to decompose the carboxylate compound and free the lithium to form said lithiated spinel.

8. 发明公开

EP0892762A1 METHOD OF PREPARATION OF LITHIUM MANGANESE OXIDE SPINEL 失效
标题翻译：制备氧化锰氧化锂的方法
公开(公告)号：EP0892762A1
公开(公告)日：1999-01-27
申请号：EP97920053.0
申请日：1997-04-02
申请人： DURACELL INC.
发明人： WANG, Enoch, I. , BOWDEN, William, L. , GIONET, Paul
IPC分类号： C01D15 , C01G45 , H01M4 , H01M10
CPC分类号： H01M4/505 , C01G45/1221 , C01P2002/32 , C01P2006/40 , H01M10/0525
摘要： A method of making lithium manganese oxide of spinel structure is disclosed. The method involves the step of prelithiating a manganese oxide by reacting it with lithium hydroxide or lithium salt and then reacting the prelithiated manganese oxide in a second step at elevated temperature to form a lithium manganese oxide spinel. In a specific embodiment manganese dioxide powder is reacted with lithium hydroxide to prelithiate the manganese dioxide and the prelithiated manganese dioxide is separated from the reaction mixture and heated and reacted with lithium carbonate at elevated temperature to convert it to lithium manganese oxide spinel. The spinel product may be used advantageously in secondary (rechargeable) batteries.
摘要翻译：公开了一种制造尖晶石结构的锂锰氧化物的方法。该方法包括通过使锰氧化物与氢氧化锂或锂盐反应，然后在升高的温度下在第二步中使预锂化的锰氧化物反应以形成锂锰氧化物尖晶石来预氧化锰氧化物的步骤。在一个具体的实施方案中，二氧化锰粉末与氢氧化锂反应以使二氧化锰预锂化，并将预锂化的二氧化锰从反应混合物中分离出来，并在升高的温度下与碳酸锂反应并转化为氧化锂锰尖晶石。尖晶石产品可有利地用于二次（可再充电）电池。

9. 发明公开

EP0842118A1 AN IMPROVED MANGANESE DIOXIDE FOR LITHIUM BATTERIES 失效
标题翻译：用于锂电池的改进的二氧化锰
公开(公告)号：EP0842118A1
公开(公告)日：1998-05-20
申请号：EP96917156.0
申请日：1996-06-05
申请人： DURACELL INC.
发明人： BOWDEN, William, L. , CAPPARELLA, Mark , FOOKSA, Radek
IPC分类号： C01G45 , H01M4 , H01M6
CPC分类号： C01G45/02 , C01G45/1228 , C01P2002/54 , C01P2006/40 , H01M4/50 , H01M4/502 , H01M2300/0014
摘要： Disclosed is a process for treating manganese dioxide containing ion-exchangeable cations by replacing the ion-exchangeable cations present in the manganese dioxide with lithium by a process comprising first replacing ion-exchangeable cations present in the manganese dioxide with hydrogen. This readily is accomplished by slurrying the manganese dioxide in an aqueous acid solution. The resulting acidic manganese dioxide then is neutralized with a basic solution of a lithium containing compound, such as lithium hydroxide. This neutralization step serves to accomplish replacement of the previously introduced hydrogen, by ion-exchange, with lithium. The manganese dioxide then is washed with water, dried, and heat-treated at an elevated temperature, in conventional manner, to convert the gamma manganese dioxide to a mixture of the gamma and beta forms, which then is used as the active cathodic component in an electrochemical cell.
摘要翻译：本发明公开了一种处理含有可离子交换阳离子的二氧化锰的方法，该方法通过用氢气置换二氧化锰中存在的离子交换阳离子的方法用锂取代存在于二氧化锰中的可离子交换阳离子。这很容易通过将二氧化锰在酸水溶液中浆化来完成。然后用含锂化合物如氢氧化锂的碱性溶液中和所得酸性二氧化锰。该中和步骤用于通过用锂进行离子交换来完成先前引入的氢的置换。然后用水洗涤二氧化锰，干燥，并在常温下在升高的温度下进行热处理，以将γ-二氧化锰转化为γ和β形式的混合物，然后将γ-二氧化锰用作活性阴极组分电化学电池。

10. 发明公开

EP0664768A1 PROCESS FOR PRODUCING MANGANESE DIOXIDE 失效
标题翻译：用于生产二氧化锰。
公开(公告)号：EP0664768A1
公开(公告)日：1995-08-02
申请号：EP93919880.0
申请日：1993-08-04
申请人： DURACELL INC.
发明人： WANG, Enoch, I. , LIN, Lifun , BOWDEN, William, L.
IPC分类号： H01M4 , C01G45 , C25B11
CPC分类号： H01M4/502 , C01G45/02 , C01P2004/03 , C01P2004/10 , C01P2006/10 , C01P2006/40 , C01P2006/60 , H01M4/50
摘要： The invention relates to the manufacture of manganese dioxide by a chemical process. The resulting manganese dioxide product takes the form of particles characterized by filament-like protrusions jutting out from its surface. The manganese dioxide particles having such surface features can be manufactured by reacting manganese sulfate with sodium peroxodisulfate in an aqueous solution. The process can be controlled to yield high density manganese dioxide. The manganese dioxide formed in the process can be deposited directly onto the surface of electrolytic manganese dioxide (EMD). The manganese dioxide product is particularly suitable for use as a cathode active material in electrochemical cells.

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