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1. 发明公开

EP0926151A2 Ester group-containing siloxane compound, and its preparation method 审中-公开
标题翻译： Estergruppe enthaltende Siloxanverbindung，de deren Herstellung
公开(公告)号：EP0926151A2
公开(公告)日：1999-06-30
申请号：EP98120197.3
申请日：1998-10-30
申请人： CHISSO CORPORATION
发明人： Yamamoto, Yuuichi , Ayama, Koichi
IPC分类号： C07F7/08 , C08G77/22
CPC分类号： C07F7/0852 , C08G77/38 , C08G77/46
摘要： There are herein disclosed a siloxane compound represented by the formula (1)
wherein R 2 is a methyl group or a phenyl group; R 3 is an alkyl group having 1 to 6 carbon atoms or A; ℓ is an integer of 0 to 500; m is an integer of 0 to 1,000; n is an integer of 0 to 500; p is an integer of 0 to 2; and A is an ester group represented by the formula (2)
wherein R 6 is hydrogen or the methyl group; s is an integer of 0 to 100; and R 1 is a branched or a straight-chain alkyl group having 1 to 30 carbon atoms, a cyclohexyl group, a phenyl group, a benzyl group, a glycidyl group, or a fluorine-containing organic group represented by the formula (3)
wherein R 4 is a saturated hydrocarbon having 0 to 6 carbon atoms, and when 0 is selected, R 4 is not present; R 5 is hydrogen or fluorine; a is 0 or 1; and b and c are each an integer of 0 to 20, but for a, b and c, 0 is not simultaneously selected,
and a preparation method of the above siloxane compound.
摘要翻译：在此公开了由式（1）表示的硅氧烷化合物其中R 2是甲基或苯基; R 3是具有1至6个碳原子的烷基或A; l为0〜500的整数; m为0〜1000的整数; n为0〜500的整数。 p为0〜2的整数。 A为由式（2）表示的酯基其中R 6为氢或甲基; s为0〜100的整数; 和R 1是具有1至30个碳原子的支链或直链烷基，由式（1）表示的环己基，苯基，苄基，缩水甘油基或含氟有机基团 3）其中R 4是具有0至6个碳原子的饱和烃，并且当选择0时，R 4不存在; R 5是氢或氟; a是0或1; b和c各自为0〜20的整数，但对于a，b和c，不同时选择0，也可以是上述硅氧烷化合物的制备方法。

2. 发明公开

EP0376183A1 Ceramic composition and method for producing the same 失效
标题翻译： Keramische Zusammensetzung und Verfahren zu ihrer Herstellung。
公开(公告)号：EP0376183A1
公开(公告)日：1990-07-04
申请号：EP89123736.4
申请日：1989-12-22
申请人： Chisso Corporation
发明人： Ayama, Koichi , Noake, Kaneo
IPC分类号： C04B35/58 , C04B35/56
CPC分类号： C04B35/571 , C04B35/589
摘要： Ceramic composition and method for producing the same, characterised by sintering a molded product comprising polysilazane and at least one of silicon nitride powder and silicon carbide powder;
said polysilazane which have a skelton structure having the repeating units of the formula:
and precursor residues having the structural units represented by the formula at least one component selected from:
and connects each other;
in a state without sintering aid, under sintering condition of pressurized atomosphere at least one of nitrogen and ammonia at 800°C to 2200°C.
摘要翻译：陶瓷组合物及其制造方法，其特征在于，烧结包含聚硅氮烷和氮化硅粉末和碳化硅粉末中的至少一种的模塑产品; 所述聚硅氮烷具有具有下式的重复单元的碳纤维结构：具有由式表示的结构单元的前体残基和至少一种选自：CHEM的组分并彼此连接的前体残基; 在没有烧结助剂的状态下，在800〜2200℃的氮气和氨气中的至少一个加压的空气的烧结条件下。

3. 发明公开

EP0926151A3 Ester group-containing siloxane compound, and its preparation method 审中-公开
标题翻译：含酯基的硅氧烷化合物和它们的制备
公开(公告)号：EP0926151A3
公开(公告)日：2000-08-09
申请号：EP98120197.3
申请日：1998-10-30
申请人： CHISSO CORPORATION
发明人： Yamamoto, Yuuichi , Ayama, Koichi
IPC分类号： C07F7/08 , C08G77/22
CPC分类号： C07F7/0852 , C08G77/38 , C08G77/46
摘要： There are herein disclosed a siloxane compound represented by the formula (1) wherein R 2 is a methyl group or a phenyl group; R 3 is an alkyl group having 1 to 6 carbon atoms or A; is an integer of 0 to 500; m is an integer of 0 to 1,000; n is an integer of 0 to 500; p is an integer of 0 to 2; and A is an ester group represented by the formula (2) wherein R 6 is hydrogen or the methyl group; s is an integer of 0 to 100; and R 1 is a branched or a straight-chain alkyl group having 1 to 30 carbon atoms, a cyclohexyl group, a phenyl group, a benzyl group, a glycidyl group, or a fluorine-containing organic group represented by the formula (3) wherein R 4 is a saturated hydrocarbon having 0 to 6 carbon atoms, and when 0 is selected, R 4 is not present; R 5 is hydrogen or fluorine; a is 0 or 1; and b and c are each an integer of 0 to 20, but for a, b and c, 0 is not simultaneously selected, and a preparation method of the above siloxane compound.

4. 发明公开

EP0296433A2 New polysilazane and process for production of the same 失效
标题翻译： Polysilazan und Verfahren zu dessen Herstellung。
公开(公告)号：EP0296433A2
公开(公告)日：1988-12-28
申请号：EP88109318.1
申请日：1988-06-10
申请人： Chisso Corporation
发明人： Ayama, Koichi , Noake, Kaneo , Serita, Tamio
IPC分类号： C08G77/62 , C04B35/00
CPC分类号： C08G77/62 , C04B35/571 , C04B35/589
摘要： There is provided a new polysilazane product from a specific precursor. Desired molecular weight of the polysilazane can be obtained by selecting proper amount of a silazane or silylamine compound
as an additive. The polysilazane is stable during storage without gelation. The polymerization of the precursor can be carried out without gelation even at a high temperature and hence can be completed in a short time. The polysilazane can be made into ceramics fiber by spinning from a solution and subsequent firing.
摘要翻译：提供了来自特定前体的新型聚硅氮烷产品。所希望的聚硅氮烷的分子量可以通过选择适量的硅氮烷或甲硅烷基胺化合物作为添加剂来获得。聚硅氮烷在储存期间不凝胶化是稳定的。前体的聚合即使在高温下也可以无凝胶化地进行，因此可以在短时间内完成。聚硅氮烷可以通过从溶液中纺丝并随后烧制而制成陶瓷纤维。

5. 发明公开

EP0913401A2 Fluorine-containing siloxane compound and process for production thereof 失效
标题翻译：氟 - 卤素硅氧烷和Verfahren zu deren Herstellung
公开(公告)号：EP0913401A2
公开(公告)日：1999-05-06
申请号：EP98105395.2
申请日：1998-03-25
申请人： CHISSO CORPORATION
发明人： Isoda, Yuichi , Ayama, Koichi
IPC分类号： C07F7/08
CPC分类号： C07F7/0852 , C07F7/0874
摘要： According to the present invention there is disclosed a process for producing a fluorine-containing siloxane compound represented by the formula (3):
[wherein A is a fluorine-containing organic group represented by the formula (4):
(wherein R 1 and R 2 are each independently a fluorine atom or a trifluoromethyl group, R 3 is a hydrogen atom or a straight chain or branched chain hydrocarbon group having 1 to 8 carbon atoms, k is an integer of 0 to 16, m is an integer of 0 to 30, n is 0 or 1, and p is an integer of 0 to 9); r is an integer of 1 to 3; R 4 is a monovalent hydrocarbon group having 1 to 6 carbon atoms; and B 1 is a hydrogen atom, a methacryloxypropyl group or a vinyl group], which process comprises reacting a fluorine-containing silane represented by the formula (1):
(wherein R 1 , R 2 , R 3 , k, m, n and p have the same definitions as given above) with a chlorosilane represented by the formula (2):
(wherein R 4 , B 1 and r have the same definitions as given above). There is also disclosed a fluorine-containing siloxane compound of the formula (3) wherein B 1 is an isocyanate-containing group.
摘要翻译：式B2Si（R4）3-r（A）r（I）的含氟硅氧烷是新的，其中A =式（II）的基团; R1，R2 = F或CF3; R3 = H或1-8C烃基; k = 0-16; m = 0-30; n = 0或1; p = 0-9; q = 1-1000; r = 1-3; R4 = 1-6C烃基; 和B2 =式（III）的含异氰酸酯基团。还要求的是制备式B1Si（R4）3-r（A）r（IV）的硅氧烷，其中A =（II; q = 1）; 通过使（V）与式B1Si（R4）3-r（C1）r（VI）的氯代硅烷反应，得到B1 = H，甲基丙烯酰氧基丙基或乙烯基。

6. 发明公开

EP0296433A3 New polysilazane and process for production of the same 失效
标题翻译：新的多晶硅及其生产方法
公开(公告)号：EP0296433A3
公开(公告)日：1990-03-14
申请号：EP88109318.1
申请日：1988-06-10
申请人： Chisso Corporation
发明人： Ayama, Koichi , Noake, Kaneo , Serita, Tamio
IPC分类号： C08G77/62 , C04B35/00
CPC分类号： C08G77/62 , C04B35/571 , C04B35/589
摘要： There is provided a new polysilazane product from a specific precursor. Desired molecular weight of the polysilazane can be obtained by selecting proper amount of a silazane or silylamine compound
as an additive. The polysilazane is stable during storage without gelation. The polymerization of the precursor can be carried out without gelation even at a high temperature and hence can be completed in a short time. The polysilazane can be made into ceramics fiber by spinning from a solution and subsequent firing.

7. 发明公开

EP0913401A3 Fluorine-containing siloxane compound and process for production thereof 失效
标题翻译：它们的制备硅氧烷和方法含氟
公开(公告)号：EP0913401A3
公开(公告)日：2001-01-31
申请号：EP98105395.2
申请日：1998-03-25
申请人： CHISSO CORPORATION
发明人： Isoda, Yuichi , Ayama, Koichi
IPC分类号： C07F7/08
CPC分类号： C07F7/0852 , C07F7/0874
摘要： According to the present invention there is disclosed a process for producing a fluorine-containing siloxane compound represented by the formula (3): [wherein A is a fluorine-containing organic group represented by the formula (4): (wherein R 1 and R 2 are each independently a fluorine atom or a trifluoromethyl group, R 3 is a hydrogen atom or a straight chain or branched chain hydrocarbon group having 1 to 8 carbon atoms, k is an integer of 0 to 16, m is an integer of 0 to 30, n is 0 or 1, and p is an integer of 0 to 9); r is an integer of 1 to 3; R 4 is a monovalent hydrocarbon group having 1 to 6 carbon atoms; and B 1 is a hydrogen atom, a methacryloxypropyl group or a vinyl group], which process comprises reacting a fluorine-containing silane represented by the formula (1): (wherein R 1 , R 2 , R 3 , k, m, n and p have the same definitions as given above) with a chlorosilane represented by the formula (2): (wherein R 4 , B 1 and r have the same definitions as given above). There is also disclosed a fluorine-containing siloxane compound of the formula (3) wherein B 1 is an isocyanate-containing group.

8. 发明授权

EP0296433B1 New polysilazane and process for production of the same 失效
标题翻译：聚硅氮烷和方法及其生产。
公开(公告)号：EP0296433B1
公开(公告)日：1994-11-23
申请号：EP88109318.1
申请日：1988-06-10
申请人： Chisso Corporation
发明人： Ayama, Koichi , Noake, Kaneo , Serita, Tamio
IPC分类号： C08G77/62 , C04B35/00
CPC分类号： C08G77/62 , C04B35/571 , C04B35/589

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