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1. 发明公开

EP0825157A2 Water-repellent glass pane and method for producing same 失效
标题翻译： Wasserabweisende Glasscheibe und Verfahren zu deren Herstellung
公开(公告)号：EP0825157A2
公开(公告)日：1998-02-25
申请号：EP97114294.8
申请日：1997-08-19
申请人： CENTRAL GLASS COMPANY, LIMITED
发明人： Akamatsu, Yoshinori , Hamaguchi, Shigeo , Nishida, Yoshihiro , Yamamoto, Hideki
IPC分类号： C03C17/30 , B05D1/18
CPC分类号： C03C17/30 , C09K3/18 , Y10T428/315 , Y10T428/31525 , Y10T428/3154 , Y10T428/31612
摘要： The invention relates to a water-repellent glass pane having a glass substrate and a water-repellent film formed thereon. This glass pane is prepared by a first or second method. The first method includes sequential steps of (a) mixing together a raw material for producing the water-repellent film, an organic solvent for diluting the raw material, and water for hydrolyzing the raw material, such that the raw material is subjected to hydrolysis and then to dehydration and polycondensation, thereby to turn a mixture of the raw material, the organic solvent and the water into a sol; (b) adjusting water content of the sol, thereby to prepare a coating liquid; and (c) applying the coating liquid to the glass substrate, in an atmosphere having a first temperature and a relative humidity. The second method includes sequential steps of: (a) subjecting a surface of the glass substrate to an abrasive treatment; (b) subjecting the surface of the glass substrate to an acid treatment; and (c) applying a coating liquid to the surface of the glass substrate. The glass pane prepared by the first or second method is superior in abrasion resistance, sunshine resistance, hardness, adhesion to the glass substrate, and water-repellency for a long time.
摘要翻译：本发明涉及一种具有形成在其上的玻璃基板和防水膜的防水玻璃板。该玻璃板通过第一种或第二种方法制备。第一种方法包括以下顺序步骤：（a）将用于制备防水膜的原料，用于稀释原料的有机溶剂和用于水解原料的水混合在一起，使原料进行水解，然后进行脱水缩聚，从而将原料，有机溶剂和水的混合物变成溶胶; （b）调节溶胶的含水量，由此制备涂布液; 和（c）在具有第一温度和相对湿度的气氛中将涂布液涂布到玻璃基板上。第二种方法包括以下顺序的步骤：（a）对玻璃基板的表面进行磨料处理; （b）对玻璃基板的表面进行酸处理; 和（c）将涂布液施加到玻璃基板的表面。通过第一种或第二种方法制备的玻璃板在耐磨性，耐日光性，硬度，与玻璃基材的粘附性以及长时间的拒水性方面都是优异的。

2. 发明授权

EP0866037B1 Multilayered water-repellent film and method of forming same on glass substrate 失效
标题翻译：多层防水膜和处理其在玻璃基板上制备
公开(公告)号：EP0866037B1
公开(公告)日：2002-04-10
申请号：EP98110212.2
申请日：1994-11-10
申请人： CENTRAL GLASS COMPANY, LIMITED , NISSAN MOTOR CO., LTD.
发明人： Takahashi, Osamu , Hamaguchi, Shigeo , Otani, Michitaka , Nishida, Yoshihiro , Nakamura, Ichiro , Sugawara, Satoko , Kondo, Takeshi , Akamatsu, Yoshinori , Kai, Yasuaki
IPC分类号： C03C17/42
CPC分类号： C03C17/34 , C03C17/007 , C03C17/42 , C03C2217/445 , C03C2217/476 , C03C2217/76 , C03C2217/77 , Y10T428/24364 , Y10T428/24479 , Y10T428/24612 , Y10T428/31612 , Y10T428/31663

3. 发明公开

EP0866037A2 Multilayered water-repellent film and method of forming same on glass substrate 失效
标题翻译：多层防水膜和处理其在玻璃基板上制备
公开(公告)号：EP0866037A2
公开(公告)日：1998-09-23
申请号：EP98110212.2
申请日：1994-11-10
申请人： CENTRAL GLASS COMPANY, LIMITED , NISSAN MOTOR CO., LTD.
发明人： Takahashi, Osamu , Hamaguchi, Shigeo , Otani, Michitaka , Nishida, Yoshihiro , Nakamura, Ichiro , Sugawara, Satoko , Kondo, Takeshi , Akamatsu, Yoshinori , Kai, Yasuaki
IPC分类号： C03C17/42
CPC分类号： C03C17/34 , C03C17/007 , C03C17/42 , C03C2217/445 , C03C2217/476 , C03C2217/76 , C03C2217/77 , Y10T428/24364 , Y10T428/24479 , Y10T428/24612 , Y10T428/31612 , Y10T428/31663
摘要： The invention relates to a method of forming on a glass substrate a multilayered water-repellent film having a first metal oxide layer and a second water-repellent layer, comprising the followings steps: (a) forming the first metal oxide layer on the glass substrate such that the first metal oxide layer has a minutely rough surface having on the surface micro-pits and/or micro-projections; (b) preparing a coating mixture comprising 0.10-20 wt% of a fluoroalkylsilane, 0.10-2 wt% of tin oxide particles doped with antimony oxide, 0.10-2 wt% of a silicon compound, water and an organic solvent; (c) applying the coating mixture to the first metal oxide layer so as to form the second layer on the first layer; and (d) heating the second layer at a temperature ranging from 100 to 300°C.
摘要翻译：本发明涉及形成在玻璃的方法衬底的多层防水膜，其具有第一金属氧化物层和第二防水层，其包括以下步骤：（a）形成在玻璃基板上的第一金属氧化物层检查没有所述第一金属氧化物层具有在表面微坑和/或微小突起一个微小的粗糙表面; （B）制备的涂层混合物，其包括氟代烷基硅烷的0.10〜20％（重量），掺杂有氧化锑锡氧化物颗粒的0.10-2％（重量），的硅化合物，水和有机溶剂0.10-2％（重量）; （C）将所述涂层混合物到所述第一金属氧化物层，从而形成在第一层上的第二层; 和（d）在范围从100至300℃的温度下加热所述第二层

4. 发明授权

EP0825157B1 Water-repellent glass pane and method for producing same 失效
标题翻译：防水性玻璃板和它们的制备方法
公开(公告)号：EP0825157B1
公开(公告)日：2002-01-02
申请号：EP97114294.8
申请日：1997-08-19
申请人： CENTRAL GLASS COMPANY, LIMITED
发明人： Akamatsu, Yoshinori , Hamaguchi, Shigeo , Nishida, Yoshihiro , Yamamoto, Hideki
IPC分类号： C03C17/30 , B05D1/18
CPC分类号： C03C17/30 , C09K3/18 , Y10T428/315 , Y10T428/31525 , Y10T428/3154 , Y10T428/31612

5. 发明公开

EP0866037A3 Multilayered water-repellent film and method of forming same on glass substrate 失效
标题翻译：多层防水膜和处理其在玻璃基板上制备
公开(公告)号：EP0866037A3
公开(公告)日：1999-02-10
申请号：EP98110212.2
申请日：1994-11-10
申请人： CENTRAL GLASS COMPANY, LIMITED , NISSAN MOTOR CO., LTD.
发明人： Takahashi, Osamu , Hamaguchi, Shigeo , Otani, Michitaka , Nishida, Yoshihiro , Nakamura, Ichiro , Sugawara, Satoko , Kondo, Takeshi , Akamatsu, Yoshinori , Kai, Yasuaki
IPC分类号： C03C17/42
CPC分类号： C03C17/34 , C03C17/007 , C03C17/42 , C03C2217/445 , C03C2217/476 , C03C2217/76 , C03C2217/77 , Y10T428/24364 , Y10T428/24479 , Y10T428/24612 , Y10T428/31612 , Y10T428/31663
摘要： The invention relates to a method of forming on a glass substrate a multilayered water-repellent film having a first metal oxide layer and a second water-repellent layer, comprising the followings steps: (a) forming the first metal oxide layer on the glass substrate such that the first metal oxide layer has a minutely rough surface having on the surface micro-pits and/or micro-projections; (b) preparing a coating mixture comprising 0.10-20 wt% of a fluoroalkylsilane, 0.10-2 wt% of tin oxide particles doped with antimony oxide, 0.10-2 wt% of a silicon compound, water and an organic solvent; (c) applying the coating mixture to the first metal oxide layer so as to form the second layer on the first layer; and (d) heating the second layer at a temperature ranging from 100 to 300°C.
摘要翻译：本发明涉及的多层防水上通过溶胶 - 凝胶处理的玻璃基板的膜形成。该膜具有第一金属氧化物层中的所有其上通过溶胶 - 凝胶过程和形成在所述第一层上的第二防水层的玻璃基板形成的。作为用于提供给膜以防水性，机械强度和耐化学性的优异的耐久性的第一方法中，第一层是通过使用其分别从金属醇盐或金属乙酰丙酮制备了三种特定溶胶的混合物制备。作为用于提供给膜以上述优点的第二方法中，第二层是通过使用涂料混合物，其包括氟烷基硅烷制备，掺杂有锑的氧化，硅化合物，水和有机溶剂的氧化锡颗粒。作为用于提供给膜以上述优点的第三方法中，第二层是通过使用另一种涂料混合物，其包括氟烷基硅烷制备，掺杂有锑的氧化，硅化合物，水，有机和酸溶剂的氧化锡颗粒。

6. 发明授权

EP0891953B1 Glass plate with water-repellent film and method for producing same 失效
标题翻译：玻璃板用斥水涂层和工艺及其制备
公开(公告)号：EP0891953B1
公开(公告)日：2006-01-11
申请号：EP97112061.3
申请日：1997-07-15
申请人： CENTRAL GLASS COMPANY, LIMITED
发明人： Akamatsu, Yoshinori , Yuasa, Akira , Yamamoto, Hideki
IPC分类号： C03C17/30 , C03C17/42 , C08J7/04
CPC分类号： C03C17/42 , C03C2217/76

7. 发明公开

EP0891953A1 Glass plate with water-repellent film and method for producing same 失效
标题翻译： ung ung ung ung ung ung ung ung ung ung ung ung ung ung ung ung ung
公开(公告)号：EP0891953A1
公开(公告)日：1999-01-20
申请号：EP97112061.3
申请日：1997-07-15
申请人： CENTRAL GLASS COMPANY, LIMITED
发明人： Akamatsu, Yoshinori , Yuasa, Akira , Yamamoto, Hideki
IPC分类号： C03C17/30 , C03C17/42 , C08J7/04
CPC分类号： C03C17/42 , C03C2217/76
摘要： The invention relates to a water-repellent glass plate having a glass substrate; a first film which is formed on the glass substrate and is made of silica; and a water-repellent second film formed on the first film. This glass plate is prepared by a method including steps of: (1) applying a first coating liquid containing tetraisocyanate silane to the glass substrate, thereby to form thereon a precursory film; and (2) subjecting the precursory film to a drying at room temperature or to a heat treatment, thereby to prepare the first film; and (3) applying a second coating liquid to the first film, thereby to form the second film on the first film. The tetraisocyanate silane of the step (1) is curable at room temperature. The second coating liquid contains an alkoxysilane having at least one fluorocarbon group substituted for at least one hydrogen atom thereof. By the provision of the first film, the water-repellent second film becomes superior in solar resistance, abrasion resistance, chemical resistance, and adhesion to the glass substrate.
摘要翻译：本发明涉及一种具有玻璃基板的防水玻璃板; 形成在玻璃基板上并由二氧化硅制成的第一膜; 以及形成在第一膜上的防水第二膜。该玻璃板通过以下步骤制备：（1）将含有四异氰酸酯硅烷的第一涂布液涂布在玻璃基板上，由此在其上形成前体膜; 和（2）在室温下对前体膜进行干燥或热处理，由此制备第一膜; 和（3）将第二涂布液施加到第一膜上，从而在第一膜上形成第二膜。步骤（1）的四异氰酸酯硅烷在室温下是可固化的。第二涂布液含有至少一个氟代烃基取代至少一个氢原子的烷氧基硅烷。通过设置第一膜，防水性第二膜在耐太阳能，耐磨性，耐化学性和与玻璃基板的粘附性方面变得优异。

8. 发明公开

EP0825157A3 Water-repellent glass pane and method for producing same 失效
标题翻译：防水玻璃板及其制造方法
公开(公告)号：EP0825157A3
公开(公告)日：1998-08-19
申请号：EP97114294.8
申请日：1997-08-19
申请人： CENTRAL GLASS COMPANY, LIMITED
发明人： Akamatsu, Yoshinori , Hamaguchi, Shigeo , Nishida, Yoshihiro , Yamamoto, Hideki
IPC分类号： C03C17/30 , B05D1/18
CPC分类号： C03C17/30 , C09K3/18 , Y10T428/315 , Y10T428/31525 , Y10T428/3154 , Y10T428/31612
摘要： The invention relates to a water-repellent glass pane having a glass substrate and a water-repellent film formed thereon. This glass pane is prepared by a first or second method. The first method includes sequential steps of (a) mixing together a raw material for producing the water-repellent film, an organic solvent for diluting the raw material, and water for hydrolyzing the raw material, such that the raw material is subjected to hydrolysis and then to dehydration and polycondensation, thereby to turn a mixture of the raw material, the organic solvent and the water into a sol; (b) adjusting water content of the sol, thereby to prepare a coating liquid; and (c) applying the coating liquid to the glass substrate, in an atmosphere having a first temperature and a relative humidity. The second method includes sequential steps of: (a) subjecting a surface of the glass substrate to an abrasive treatment; (b) subjecting the surface of the glass substrate to an acid treatment; and (c) applying a coating liquid to the surface of the glass substrate. The glass pane prepared by the first or second method is superior in abrasion resistance, sunshine resistance, hardness, adhesion to the glass substrate, and water-repellency for a long time.
摘要翻译：本发明涉及一种具有玻璃基板和形成在其上的防水膜的防水玻璃板。该玻璃板通过第一种或第二种方法制备。第一种方法包括以下顺序步骤：（a）将用于制造防水膜的原材料，用于稀释原材料的有机溶剂和用于水解原材料的水混合在一起，使得原材料经受水解并且然后进行脱水和缩聚，从而将原料，有机溶剂和水的混合物转化为溶胶; （b）调节溶胶的含水量，从而制备涂布液; 和（c）在具有第一温度和相对湿度的气氛中将涂布液施涂到玻璃基材上。第二种方法包括以下顺序步骤：（a）使玻璃基材的表面经受研磨处理; （b）对玻璃基板的表面进行酸处理; 和（c）将涂布液施加到玻璃基材的表面上。通过第一或第二种方法制备的玻璃板在耐磨性，抗日光性，硬度，对玻璃基材的粘合性和长期的防水性方面优异。

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