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1. 发明公开

EP2516335A2 RE-USE OF SURFACTANT-CONTAINING FLUIDS 审中-公开
标题翻译：回用油液的表面活性剂
公开(公告)号：EP2516335A2
公开(公告)日：2012-10-31
申请号：EP10842708.9
申请日：2010-12-21
申请人： Baker Hughes Incorporated
发明人： CREWS, James, B. , HUANG, Tianping
IPC分类号： C02F1/28 , B01D15/00 , C02F1/58
CPC分类号： B01J20/041 , B01J20/0211 , B01J20/0244 , B01J20/06 , B01J20/08 , B01J20/12 , B01J20/18 , B01J20/20 , B01J20/205 , B01J20/28004 , B01J20/28007 , B01J20/3204 , B01J20/3236 , B01J20/3289 , B01J20/3408 , B01J20/3416 , B01J20/3433 , B01J20/3475 , B01J2220/46 , B01J2220/66 , B82Y30/00 , C02F1/281 , C02F1/288 , C02F2305/08
摘要： The components of surfactant-laden fluids, such as those used in hydrocarbon recovery operations such as for stimulation, e.g. hydraulic fracturing, may be re-used and re-cycled into components for subsequent use in a wide range of similar or different operational fluids. In particular, aqueous fluids gelled with viscoelastic surfactants and having components therein to pseudo-crosslink the elongated VES micelles and for internal breaking may be separated into its component parts by relatively inexpensive methods such as filtration. One filtration method includes contacting the surfactant- containing fluid with a particle pack having particulate additives therein which filter out or extract fine solids from the fluid. In an alternate embodiment the surfactant-laden fluid is a nano- and/or micro-emulsion wellbore cleanup fluid.

2. 发明公开

EP2134805A1 COMPOSITIONS AND METHODS FOR WATER AND GAS SHUT-OFF IN SUBTERRANEAN WELLS WITH VES FLUIDS 有权
标题翻译：水和气体组合物和方法切断。与VES流体地下HOLES
公开(公告)号：EP2134805A1
公开(公告)日：2009-12-23
申请号：EP08732575.9
申请日：2008-03-20
申请人： Baker Hughes Incorporated
发明人： HUANG, Tianping , CREWS, James, B. , WILLINGHAM, John, R.
IPC分类号： C09K8/504 , C09K8/506
CPC分类号： C09K8/506 , C09K8/5045
摘要： Viscoelastic surfactant (VES) based fluid systems for zone isolation and flow control are effective in water and/or gas shutoff applications. The fluid systems may include brine, a viscosity enhancer, as well as the VES, and optionally a stabilizer for high temperature applications. The stabilizer may be an alkali earth metal oxide, alkali earth metal hydroxide, alkali metal oxide, alkali metal hydroxide, AI2O3, and mixtures thereof. The viscosity enhancer may include pyroelectric particles, piezoelectric particles, and mixtures thereof. The fluid system is easy to pump into the formation, and after pumping, the fluid system will generate very high viscosities to prevent the VES fluid from flowing back to stop undesirable water and/or gas production.

3. 发明公开

EP2125990A2 METHODS AND COMPOSITIONS FOR FRACTURING SUBTERRANEAN FORMATIONS 审中-公开
标题翻译：方法和组合物打破地下岩层
公开(公告)号：EP2125990A2
公开(公告)日：2009-12-02
申请号：EP08732436.4
申请日：2008-03-19
申请人： BAKER HUGHES INCORPORATED
发明人： CREWS, James, B. , HUANG, Tianping , WILLINGHAM, John, R. , TREADWAY, James, H. , GABRYSCH, Allen, D. , KELLY, Patrick, A. , WOOD, William, R.
IPC分类号： C09K8/60 , C09K8/68
CPC分类号： C09K8/68 , C09K8/602 , C09K2208/24 , C09K2208/26 , C09K2208/30
摘要： Viscoelastic surfactant (VES) gelled aqueous fluids containing water, a VES, an internal breaker, a VES stabilizer, a fluid loss control agent and a viscosity enhancer are useful as treating fluids and particularly as fracturing fluids for subterranean formations. These VES-based fluids have faster and more complete clean-up than polymer-based fracturing fluids. The use of an internal breaker permits ready removal of the unique VES micelle based pseudo- filter cake with several advantages including reducing the typical VES loading and total fluid volume since more VES fluid stays within the fracture, generating a more optimum fracture geometry for enhanced reservoir productivity, and treating reservoirs with permeability above the present VES limit of approximately 400 md to at least 2000 md.

4. 发明公开

EP2111434A2 ORGANIC ACID TREATING FLUIDS WITH VISCOELASTIC SURFACTANTS AND INTERNAL BREAKERS 有权
标题翻译：有机酸和粘弹性表面和内部交换机处理液
公开(公告)号：EP2111434A2
公开(公告)日：2009-10-28
申请号：EP08728149.9
申请日：2008-01-23
申请人： BAKER HUGHES INCORPORATED
发明人： HUANG, Tianping , CREWS, James, B.
IPC分类号： C09K8/72 , C09K8/60
CPC分类号： C09K8/74 , C09K8/602 , C09K2208/26 , C09K2208/30 , Y10S507/921
摘要： An aqueous fluid system that contains an aqueous dicarboxylic acid solution, a viscoelastic surfactant as a gelling agent to increase the viscosity of the fluid, and an internal breaker such as mineral oil and/or fish oil to controllably break the viscosity of the fluid provides a self-diverting acid treatment of subterranean formations. The internal breaker may be at least one mineral oil, a polyalphaolefin oil, a saturated fatty acid, and/or is an unsaturated fatty acid. The VES gelling agent does not yield viscosity until the organic acid starts to spend. Full viscosity yield of the VES gelling agent typically occurs at about 6.0 pH. The internal breaker allows the VES gelling agent to fully viscosify the spent organic acid at 6.0 pH and higher, but as the spent-acid VES gelled fluid reaching reservoir temperature, controllable break of the VES fluid viscosity over time can be achieved.

5. 发明公开

EP2981671A1 METHOD TO GENERATE DIVERSION AND DISTRIBUTION FOR UNCONVENTIONAL FRACTURING IN SHALE 审中-公开
标题翻译：工艺的用于制造石板非常规BREAK教育分流，而且分布
公开(公告)号：EP2981671A1
公开(公告)日：2016-02-10
申请号：EP14779550.4
申请日：2014-03-27
申请人： Baker Hughes Incorporated
发明人： CREWS, James, B.
IPC分类号： E21B43/22 , C09K8/58
CPC分类号： E21B43/267 , C09K8/62 , C09K8/80 , E21B21/062 , E21B43/26
摘要： Relatively high viscosity materials and methods for introducing them as discrete bodies or masses into relatively low viscosity fluids, such as brine, give fracturing fluids that help control the diversion and distribution of fluids as they are pumped downhole against a subterranean formation, particularly shale, to fracture it. A wide range of relatively viscous materials may be used, including polymers, crosslinked polymers and/or surfactant gels, for instance gels created with viscoelastic surfactants (VESs). Once the fracturing fluids containing these bodies or masses are within the hydraulic fracture, the processes of paths of least resistance, flow deviation, viscous material flow displacement, total fluid diversion,
in situ fluid viscosity generation and distribution of delayed release treatment additives may be deployed.

6. 发明公开

EP2494002A2 DRILL-IN FLUIDS FOR OIL AND GAS RESERVOIRS WITH HIGH CARBONATE CONTENTS 无效
标题翻译：钻井液对于高碳酸酯部分油气藏
公开(公告)号：EP2494002A2
公开(公告)日：2012-09-05
申请号：EP10828768.1
申请日：2010-10-19
申请人： Baker Hughes Incorporated
发明人： HUANG, Tianping , CREWS, James, B. , WILLINGHAM, John, R.
IPC分类号： C09K8/60 , C09K8/66 , C09K8/02 , E21B43/26
CPC分类号： C09K8/12 , C09K8/506 , C09K8/524 , C09K2208/26 , C09K2208/30
摘要： Compositions including relatively low reactivity acids, mixed with viscoelastic surfactants (VESs) and internal breakers may serve as drilling fluids to open underground hydrocarbon reservoirs with carbonate contents of 10 wt % or above. The drilling fluids have low viscosities in the drilling pipe. After the fluid flows out of the drill bit, the acids react with carbonates in the formation thereby increasing the pH of the drilling fluids causing the VES to gel the fluid at the bottom of the hole and the downhole annulus between the drilling pipe and the formation rock. The viscosified drilling fluid will reduce fluid loss and will carry no dissolved drilling debris to the surface. After drilling through the targeted formation, the internal breakers in the viscosified drilling fluids will break down the fluids to permit their removal, and the well is ready to produce with very little or no near well bore damage.

7. 发明公开

EP2297266A2 SUSPENSION OF CONCENTRATED PARTICULATE ADDITIVES CONTAINING OIL FOR FRACTURING AND OTHER FLUIDS 审中-公开
标题翻译：含油的浓缩颗粒添加剂悬浮在压裂液和其他流体中
公开(公告)号：EP2297266A2
公开(公告)日：2011-03-23
申请号：EP09751076.2
申请日：2009-04-15
申请人： Baker Hughes Incorporated
发明人： HUANG, Tianping , CREWS, James, B.
IPC分类号： C09K8/04 , C09K8/52
CPC分类号： C09K8/5045 , C09K8/506 , C09K8/516 , C09K2208/30
摘要： The handling, transport and delivery of particulate materials, particularly fine particles, may be difficult. Alkaline earth metal oxide particles such as magnesium oxide (MgO) may be suspended in glycerin and/or alkylene glycols such as propylene glycol up to loadings of 51 wt%. Such suspensions or slurries make it easier to deliver MgO and similar agents into fluids, such as aqueous fluids gelled with viscoelastic surfactants (VES). These concentrated suspensions or slurries may be improved in their stability by the inclusion of minor amounts of a vegetable oil and/or a fish oil The MgO serves as stabilizers and/or fluid loss control agents for VES-gelled fluid used to treat subterranean formations,
e.g . for well completion or stimulation in hydrocarbon recovery operations. The particle size of the magnesium oxide or other agent may be between 1 nanometer to 0.4 millimeter.
摘要翻译：颗粒材料特别是细颗粒的处理，运输和输送可能是困难的。碱土金属氧化物颗粒例如氧化镁（MgO）可以悬浮在甘油和/或亚烷基二醇如丙二醇中，直至负载量为51重量％。这种悬浮液或浆液使得将MgO和类似的试剂输送到流体中变得更容易，所述流体例如用粘弹性表面活性剂（VES）凝胶化的含水流体。通过加入少量的植物油和/或鱼油，可以提高这些浓缩悬浮液或浆液的稳定性。MgO用作用于处理地下地层的VES凝胶化流体的稳定剂和/或流体损失控制剂，例如用于油气回收作业的完井或增产。氧化镁或其他试剂的粒度可以在1纳米至0.4毫米之间。

8. 发明公开

EP2197977A1 NANO-SIZED PARTICLE-COATED PROPPANTS FOR FORMATION FINES FIXATION IN PROPPANT PACKS 有权
标题翻译：纳米粒子涂覆的支撑是指构成一个罚款固定支撑装置套餐
公开(公告)号：EP2197977A1
公开(公告)日：2010-06-23
申请号：EP08867707.5
申请日：2008-10-23
申请人： Baker Hughes Incorporated
发明人： HUANG, Tianping , CREWS, James, B. , WILLINGHAM, John, R. , PACE, James, R. , BELCHER, Christopher, K.
IPC分类号： C09K8/80 , C09K8/68 , C09K8/66 , C09K8/516
CPC分类号： C09K8/516 , C09K8/665 , C09K8/68 , C09K8/805 , E21B43/267
摘要： A fracturing fluid, gravel pack fluid and/or frac pack fluid containing particles such as proppants, gravel and/.or sand, may contain an effective amount of a nano-sized particulate additive to fixate or reduce fines migration, where the particulate additive is an alkaline earth metal oxide, alkaline earth metal hydroxide, alkali metal oxides, alkali metal hydroxides transition metal oxides, transition metal hydroxides, post-transition metal oxides, post-transition metal hydroxides piezoelectric crystals and pyroelectric crystals. The nano-sized particulate additive is bound to the particles with a coating agent such as an oil. The particle size of the magnesium oxide or other agent may be nanometer scale, which scale may provide unique particle charges that help fixate the formation fines. The carrier fluid used in the treating fluid may be aqueous, brine, alcoholic or hydrocarbon- based.

9. 发明公开

EP2430111A2 METHODS OF USING VISCOELASTIC SURFACTANT GELLED FLUIDS TO PRE-SATURATE UNDERGROUND FORMATIONS 审中-公开
标题翻译：使用粘弹性表面活性流体的方法胶凝海底地层以presaturate
公开(公告)号：EP2430111A2
公开(公告)日：2012-03-21
申请号：EP10772622.6
申请日：2010-04-30
申请人： Baker Hughes Incorporated
发明人： HUANG, Tianping , CREWS, James, B. , WILLINGHAM, John, Robert
IPC分类号： C09K8/584
CPC分类号： C09K8/602 , C09K8/506 , C09K8/68 , C09K2208/10 , C09K2208/26 , C09K2208/30
摘要： Viscoelastic surfactant (VES) based fluid systems are effective to pre-saturate high permeability subterranean formations prior to a treatment operation that would undesirably suffer from high fluid leakoff. The fluid systems may include brine, a viscosity enhancer, as well as the VES, and a high temperature stabilizer. The stabilizer may be an alkaline earth metal oxide, alkaline earth metal hydroxide, alkali metal oxide, alkali metal hydroxide, Al
2 O
3 , and mixtures thereof. The viscosity enhancer may include pyroelectric particles, piezoelectric particles, and mixtures thereof. The fluid system is easy to pump into the formation, and after initial pumping, the fluid system will soak into and occupy or "pre-saturate" the pores of the formation prior to pumping of a second treating fluid for fracturing, gravel packing, frac-packing, and the like. The methods are practiced in the absence of acids typically used in acidizing operations, such as hydrochloric acid and hydrofluoric acid.

10. 发明授权

EP1869285B1 COMPOSITIONS AND USE OF MONO-AND POLYENOIC ACIDS FOR BREAKING VES-GELLED FLUIDS 失效转让
标题翻译：成分与单和多烯酸的使用，打破从与粘弹性表面活性胶状流体
公开(公告)号：EP1869285B1
公开(公告)日：2009-03-04
申请号：EP06738691.2
申请日：2006-03-16
申请人： Baker Hughes Incorporated
发明人： CREWS, James, B.
IPC分类号： E21B43/267 , E21B43/25 , C09K8/00
CPC分类号： C09K8/68 , C09K8/602 , C09K2208/26 , C09K2208/30
摘要： Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities reduced (gels broken) by the direct or indirect action of a composition that contains at least one unsaturated fatty acid, such as a monoenoic acid and/ or polyenoic acid. The unsaturated fatty acid may be contained in an oil-soluble internal phase of the fluid. The breaking composition is believed to act possibly by rearranging, disaggregating or otherwise attacking the micellar structure of the VES-gelled fluid. In a specific, non-limiting instance, a brine fluid gelled with an amine oxide surfactant can have its viscosity broken with an oil such as flax (linseed) oil, soybean oil and/or fish oils containing relatively high amounts of unsaturated fatty acids. The unsaturated fatty acids are thought to auto-oxidize into products such as aldehydes, ketones and saturated fatty acids that break the VES gel.

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