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1. 发明公开

EP1713777A1 VERFAHREN ZUR HERSTELLUNG VON TERRYLEN-3,4:11,12-TETRACARBONSÄUREDIIMIDEN 审中-公开
标题翻译：用于生产涤纶-3,4：11,12四甲
公开(公告)号：EP1713777A1
公开(公告)日：2006-10-25
申请号：EP05700915.1
申请日：2005-01-14
申请人： BASF Aktiengesellschaft , MPG Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.
发明人： KÖNEMANN, Martin , MÜLLEN, Klaus , REUTHER, Erik
IPC分类号： C07D221/14 , C07D221/18
CPC分类号： C07D221/14 , C07D221/18 , C07D471/06
摘要： The invention relates to a method for producing terrylen-3,4:11,12-tetracarboxylic acid diimids of general formula (I), wherein R and R' are independently hydrogen, possibly substituted C1-C30-alkyl, C5-C8-cycloalkyl, aryl or hetaryl consisting in a) reacting a diboran (II) in the presence an aprotic organic solvent, a transition metal-based catalyst and a base with a1) a 9-brom-perylen-3,4-dicarboxyl acid imid (IIIa) or a2) a naphthalene-1,8-dicarboxylic-acid imid (IIIb), b1) in submitting a formed 9-(dioxaborolan-2-yl)perylene-3,4-dicarboxylic acid imid (IVa) in the presence of an organic solvent preferably mixed with water, a transition metal-based catalyst and a base to a Suzuki-coupling reaction with a naphthalene-1,8-dicarboxylic carbon imid (IIIb) or b2) a submitting a formed 4-(dioxaborolan-2-yl)naphthalene-1,8-dicarboxylic acid imid (IVb) in the presence of an organic solvent preferably mixed with water, a transition metal-based catalyst and a base to a Suzuki-coupling reaction with a 9-brom-perylen-3,4-dicarbon acid imid (IIIa) and c)in transforming a formed 9-(4-naphthalene-1,8-dicarboxylic acid imid) perylene-3,4-dicarboxylic acid imid (V) into the terrylen-3,4:11,12-tetracarbon acid di-imid base (I) by cyclodehydration in an organic reaction medium exhibiting hydroxy and amino functions and containing a substantially insoluble base.

2. 发明授权

EP1373214B1 RYLENDERIVATE UND DEREN VERWENDUNG ALS FARBSTOFFE 有权
标题翻译：嵌苯衍生物及其作为染料使用
公开(公告)号：EP1373214B1
公开(公告)日：2007-08-22
申请号：EP02716770.9
申请日：2002-02-14
申请人： BASF Aktiengesellschaft , Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.
发明人： KRIEGER, Matthias , BÖHM, Arno , REUTHER, Erik , MÜLLEN, Klaus
IPC分类号： C07D221/18 , C07D491/06 , C09B3/14 , C09B3/18 , C09B3/20
CPC分类号： C07D491/06 , C07D221/18 , C07D471/06 , C09B5/62
摘要： The invention relates to rylene derivatives of the general formula (I), in which: R represents hydrogen or optionally substituted C1-C30 alkyl, aryl or heteroaryl; R1 represents hydrogen or bromine; R2 represents hydrogen or C¿1?-C6 alkyl; R?3¿ represents hydrogen, C¿1?-C18 alkyl or optionally substituted aryl or heteroaryl; and n represents 2 or 3.

3. 发明授权

EP1513841B1 1,6,9,14-TETRASUBSTITUIERTE TERRYLENTETRACARBONS UREDIIMIDE 有权
标题翻译：尿嘧啶
公开(公告)号：EP1513841B1
公开(公告)日：2008-05-14
申请号：EP03735536.9
申请日：2003-06-04
申请人： BASF SE , Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.
发明人： BÖHM, Arno , KRIEGER, Matthias , REUTHER, Erik , MÜLLEN, Klaus
IPC分类号： C07D471/06 , C09B5/62
CPC分类号： C07D471/06 , C09B5/62
摘要： The invention relates to 1,6,9,14-tetrasubstituted terrylene tetracarboxylic acid diimides of general formula (I), in which the variables are defined as follows: X, Y independently of one another represent bromium; cyano; aryloxy, arylthio, hetaryloxy or hetarylthio, which can respectively be mono- or polysubstituted by C1-C12 alkyl, C1-C12 alkoxy, -COOR , -SO3R , halogen, hydroxy, carboxy, cyano, -CONHR and/or -NHCOR ; a group of formula -L-R ; a group of formula -NR 2; R, R' independently of one another represent hydrogen; C1-C30 alkyl, whose carbon chain can be interrupted by one or more groupings -O-, -S-, -NR1-, -CO- and/or -SO2- and which can be mono- or polysubstituted by cyano, C1-C6 alkoxy, aryl, which may be substituted by C1-C18 alkyl or C1-C6 alkoxy and/or a 5- to 7-membered heterocyclic group that is bonded by means of a nitrogen atom and that can contain additional heteroatoms and be aromatic; C5-C8 cycloalkyl, whose carbon skeleton can be interrupted by one or more groupings -O-, -S- and/or -NR - and/or which can be mono- or polysubstituted by C1-C6 alkyl; aryl or hetaryl, which can be mono- or polysubstituted by C1-C18 alkyl, C1-C6 alkoxy, cyano, -CONHR , -NHCOR and/or aryl- or hetarylazo, which can be respectively substituted by C1-C10 alkyl, C1-C6 alkoxy or cyano; and L represents 1,2-ethylene, 1,2-ethenylene or 1,2-ethynylene.

4. 发明公开

EP1373214A1 RYLENDERIVATE UND DEREN VERWENDUNG ALS FARBSTOFFE 有权
标题翻译：嵌苯衍生物及其作为染料使用
公开(公告)号：EP1373214A1
公开(公告)日：2004-01-02
申请号：EP02716770.9
申请日：2002-02-14
申请人： BASF AKTIENGESELLSCHAFT , Max-Planck-Gesellschaft zur Förderungder Wissenschaften e.V.
发明人： KRIEGER, Matthias , BÖHM, Arno , REUTHER, Erik , MÜLLEN, Klaus
IPC分类号： C07D221/18 , C07D491/06 , C09B3/14 , C09B3/18 , C09B3/20
CPC分类号： C07D491/06 , C07D221/18 , C07D471/06 , C09B5/62
摘要： The invention relates to rylene derivatives of the general formula (I), in which: R represents hydrogen or optionally substituted C1-C30 alkyl, aryl or heteroaryl; R1 represents hydrogen or bromine; R2 represents hydrogen or C¿1?-C6 alkyl; R?3¿ represents hydrogen, C¿1?-C18 alkyl or optionally substituted aryl or heteroaryl; and n represents 2 or 3.

5. 发明公开

EP1513841A1 1,6,9,14-TETRASUBSTITUIERTE TERRYLENTETRACARBONS UREDIIMIDE 有权
公开(公告)号：EP1513841A1
公开(公告)日：2005-03-16
申请号：EP03735536.9
申请日：2003-06-04
申请人： BASF AKTIENGESELLSCHAFT , Max-Planck-Gesellschaft zur Förderungder Wissenschaften e.V.
发明人： BÖHM, Arno , KRIEGER, Matthias , REUTHER, Erik , MÜLLEN, Klaus
IPC分类号： C07D471/06 , C09B5/62
CPC分类号： C07D471/06 , C09B5/62
摘要： The invention relates to 1,6,9,14-tetrasubstituted terrylene tetracarboxylic acid diimides of general formula (I), in which the variables are defined as follows: X, Y independently of one another represent bromium; cyano; aryloxy, arylthio, hetaryloxy or hetarylthio, which can respectively be mono- or polysubstituted by C1-C12 alkyl, C1-C12 alkoxy, -COOR , -SO3R , halogen, hydroxy, carboxy, cyano, -CONHR and/or -NHCOR ; a group of formula -L-R ; a group of formula -NR 2; R, R' independently of one another represent hydrogen; C1-C30 alkyl, whose carbon chain can be interrupted by one or more groupings -O-, -S-, -NR1-, -CO- and/or -SO2- and which can be mono- or polysubstituted by cyano, C1-C6 alkoxy, aryl, which may be substituted by C1-C18 alkyl or C1-C6 alkoxy and/or a 5- to 7-membered heterocyclic group that is bonded by means of a nitrogen atom and that can contain additional heteroatoms and be aromatic; C5-C8 cycloalkyl, whose carbon skeleton can be interrupted by one or more groupings -O-, -S- and/or -NR - and/or which can be mono- or polysubstituted by C1-C6 alkyl; aryl or hetaryl, which can be mono- or polysubstituted by C1-C18 alkyl, C1-C6 alkoxy, cyano, -CONHR , -NHCOR and/or aryl- or hetarylazo, which can be respectively substituted by C1-C10 alkyl, C1-C6 alkoxy or cyano; and L represents 1,2-ethylene, 1,2-ethenylene or 1,2-ethynylene.
摘要翻译：本发明涉及通式（I）的1,6,9,14-四取代的三萘嵌苯四羧酸二酰亚胺，其中变量定义如下：X，Y彼此独立地代表溴; 氰基; 芳氧基，芳硫基，杂芳氧基或杂芳硫基，其可以分别被C 1 -C 12烷基，C 1 -C 12烷氧基，-COOR 1，-SO 3 R 1，卤素，羟基，羧基，氰基，-CONHR 2和/或-NHCOR 2; 式-L-R 3的基团; 式-NR 2 2的基团; R，R'彼此独立地代表氢; 其碳链可以被一个或多个基团-O - ， - S - ， - NR 1 - ， - CO-和/或-SO 2 - 中断并且可以被氰基单取代或多取代的C 1 -C 30烷基， C6烷氧基，芳基，其可以被C1-C18烷基或C1-C6烷氧基和/或5-7元杂环基团取代，所述杂环基团借助氮原子键合并且可以包含额外的杂原子并且是芳族的; C5-C8环烷基，其碳骨架可以被一个或多个基团-O-，-S-和/或-NR1-打断和/或可以被C1-C6烷基单取代或多取代; 芳基或杂芳基，其可以被C1-C18烷基，C1-C6烷氧基，氰基，-CONHR2，-NHCOR2和/或芳基或杂芳基偶氮单或多取代，它们可以分别被C1 -C10烷基，C1-C6烷氧基或氰基; L代表1,2-亚乙基，1,2-亚乙烯基或1,2-亚乙炔基。

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