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1. 发明公开

EP3187478A1 METHOD FOR PRODUCING HYDROFLUOROOLEFIN 审中-公开
标题翻译：生产氢氟烯烃的方法
公开(公告)号：EP3187478A1
公开(公告)日：2017-07-05
申请号：EP15836384.6
申请日：2015-08-24
申请人： Asahi Glass Company, Limited
发明人： WANG, Xu , TERAZONO, Shinji , KANDA, Masahiro , KAWAGUCHI, Satoshi , KASAGAWA, Mitsugu
IPC分类号： C07C17/23 , C07C21/18 , C07B61/00
CPC分类号： C07C17/23 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/46 , B01J23/462 , B01J23/464 , B01J23/468 , B01J23/48 , B01J23/50 , B01J23/52 , B01J23/72 , C07B61/00 , C07C17/354 , C07C21/18
摘要： A method for producing a hydrofluoroolefin, which comprises reacting a chlorofluoroolefin represented by the following formula (1) with hydrogen in the presence of a platinum group metal catalyst supported on a carbon carrier, to obtain a hydrofluoroolefin represented by the following formula (2),
wherein the carbon carrier has acidic functional groups, and the total acidic functional group amount in the carbon carrier is at most 50 µmol/g:

CZX=CClY (1)

wherein X is F or Cl, Y is F, Cl or H, and Z is F or CF 3 ;

CZX'=CHY' (2)

wherein X' is F when X is F, or X' is H when X is Cl, Y' is F when Y is F, or Y' is H when Y is Cl or H, and Z is the same as Z in the formula (1).
摘要翻译：一种氢氟烯烃的制造方法，其特征在于，在负载在碳载体上的铂族金属催化剂的存在下，使下述式（1）所示的氯氟烯烃与氢反应，得到下述式（2）所示的氢氟烯烃，其中所述碳载体具有酸性官能团，并且所述碳载体中的总酸性官能团量为至多50μmol/ g：CZX = CClY（1）其中X为F或Cl，Y为F，Cl或H，和 Z是F或CF 3; CZX'= CHY'（2）其中当X是F时X'是F，或当X是Cl时X'是H，当Y是F时Y'是F或当Y是Cl或H时Y'是H， Z与式（1）中的Z相同。

2. 发明公开

EP3187477A1 PROCESS FOR PRODUCING HYDROFLUOROOLEFIN 审中-公开
标题翻译：生产氢氟烯烃的方法
公开(公告)号：EP3187477A1
公开(公告)日：2017-07-05
申请号：EP15835895.2
申请日：2015-08-24
申请人： Asahi Glass Company, Limited
发明人： TERAZONO, Shinji , WANG, Xu , KANDA, Masahiro , KAWAGUCHI, Satoshi , KASAGAWA, Mitsugu
IPC分类号： C07C17/23 , C07C21/18 , C07B61/00
CPC分类号： C07C17/23 , C07B61/00 , C07C17/354 , C07C21/18
摘要： To provide a method for producing a hydrofluoroolefin, wherein formation of an over-reduced product having hydrogen added to a material chlorofluoroolefin and an over-reduced product having not only chlorine atoms but also fluorine atoms in the chlorofluoroolefin replaced with hydrogen atoms, as by-products, is suppressed.
A method for producing a hydrofluoroolefin, which comprises reacting a specific chlorofluoroolefin with hydrogen in the presence of a catalyst supported on a carrier, to obtain a specific hydrofluoroolefin,
wherein the catalyst is a catalyst composed of an alloy containing at least one platinum group element selected from the group consisting of palladium and platinum, and at least one second element selected from the group consisting of manganese, copper, aluminum, gold, lithium, sodium, potassium, magnesium, silver, zinc, cadmium, indium, silicon, germanium, tin, lead, arsenic, antimony and bismuth.
摘要翻译：本发明提供一种氢氟烯烃的制造方法，其中，在原料氯氟烯烃中添加氢的过量还原物和氯原子中不仅含有氯原子而且还含有氟原子的过度还原物被氢原子取代而成为副产物，产品，被压制。一种氢氟烯烃的制造方法，其特征在于，在负载在载体上的催化剂的存在下，使特定的氯氟烯烃与氢反应，得到特定的氢氟烯烃，其中，催化剂是由含有选自至少一种铂族元素选自由锰，铜，铝，金，锂，钠，钾，镁，银，锌，镉，铟，硅，锗，锡组成的组中的至少一种第二元素，铅，砷，锑和铋。

3. 发明公开

EP3228611A1 METHOD FOR PRODUCING HYDROFLUOROOLEFIN 审中-公开
标题翻译：生产氢氟烯烃的方法
公开(公告)号：EP3228611A1
公开(公告)日：2017-10-11
申请号：EP15864619.0
申请日：2015-12-01
申请人： Asahi Glass Company, Limited
发明人： WANG, Xu , TERAZONO, Shinji , HAYASAKA, Yuki , SUZUKI, Toshio , KAWAGUCHI, Satoshi , KASAGAWA, Mitsugu
IPC分类号： C07C17/23 , C07C21/18 , B01J23/52 , C07B61/00
CPC分类号： C07C17/23 , B01J21/18 , B01J23/44 , B01J23/52 , B01J35/0006 , B01J35/0073 , B01J35/026 , B01J37/08 , C07C21/18
摘要： To provide a method for producing a hydrofluoroolefin, wherein formation of an over-reduced product having hydrogen added to an aimed hydrofluorolefin and an over-reduced product having some of fluorine atoms in the aimed product replaced with hydrogen atoms, as by-products, is suppressed.
A method for producing a hydrofluoroolefin, which comprises reacting a specific chlorofluoroolefin with hydrogen in the presence of a catalyst supported on a carrier, to obtain a specific hydrofluoroolefin, wherein the catalyst is a catalyst composed of particles of an alloy containing at least one platinum group metal selected from the group consisting of palladium and platinum, and gold, and the proportion of the gold at the surface of the alloy particles is from 5 to 30 mass% per 100 mass% in total of the platinum group metal and the gold at the surface of the alloy particles.
摘要翻译：提供一种氢氟烯烃的制造方法，其特征在于，在目标氢氟烯烃中添加了氢的过度还原物和由氢原子取代的目标物中的一部分氟原子作为副产物形成的过还原物是抑制。一种氢氟烯烃的制造方法，其特征在于，在载体上负载催化剂的条件下，使特定的氯氟烯烃与氢反应，得到特定的氢氟烯烃，其中，催化剂是由含有至少一个铂基团的合金选自由钯和铂组成的组中的金属和金，并且合金颗粒表面上的金的比例为每100质量％铂族金属和金的总和为5至30质量％合金颗粒的表面。

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