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    • 7. 发明公开
    • A METHOD OF PRUSSIAN BLUE DRESS ELECTRODE
    • VERFAHREN ZUR HERSTELLUNG EINER PREUSSISCHBLAU-ELEKTRODE
    • EP2420827A1
    • 2012-02-22
    • EP09843214.9
    • 2009-04-16
    • Nanjing University of Technology
    • JIN, WanqinCHU, ZhenyuLIU, YuXU, Nanping
    • G01N27/30
    • G01N27/30
    • A method of Prussian blue dress electrode is provided. The method includes: a based substrate is surface preprocessed; the preprocessed electrode is mounted in aerosol deposition box; an anion solution and KCl water solution are prepared, a cationic solution and KCl water solution are prepared, two have the same concentration; the anion solution is K 4 Fe(CN) 6 or K 3 Fe(CN) 6 solution, the cationic solution is FeCl 3 or (NH 4 )Fe(SO 4 ) 2 solution; the prepared anion solution and KCl water solution are loaded into an ultrasonic atomizer, the solution is ultrasonic atomized to aerosol, then the solution is pressed in the aerosol deposition box; the cationic solution and KCl water solution are ultrasonic atomized to aerosol after some time, then the solution is pressed in the aerosol deposition box for some time, the Prussian blue dress electrode is obtained.
    • 提供普鲁士蓝色礼服电极的方法。 该方法包括:对基底进行表面预处理; 预处理电极安装在气溶胶沉积盒中; 制备阴离子溶液和KCl水溶液,制备阳离子溶液和KCl水溶液,两种浓度相同; 阴离子溶液为K 4 Fe(CN)6或K 3 Fe(CN)6溶液,阳离子溶液为FeCl 3或(NH 4)Fe(SO 4)2溶液; 将制备的阴离子溶液和KCl水溶液装入超声波雾化器中,将溶液超声雾化成气溶胶,然后将溶液压在气溶胶沉积盒中; 阳离子溶液和KCl水溶液经过一段时间超声雾化成气溶胶,然后将溶液在气溶胶沉积盒中压制一段时间,得到普鲁士蓝色连衣裙电极。
    • 8. 发明公开
    • METHOD FOR PREPARING POLYLACTIC ACID AND PRODUCTS THEREOF USING A TWIN-SCREW EXTRUDER
    • 用于生产及其产品聚乳酸使用一台双螺杆挤出机
    • EP2327735A1
    • 2011-06-01
    • EP09809268.7
    • 2009-09-01
    • Nanjing University of Technology
    • LI, ZhenjiangKAN, SuliGUO, ChangWANG, YanqinSHENG, ShichuanSONG, PingOUYANG, Pingkai
    • C08G63/08C08G63/82
    • C08G63/823B29C47/0004B29C47/0021B29C47/40B29C47/662B29C47/767B29C47/827B29C67/246B29C2947/92704B29C2947/92895B29K2067/046B29K2995/006C08G63/08C08G63/785
    • A method for preparing polylactic acid and products thereof using a twin-screw extruder, in which a carbene carbon dioxide adduct of formula (I) is mixed with lactide, and then reactive extruded through a twin-screw extruder to produce polylactic acid and products thereof. In formula (I), the dotted line represents optional double bond; X 1 is selected from S or N; X 2 is selected from C or N; R 1 , R 2 are selected from the same or different groups of hydrogen, alkyl with 1 to 10 carbon atoms, alkyl with 1 to 10 carbon atoms and substituted by one or more of halogen atom, hydroxyl group, phenyl and cyano group, cycloalkyl with 3 to 6 carbon atoms, halogen atom, adamantyl, phenyl and phenyl substituted by one or more of halogen atom, hydroxyl group, alkyl and cyano group; R 3 , R 4 are selected from the same or different groups of hydrogen, halogen atom, cyano group, hydroxyl group, alkyl with 1 to 4 carbon atoms, alkyl with 1∼4 carbon atoms and substituted by one or more of halogen atom, hydroxyl group, phenyl and cyano group, phenyl and phenyl substituted by one or more of halogen group, hydroxyl group, alkyl and cyano group; or R 3 and R 4 are connected to form a ring with 3 to 8 carbon atoms; or R 2 and R 3 are connected to form a five- or six-membered N-containing heterocycle which is unsubstituted.
    • 一种通过双螺杆挤出机制造的聚乳酸及其产品使用双螺杆挤出机,其中,式(I)的一个卡宾二氧化碳加合物与丙交酯混合,然后反应性挤出法生产的聚乳酸及其产品 , 在式(I)中,虚线darstellt任选的双键; X 1选自S或N的; X 2选自C或N的; R 1,R 2选自氢的相同或不同的基团,烷基具有1至10个碳原子,烷基具有由一个或多个卤素原子,羟基,苯基和氰基,环烷基的1至10个碳原子和substituiertem 具有3至6个碳原子,卤原子,金刚烷基,苯基和苯基substituiertem被一个或多个卤素原子,羟基,烷基和氰基的; R 3,R 4被一个或多个卤素原子的,羟基选自氢,卤素原子,氰基,羟基,烷基的相同或不同的基团选自具有1至4个碳原子,烷基具有1¼4碳原子和substituiertem ,苯基和氰基,苯基和苯基substituiertem被一个或多个卤素基团,羟基,烷基和氰基的; 或R 3和R 4连接,以形成具有3至8个碳原子的环; 或R 2和R 3连接以形成五元或六元含N杂环所有这是unsubstituiertem。