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31. 发明公开

EP1120435A1 APPARATUS AND METHOD FOR PRODUCING RESIN 有权
标题翻译： VORRICHTUNG UND VERFAHREN ZUR HERSTELLUNG VON HARZ
公开(公告)号：EP1120435A1
公开(公告)日：2001-08-01
申请号：EP00944312.8
申请日：2000-07-06
申请人： TEIJIN LIMITED
发明人： HATONO, Kazuki , HIRATA, Masumi , KANEKO, Hiroaki , SAWAKI, Toru , FUNAKOSHI, Wataru , SASAKI, Katsushi , SIMONARU, Masasi , KIYOSHIGE, Kouji
IPC分类号： C08G85/00 , C08G64/20 , C08J3/00 , B01F7/08
CPC分类号： B29C47/767 , B29C47/0009 , B29C47/38 , B29C47/402 , C08G64/205 , C08G64/307
摘要： A method of producing a polycarbonate or the like which is excellent in hydrolysis and heat stability such as a reduction in molecular weight at the time of molding and color retention and moldability such as releasability and transferability, rarely experiences residence deterioration such as coloring, crosslinking and gel formation and has an extremely small content of foreign matter by employing a special structure for an opening in the side surface of a horizontal cylindrical vacuum resin treating apparatus, supplying a molten polycarbonate into a unidirectional rotary intermeshing double-screw extruder under specific conditions, adding a specific agent under specific conditions and cleaning the inner surface of a production apparatus by a specific method.
摘要翻译：水解和热稳定性优异的聚碳酸酯等的制造方法，例如成型时的分子量的降低和保色性以及脱模性和转印性等成型性，很少发生着色，交联等的停留劣化，凝胶形成，并且通过采用在水平圆筒形真空树脂处理装置的侧表面中的开口的特殊结构，并且在特定条件下将熔融聚碳酸酯供给到单向旋转啮合双螺杆挤出机中，使异物含量极少，添加在特定条件下的特定试剂，并通过具体方法清洁生产装置的内表面。

32. 发明公开

EP1081174A1 PROCESS FOR PRODUCING POLYCARBONATE 有权
标题翻译：生产聚碳酸酯的方法
公开(公告)号：EP1081174A1
公开(公告)日：2001-03-07
申请号：EP00906671.3
申请日：2000-03-03
申请人： Ube Industries, Ltd.
发明人： NISHIHIRA, Keigo , TANAKA, Shuji, Ube Production Center , YOSHIDA, Shinichi, Ube Production Center
IPC分类号： C08G64/20 , C07C68/00 , C07C69/96
CPC分类号： C08G64/307 , C07C68/00 , C07C69/96
摘要： A process for preparing polycarbonate is composed of the steps of transesterifying a dialkyl oxalate and a phenolic compound to give a diaryl oxalate; decarbonylating the diaryl oxalate to give a diaryl carbonate; reacting the diaryl carbonate with a polyvalent hydroxyl compound in the presence of a catalyst containing an amine compound or an ammonium compound to give the polycarbonate, removing a phenolic by-product/amine by-product mixture; collecting the mixture; purifying the mixture so that the amount of the amine by-product in the mixture is reduced to give a phenolic by-product mixture not containing the amine by-product in an amount of more than 600 ppm; and, utilizing thus purified phenolic mixture as a whole or a part of the phenolic compound in the first step.
摘要翻译：制备聚碳酸酯的方法由以下步骤组成：使草酸二烷基酯和酚类化合物酯交换，得到草酸二芳基酯; 使草酸二芳基酯脱羧得到碳酸二芳基酯; 在含有胺化合物或铵化合物的催化剂存在下使碳酸二芳基酯与多价羟基化合物反应以得到聚碳酸酯，除去酚类副产物/胺副产物混合物; 收集混合物; 纯化该混合物，使得混合物中胺副产物的量减少，得到不含胺含量超过600ppm的副产物的酚类副产物混合物; 并且在第一步中使用如此纯化的酚类混合物作为整体或部分酚类化合物。

33. 发明公开

EP1063253A1 Light diffusing block copolycarbonates 审中-公开
标题翻译： Lichtstreuende嵌段聚碳酸酯
公开(公告)号：EP1063253A1
公开(公告)日：2000-12-27
申请号：EP99112160.9
申请日：1999-06-24
申请人： Bayer Aktiengesellschaft
发明人： Marek, Miroslav, Dr. , Bruder, Friedrich-Karl, Dr. , Douzinas, Konstadinos, Dr.
IPC分类号： C08G64/18 , C08G64/14 , C08G64/20 , C08G63/64 , C08G81/02 , C08L69/00 , C08F8/14 , C08F10/00 , E04D3/35
CPC分类号： B32B27/08 , B32B27/20 , B32B27/32 , B32B27/365 , B32B2369/00 , C08G63/64 , C08G64/18 , C08G64/30 , C08G81/024 , C08L69/00 , C08L53/00
摘要： The invention describes a copolymer with at least one mono- or α,ω-dihydroxypolyolefine and at least one polycarbonate where the content of polyolefine segment is in the range 0,005- 60 wt.%, methods of preparation and the use of compositions containing the copolymer for light diffusion.
摘要翻译：本发明描述了具有至少一种单或α，ω-二羟基聚烯烃和至少一种聚碳酸酯的共聚物，其中聚烯烃链段的含量在0.005-60重量％的范围内，制备方法和使用含有共聚物的组合物用于光扩散。

34. 发明公开

EP0995768A2 Process for production of aromatic polycarbonate resin and molded article of aromatic polycarbonate resin 审中-公开
标题翻译：芳香族化合物聚碳酸酯和Geformstand Gegenstand aus aromatischem Polycarbonatharz
公开(公告)号：EP0995768A2
公开(公告)日：2000-04-26
申请号：EP99308088.6
申请日：1999-10-13
申请人： TEIJIN LIMITED
发明人： Matsumoto, Kyosuke, Teijin Ltd. Iwakuni Res. Ctr. , Simonaru, Masasi, Teijin Ltd. Iwakuni Res. Ctr. , Sawaki, Toru, Teijin Ltd. Iwakuni Res. Ctr. , Sasaki, Katsushi, Teijin Ltd. Iwakuni Res. Ctr. , Murakami, Masahiro, Teijin Ltd. Iwakuni Res. Ctr. , Matsuoka, Yoshiki, Teijin Ltd. Iwakuni Res. Ctr.
IPC分类号： C08G64/20
CPC分类号： C08G64/307
摘要： An aromatic polycarbonate resin is produced under the conditions that the flow velocity of the reaction mixture in a pipe through which a molten reaction mixture passes is a specific value or over, the viscosity-average molecular weight of the reaction mixture is 1,000 or over, the sum of the average retention times of the reaction mixture is not longer than 3 hours, the wall temperature of the pipe through which a molten reaction mixture passes is set to be higher than the temperature of the reaction mixture in the pipe, the catalyst deactivation agent is added within 2 hours after the completion of the melt polycondensation reaction, the filtration is carried out by using a filter having a specific retained particle size under a specific pressure difference, specific treated amount of the aromatic polycarbonate resin per unit area of the filter and a ratio of W (flow quantity of filtered polymer) x 1,000/A (maximum area of the polymer path in the filtration vessel) falling within a specific range, etc.
The present invention provides a process for producing an aromatic polycarbonate resin and its molded article having excellent color and transparency as well as excellent color stability and thermal stability in high efficiency while suppressing contamination with foreign matters and the discoloration and gel formation of the resin.
摘要翻译：在熔融反应混合物通过的管中的反应混合物的流速为特定值以上的条件下制造芳族聚碳酸酯树脂，反应混合物的粘均分子量为1000以上，反应混合物的平均保留时间的总和不超过3小时，熔融反应混合物通过的管的壁温设定为高于管中的反应混合物的温度，催化剂失活剂在熔融缩聚反应完成后2小时内加入，过滤通过使用具有特定保留粒径的特定压力差的过滤器，每单位面积过滤器的芳族聚碳酸酯树脂的特定处理量，过滤聚合物的W（过滤聚合物的流量）×1,000 / A（过滤容器中的聚合物路径的最大面积）的比率落入特定范围等。本发明提供一种芳香族聚碳酸酯树脂及其成型体的制造方法，其具有优异的颜色和透明性，并且在高效率下具有优异的颜色稳定性和热稳定性，同时抑制异物污染和变色和凝胶形成的树脂。

35. 发明公开

EP0949288A1 Method of preparing polycarbonates by solide state polymerization 失效
标题翻译： Verfahren zur Darstellung von Polycarbonaten durch Festphasenpolykendingensation
公开(公告)号：EP0949288A1
公开(公告)日：1999-10-13
申请号：EP98302761.6
申请日：1998-04-08
申请人： GENERAL ELECTRIC COMPANY
发明人： Idage, Bhaskar Bhairavnath , Sivaram, Swaminathan , Varadarajan, Godavarthi Satyanarayana , King, Joseph Anthony, Jr.
IPC分类号： C08G64/40 , C08G64/20
CPC分类号： C08G64/40 , C08G64/30
摘要： Crystallization of precursor polycarbonates prior to solid state polymerization is achieved by contact with a non-solvent comprising, at least in part, a dialkyl carbonate such as dimethyl carbonate. The non-solvent can be a mixture, typically of dimethyl carbonate with water or an alkanol such as methanol.
摘要翻译：在固态聚合之前，前体聚碳酸酯的结晶通过与至少部分由碳酸二烷基酯如碳酸二甲酯组成的非溶剂的接触来实现。非溶剂可以是通常为碳酸二甲酯与水或链烷醇如甲醇的混合物。

36. 发明公开

EP0896013A1 Crosslinked polycarbonate and polylactic acid composition containing the same 失效
标题翻译： V tes tes tes t t t t t t t t t t t t t t t t t t
公开(公告)号：EP0896013A1
公开(公告)日：1999-02-10
申请号：EP98114235.9
申请日：1998-07-29
申请人： Shimadzu Corporation , MITSUI CHEMICALS, INC.
发明人： Ishihara, Jiro , Kuyama, Hiroki , Ozeki, Eiichi , Ishitoku, Takeshi , Tanaka, Masahide , Sakamoto, Naoya
IPC分类号： C08G64/20 , C08L69/00 , C08L67/04 , C08L67/00 , C08G64/02
CPC分类号： C08G64/0216 , C08G64/226 , C08G64/305
摘要： A crosslinked polycarbonate is obtained by polycondensation of diol (A), trivalent or more polyhydric alcohol (B) whose arbitrary two hydroxy groups are not in the positional relationship of 1,2-disubstitution or 1,3-disubstitution, and carbonyl component (C) such as carbonic acid diesters. In the polycondensation step, no side reaction does not occur.
This crosslinked polycarbonate is used as a modifier for polylactic acids. The brittleness of the polylactic acid is improved while maintaining mechanical strength, thermostability, and transparency.
摘要翻译：通过二醇（A），任意两个羟基不与1,2-二取代或1,3-二取代的位置关系的三价以上的多元醇（B）和羰基成分（C）的缩聚得到交联聚碳酸酯）如碳酸二酯。在缩聚步骤中，不会发生副反应。该交联聚碳酸酯用作聚乳酸的改性剂。改善聚乳酸的脆性，同时保持机械强度，热稳定性和透明度。

37. 发明公开

EP0849305A2 Method for preparing polycarbonate by solid state polymerization 失效
标题翻译： Verfahren zur Herstellung von Polycarbonat durch Festphasenpolykendingensation
公开(公告)号：EP0849305A2
公开(公告)日：1998-06-24
申请号：EP97302927.5
申请日：1997-04-29
申请人： GENERAL ELECTRIC COMPANY
发明人： Varadarajan, Godavarthi S. , Idage, Bhaskar , Sivaram, Swaminathan , King, Joseph Anthony , Hait, Sukhendu Bikash
IPC分类号： C08G64/20 , C08G64/40 , C08G64/30
CPC分类号： C08G64/42 , C08G64/14 , C08G64/20 , C08G64/307
摘要： Solid state polycarbonate formation comprises an initial step of converting a precursor polycarbonate to an enhanced crystallinity precursor polycarbonate and a second step of polymerizing said enhanced crystallinity precursor polycarbonate in the solid state. Several options are employed. These include modifying the precursor polycarbonate by contact with a dihydroxy compound or diaryl carbonate, conversion of the precursor polycarbonate to the enhanced crystallinity polymer by contact with at least one compound selected from the group consisting of alkali metal hydroxides, tetraalkylammonium hydroxides, tetraalkylammonium carboxylates, tetraalkylphosphonium hydroxides and tetraalkylphosphonium carboxylates, and conducting the solid state polymerization in the presence of a catalytic amount of at least one tetralkylammonium or tetraalkylphosphonium carboxylate. The preferred tetralkylammonium compounds are tetramethylammonium maleate and tetramethylammonium hydroxide. Polymerization may be conducted in the presence of a solvent resistance-imparting monomer such as hydroquinone or resorcinol or a branching agent such as 1,1,1-tris(4-hydroxyphenyl)ethane.
摘要翻译：固态聚碳酸酯形成包括将前体聚碳酸酯转化为增强的结晶性前体聚碳酸酯的初始步骤和将固体状态的所述增强的结晶度前体聚碳酸酯聚合的第二步骤。采用了几个选项。这些包括通过与二羟基化合物或碳酸二芳基酯接触来改性前体聚碳酸酯，通过与至少一种选自碱金属氢氧化物，四烷基铵氢氧化物，四烷基铵羧酸盐，四烷基鏻鎓盐的化合物接触，将前体聚碳酸酯转化为增强的结晶度聚合物氢氧化物和四烷基鏻羧酸盐，并在催化量的至少一种四烷基铵或四烷基鏻羧酸盐的存在下进行固态聚合。优选的四烷基铵化合物是马来酸四甲基铵和氢氧化四甲基铵。聚合可以在赋予耐溶剂性的单体如氢醌或间苯二酚或支化剂如1,1,1-三（4-羟基苯基）乙烷的存在下进行。

38. 发明授权

EP0434888B1 Process for producing an aromatic polycarbonate 失效
标题翻译：一种生产芳族聚碳酸酯的过程
公开(公告)号：EP0434888B1
公开(公告)日：1996-06-19
申请号：EP90106825.4
申请日：1990-04-10
申请人： Mitsubishi Chemical Corporation
发明人： Tamura, Mitsuhiko , Akihara, Isao
IPC分类号： C08G64/20 , C08G64/04
CPC分类号： C08G64/24 , C08G64/26

39. 发明公开

EP0561363A3 Process for producing polycarbonate 失效
标题翻译：生产聚碳酸酯的方法
公开(公告)号：EP0561363A3
公开(公告)日：1994-02-16
申请号：EP93104302.0
申请日：1993-03-16
申请人： IDEMITSU PETROCHEMICAL CO. LTD.
发明人： Kuze, Shigeki, c/o Idemitsu Petrochemical Co., Ltd , Okumura, Ryozo, c/o Idemitsu Petrochemical Co. Ltd , Suwabe, Yoshinobu, c/o Idemitsu Petrochem. Co. Ltd
IPC分类号： C08G64/20 , C08G64/04
CPC分类号： C08G64/307
摘要： There is disclosed a process for producing a polycarbonate which comprises reacting, by the melt method, (A) a dihydroxy compound with (B) a carbonic diester having a chlorine content derived from chloroformate group of not more than a prescribed level. According to the above process, a polycarbonate which is excellent in transparency, tone of color, heat resistance and water resistance can be efficiently and economically produced.
摘要翻译：公开了一种生产聚碳酸酯的方法，该方法包括通过熔融法使（A）二羟基化合物与（B）具有来自氯甲酸酯基团的氯含量不超过规定水平的碳酸二酯反应。根据上述方法，可以有效且经济地制造透明性，色调，耐热性和耐水性优异的聚碳酸酯。

40. 发明公开

EP0529093A1 PROCESS FOR PRODUCING POLYCARBONATE 失效
标题翻译：生产聚碳酸酯的方法
公开(公告)号：EP0529093A1
公开(公告)日：1993-03-03
申请号：EP92906162.0
申请日：1992-02-28
申请人： DAICEL CHEMICAL INDUSTRIES, LTD.
发明人： YAMATO, Tsutomu , OSHINO, Yasuhiro , FUKUDA, Yutaka , KANNO, Tatsuya , KUWANA, Takaaki
IPC分类号： C08G64/30 , C08G64/20
CPC分类号： C08G64/307 , C08G64/30
摘要： A process for industrially producing a colorless, transparent polycarbonate with a high molecular weight efficiently by the melt polycondensation of a dihydroxy compound with a carbonic diester through transesterification, which comprises preparing a polycarbonate prepolymer in the first-stage reaction and conducting the polycondensation thereof either under the condition of a residence time ranging from 15 to less than 60 minutes or by using at least one self-cleaning twin-screw paddle extruder in the second-stage reaction.
摘要翻译：通过酯交换反应使二羟基化合物与碳酸二酯熔融缩聚，有效地工业生产高分子量的无色透明聚碳酸酯的方法，该方法包括在第一步反应中制备聚碳酸酯预聚物，并在其下进行缩聚停留时间为15至小于60分钟的条件或通过在第二阶段反应中使用至少一个自清洁双螺杆桨式挤出机。

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