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    • 22. 发明公开
    • Method and apparatus for producing nano-particles of molybdenum oxide
    • Verfahren und Vorrichtung zur Herstellung vonMolybdänoxid-Nanopartikeln
    • EP1486240A2
    • 2004-12-15
    • EP04009227.2
    • 2004-04-19
    • Cyprus Amax Minerals Company
    • Taube, Joel A.
    • B01D7/00C01G39/02
    • B82Y30/00B01D7/00C01G39/02C01P2004/04C01P2004/10C01P2004/64C01P2006/12Y10S977/775Y10S977/776Y10S977/811
    • Apparatus for producing nano-particles according to the present invention may comprise a furnace defining a vapor region therein. A precipitation conduit having an inlet end and an outlet end is positioned with respect to the furnace so that the inlet end is open to the vapor region. A quench fluid supply apparatus supplies quench fluid in a gas state and quench fluid in a liquid state. A quench fluid port positioned within the precipitation conduit is fluidically connected to the quench fluid supply apparatus so that an inlet to the quench fluid port receives quench fluid in the gas state and quench fluid in the liquid state. The quench fluid port provides a quench fluid stream to the precipitation conduit to precipitate nano-particles within the precipitation conduit. A product collection apparatus connected to the outlet end of the precipitation conduit collects the nano-particles produced within the precipitation conduit.
    • 根据本发明的用于生产纳米颗粒的设备可以包括在其中限定蒸气区域的炉。 具有入口端和出口端的沉淀管相对于炉定位,使得入口端对蒸气区开放。 骤冷流体供给装置以气体状态供给骤冷流体,并且以液态骤冷液体。 位于沉淀管道内的骤冷流体端口流体连接到骤冷流体供应装置,使得骤冷流体端口的入口容纳处于气体状态的骤冷流体并骤冷处于液态的流体。 骤冷流体端口向沉淀管道提供骤冷流体流以沉淀沉淀管道内的纳米颗粒。 连接到沉淀管道的出口端的产品收集装置收集在沉淀管道内产生的纳米颗粒。
    • 29. 发明公开
    • Distillative freezing process for separating close boiling mixtures
    • 破坏者Ausfrierverfahren zum Trennen von Stoffen mit dicht beieinanderliegenden Siedepunkten。
    • EP0044366A1
    • 1982-01-27
    • EP80302490.0
    • 1980-07-23
    • Cheng, Chen-YenCheng, Sing-Wang
    • Cheng, Chen-YenCheng, Sing-Wang
    • B01D9/04
    • B01D3/06B01D3/065B01D7/00B01D9/00B01D9/0018C01B3/50C01B7/0712C01B7/075C01B11/028C01B13/0248C01B15/013C01B33/046C01B33/10778C01F7/62C01G23/075C01G49/10C07C7/14C07C17/383C07C17/392C07C29/78C07C37/84C07C45/81C07C51/43C07C253/34C07C2601/14C07C47/04C07C57/04C07C53/08C07C53/16C07C57/145C07C63/16C07C31/12C07C39/04C07C39/06C07C39/14C07C39/30C07C35/12C07C255/08
    • A crystallization separation process for separating an at least partially liquid mixture containing two volatile components (A and B) the two components forming a binary system in which the vapor pressure ratio of A:B is 0.1 to 10 at the B-triple point and is less than the ratio of the heat of sublimation to the heat of melting of the B-component at the B-triple point, the constant pressure phase diagram having a B-enriched solid-vapor two phase region covering a substantial concentration range above the three phase state temperature and a B-enriched solid and liquid region below such temperature wherein a first vapor mixture and first condensed mass are formed by vaporizing the two components in a first zone at a temperature and pressure lower than the triple point temperature and pressure, the first condensed mass comprising a mother liquor and a solid phase which is B-enriched, the heat released in the formation of the solid being utilized to vaporize the volatile components.
      Such process can be extended to a gas mixture containing two volatile and condensable components (A and B) into substantially pure B and a B-lean component, in which heat is removed from the gas to cause part of the B to desublime, the A remaining in the vapor stream, the vapor stream then having heat removed therefrom while the vapor is at a temperature and pressure below the B-triple point values thereby causing formation of a further condensed mass.
    • 一种用于分离含有两种挥发性组分(A和B)的至少部分液体混合物的结晶分离方法,所述两种组分形成二元体系,其中A:B的蒸气压比在B三重点为0.1至10,并且为 小于B-三重点的B成分的升华热量与熔融热的比例,具有覆盖三分之一以上的实质浓度范围的富含B的固体蒸气两相区域的恒压相图 相状态温度和低于这种温度的富含B的固体和液体区域,其中通过在低于三重点温度和压力的温度和压力下将第一区域中的两种组分蒸发而形成第一蒸气混合物和第一冷凝物质, 包含母液和富含B的固相的第一浓缩物质,在形成固体中释放的热量用于蒸发挥发性组分。 这种方法可以扩展到含有两种挥发性和可冷凝组分(A和B)的气体混合物,成为基本上纯的B和贫B组分,其中热量从气体中除去以使B的一部分发生沉淀,A 保留在蒸汽流中,然后蒸汽流从其中除去热量,同时蒸汽处于低于B-三重点值的温度和压力下,从而形成另外的冷凝物质。