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11. 发明公开

EP2574920A1 Real-Time Compositional Analysis of Hydrocarbon Based Fluid Samples 有权
标题翻译： Echtzeitzusammensetzungsanalyse aus kohlenwasserstoffbasiertenFlüssigkeitsproben
公开(公告)号：EP2574920A1
公开(公告)日：2013-04-03
申请号：EP12186377.3
申请日：2012-09-27
申请人： Services Petroliers Schlumberger SA , Schlumberger Holdings Limited , SCHLUMBERGER TECHNOLOGY B.V. , PRAD Research and Development Limited
发明人： Zhdaneev, Oleg , Harrison, Christopher , Zuo, Youxiang , Zhang, Dingan , Steinecker, William , Lambertus, Gordon , Bostrom, Neil
IPC分类号： G01N33/28 , E21B49/10 , G01N30/02 , G01N21/31
CPC分类号： G01N33/2823 , E21B49/10 , G01N21/3504 , G01N21/3577 , G01N21/359 , G01N21/643 , G01N30/8658 , G01N2030/8854
摘要： A fluid analyzer (100) includes an optical analyzer (114) and a composition analyzer, such as a gas chromatograph (116). A data processor (118) is configured to determine a quantity, such as a weight percentage, of a target component of the fluid sample in response to results obtained from optical analyzer (114) and composition analyzer (116). The results are obtained at least in near real-time.
摘要翻译：流体分析器（100）包括光学分析器（114）和诸如气相色谱仪（116）的成分分析仪。数据处理器（118）被配置为响应于从光学分析器（114）和组成分析器（116）获得的结果来确定流体样本的目标分量的量，例如重量百分比。结果至少实时获得。

12. 发明授权

EP2226631B1 METHOD FOR ANALYSIS OF LOW-MOLECULAR-WEIGHT ORGANIC COMPOUND HAVING 20 OR LESS CARBON ATOMS IN WATER- AND OIL-REPELLENT COMPOSITION 有权
标题翻译：分析水和油拒斥组合物中具有20或更少碳原子的低分子量有机化合物的方法
公开(公告)号：EP2226631B1
公开(公告)日：2011-10-26
申请号：EP08865672.3
申请日：2008-12-17
申请人： Asahi Glass Company, Limited
发明人： HIKIMA, Satoshi
IPC分类号： G01N30/88 , G01N27/62 , G01N30/06 , G01N30/72 , C07C29/74 , G01N1/40
CPC分类号： G01N30/88 , G01N30/06 , G01N30/72 , G01N2030/884 , G01N2030/8845 , G01N2030/885 , G01N2030/8854
摘要： Disclosed is a method which can analyze a low-molecular-weight organic compound having 20 or less carbon atoms contained in a water- and oil-repellent composition in a trace amount with high accuracy. Specifically disclosed is an analysis method which comprises the following steps (a) to (c): (a) mixing a water- and oil-repellent composition comprising a medium and a fluorinated polymer dispersed or dissolved in the medium with an alcohol having 1 to 5 carbon atoms, and causing the fluorinated polymer to aggregate, thereby producing a solution containing aggregates of the fluorinated polymer; (b) separating the solution containing the aggregates of the fluorinated polymer into a liquid fraction and a solid fraction, thereby producing a liquid phase; and (c) measuring the concentration of a low-molecular-weight organic compound having 20 or less carbon atoms in the liquid phase by employing LC-MS, LC-MS/MS or GC-MS, wherein the fluorinated polymer has a repeating unit derived from a compound having a perfluoroalkyl group.
摘要翻译：公开了一种能够高精度地分析微量的防水防油组合物中所含的碳原子数为20以下的低分子有机化合物的方法。（a）〜（c）的分析方法：（a）将包含介质和分散或溶解在介质中的氟化聚合物的拒水拒油组合物与1〜 5个碳原子，并使氟化聚合物聚集，由此制备含有氟化聚合物聚集体的溶液; （b）将含有氟化聚合物的聚集体的溶液分离成液体部分和固体部分，由此产生液相; 和（c）通过使用LC-MS，LC-MS / MS或GC-MS测量液相中具有20个或更少碳原子的低分子量有机化合物的浓度，其中所述氟化聚合物具有重复单元衍生自具有全氟烷基的化合物。

13. 发明公开

EP2340354A2 METHOD FOR CORRECTING THE MEASURED CONCENTRATIONS OF GAS COMPONENTS IN DRILLING MUD 无效转让
标题翻译：方法进行校正气体成分的泥实测浓度
公开(公告)号：EP2340354A2
公开(公告)日：2011-07-06
申请号：EP09819676.9
申请日：2009-10-01
申请人： Chevron U.S.A. Incorporated
发明人： HANSON, Scott, A.
IPC分类号： E21B47/00 , G01N7/00
CPC分类号： E21B49/005 , G01N33/2823 , G01N2030/8854
摘要： A method of characterizing formation fluid present in a subsurface earth formation during drilling using methods for correcting the measured concentrations of gas components in drilling mud. Gas trap values for the gas components of interest, light hydrocarbons, are measured during mud logging and are corrected using relative response factors, determined from laboratory fluid analysis values and relative extraction efficiency values. The relative response factors for each gas component of interest can be used for correcting additional gas trap values measured in the same well or for correcting gas trap values measured in surrounding wells utilizing a similar drilling fluid. The corrected gas trap values for each of the gas components of interest can be utilized to calculate gas/oil ratios for characterizing the formation fluid from the volume of drilling mud.

14. 发明公开

EP2239553A1 A carbon compounds collecting system 审中-公开
标题翻译： Kohlenstoffverbindungssammelsystem
公开(公告)号：EP2239553A1
公开(公告)日：2010-10-13
申请号：EP09305310.6
申请日：2009-04-09
申请人： Total S.A.
发明人： Dessort, Daniel , Duclerc, Dominique , Le Van Loi, Robert , Cassagne, Alain
IPC分类号： G01N1/02 , G01N33/24
CPC分类号： G01N33/241 , G01N1/22 , G01N2030/8854
摘要： A collecting system for collecting at least part of the volatilisable or pyrolysable carbon compounds comprised in a core (10) taken from a well is disclosed. The system comprises:
• at least a heating device (32) comprising a laser source (36), the heating device (36) being configured so as to focus on the surface of the core (10) a laser beam issued from the laser source (36), the laser beam having at the surface of the core (10) a power density of at least 2 W/mm 2 , so as to cause the volatilisation or the thermal decomposition of at least part of the hydrocarbons comprised in a core (10)
• at least a collecting device (34) configured to collect at least part of the substance released from the core (10) due to the volatilisation or the thermal decomposition of part of the hydrocarbons of the core (10) when the laser beam is focused at the surface of the core (10).
摘要翻译：公开了一种用于收集包含在从井中取出的核心（10）中的至少一部分可挥发或可热解的碳化合物的收集系统。所述系统包括：至少一个包括激光源（36）的加热装置（32），所述加热装置（36）构造成聚焦在所述芯体（10）的表面上，所述激光束从所述激光器源（36），在芯（10）的表面具有至少2W / mm 2的功率密度的激光束，以便使至少部分包含在一个或多个碳氢化合物中的烃的挥发或热分解核心（10）至少一个收集装置（34），其被配置为收集由于芯部（10）的一部分烃的挥发或热分解而从芯部（10）释放的物质的至少一部分，激光束聚焦在芯（10）的表面。

15. 发明公开

EP2223100A1 HIGH PRESSURE AND HIGH TEMPERATURE CHROMATOGRAPHY 审中-公开
标题翻译：高高压和高温色谱
公开(公告)号：EP2223100A1
公开(公告)日：2010-09-01
申请号：EP08862623.9
申请日：2008-09-25
申请人： Services Pétroliers Schlumberger , Schlumberger Holdings Limited , Schlumberger Technology B.V. , Prad Research And Development Ltd
发明人： SHAH, Jagdish , BOSTROM, Neil-William , ZHDANEEV, Oleg , RAGHURAMAN, Bhavani , PASO, Kristofer Gunnar
IPC分类号： G01N30/22 , G01N33/28
CPC分类号： G01N33/2823 , E21B47/10 , G01N30/22 , G01N30/32 , G01N30/88 , G01N2030/8809 , G01N2030/8854
摘要： Methods and related systems are described. for high pressure chromatographic analysis. The described system includes a flowpath adapted to flow a mobile phase and the sample at high pressures, an injector (173) adapted to inject the fluid sample into a flowpath, a separation column (177) adapted to operate at high pressures for separating various components, a detector (179) and a processor (105) that calculates the amount of at least one component of the fluid sample. The system can operate a pressures above 20 atm or even 100 atm, and temperatures above about 100 degrees Celsius. The system can be deployed in a wellbore in a subterranean rock formation (110), and can include fluid collection system for obtaining the fluid sample downhole. The system can also be located close to a wellhead and includes a tap in fluid communication with a surface flowline carrying produced fluids and the injector.

16. 发明公开

EP2118645A1 METHOD OF ANALYSING THE HYDROCARBON COMPOUNDS IN A BITUMINOUS MATERIAL 审中-公开
标题翻译： VERFAHREN ZURANALYZE DER KOHLENWASSERSTOFFVERBINDUNGEN IN EINEM BITUMINENSEN MATERIAL
公开(公告)号：EP2118645A1
公开(公告)日：2009-11-18
申请号：EP08717498.3
申请日：2008-03-07
申请人： Shell Internationale Research Maatschappij B.V.
发明人： BLOMBERG, Jan , LE COUTALLER, Patricia , DEYGOUT, François Julien Raoul
IPC分类号： G01N30/46 , G01N33/28 , G01N30/12
CPC分类号： G01N30/463 , G01N33/28 , G01N2030/127 , G01N2030/8854 , G01N2030/8886
摘要： A method of analysing the hydrocarbon compounds in a bituminous material by means of comprehensive multi¬ dimensional gas chromatography is disclosed. The method may be used to measure the quantity of polycyclic aromatic compounds (PACs) in a bituminous material and may be used to determine the mutagenic tendency of a bituminous material.
摘要翻译：公开了通过全面的多维气相色谱分析沥青材料中的烃化合物的方法。该方法可用于测量沥青材料中多环芳族化合物（PAC）的量，并且可用于确定沥青材料的诱变倾向。

17. 发明公开

EP1877946A2 A NEW DATA PROCESSING/VISUALIZATION METHOD FOR TWO(MULTI)DIMENSIONAL SEPARATION GAS CHROMATOGRAPHY xMASS SPECTROMETRY(GCxMS) TECHNIQUE WITH A TWO (MULTIPLY) DIMENSIONAL SEPARATION CONCEPT AS AN EXAMPLE 审中-公开
标题翻译：新的数据处理和可视化步骤中使用两个或分离多维的概念作为范例来GC-X-MASS双链和多维分离及方法
公开(公告)号：EP1877946A2
公开(公告)日：2008-01-16
申请号：EP06759174.3
申请日：2006-05-05
申请人： EXXONMOBIL RESEARCH AND ENGINEERING COMPANY
发明人： WANG, Frank C. , QIAN, Kuangnan
IPC分类号： G06F19/00
CPC分类号： G01N30/8651 , G01N30/463 , G01N30/72 , G01N2030/8854 , Y10T436/11
摘要： This invention is a data processing/visualization method which includes the software development and operation to apply to any multi- dimensional separation. The GC-MS analysis of diesel is an example to demonstrate this software development and operation. The steps of this method includes (1) displaying the total ion chromatogram obtained from a GC-MS experiment, (2) displaying each mass spectrum versus retention time, (3) selecting a normal paraffin family as the reference compound family for relative polarity display, (4) transforming every mass slice to line-up normal paraffin compound family in the same relative retention time (position), (5) rotating the axis to best display the two (multi) dimensional data.

18. 发明公开

EP1859264A1 METHOD FOR ANALYZING ACTIVATED POLYETHYLENE GLYCOL COMPOUNDS 审中-公开
标题翻译：程序已激活，聚乙二醇化合物分析
公开(公告)号：EP1859264A1
公开(公告)日：2007-11-28
申请号：EP06736915.7
申请日：2006-03-03
申请人： Dow Global Technologies Inc.
发明人： WALLINGFORD, Ross, A. , TUROWSKI, Maciej
IPC分类号： G01N30/88 , A61K47/48
CPC分类号： G01N30/88 , A61K47/60 , G01N2030/8813 , G01N2030/8854 , Y10T436/200833 , Y10T436/2575
摘要： A chemical analysis method for the determination Of RO(CH2CH2O)nH, RO(C2H4O)nA, and AO(C2H4O)nA in a mixture thereof, wherein R is an alkyl group, A is a functional group for coupling with a surface or a biologically active material or another thing of use and n is an interger greater than 10. The method includes the step of chromatographing a sample of the mixture by liquid chromatography under critical conditions to determine the relative amounts Of RO(CH2CH2O)nH, RO(C2H4O)nA, and AO(C2H4O)nA in the mixture, hi addition a a chemical analysis method for the determination Of RO(CH2CH2O)nH, RO(C2H4O)nA, and AO(C2H4O)nA in a mixture thereof, wherein R is an alkyl group, A is a functional group for coupling with a biologically active material and n is an interger greater than 10. The method includes two steps. The first step is derivatizing the A groups of the mixture with a derivatizing agent to form a derivatized mixture comprising RO(CH2CH2O)nH , RO(C2H4O)nAD, and DAO(C2H4O)nAD , wherein AD is the derivatized A group. The second step is chromatographing a sample of the derivatized mixture by liquid chromatography under critical conditions to determine the relative amounts Of RO(CH2CH2O)nH, RO(C2H4O)nAD,and DAO(C2H4O)nAD in the derivatized mixture.

19. 发明公开

EP1707959A1 DEVICE AND METHOD FOR ANALYZING POLYCYCLIC AROMATIC HYDROCARBON HAVING NITRO GROUP IN DIESEL PARTICULATE 审中-公开
标题翻译：装置和方法用于柴油机颗粒分析多环芳烃硝基
公开(公告)号：EP1707959A1
公开(公告)日：2006-10-04
申请号：EP04747283.2
申请日：2004-07-09
申请人： Isuzu Motors Limited
发明人： SHIBATA, Keiko, Isuzu Advanced Engineering Ctr Ltd
IPC分类号： G01N30/84 , G01N30/74 , B01J20/287 , G01N31/10
CPC分类号： G01N30/461 , B01J20/287 , G01N2030/062 , G01N2030/8405 , G01N2030/8854
摘要： The invention provides an apparatus and method for efficiently analyzing nitropolycyclic aromatic hydrocarbon contained in diesel particulates.
The invention comprises a step of extracting soluble organic fraction from diesel particulates contained in the exhaust of a diesel engine using a solvent, a step of concentrating and drying the extraction obtained by the extraction step, and a step of separating and extracting the solution via high-performance liquid chromatograph, wherein the separation step via the high-performance liquid chromatograph comprises a separation step using a silica gel/C8 column, a reduction step using an alumina/Pt-Rh reduction column, and a separation step using an ODS column, and further comprises a subsequent step of quantifying the nitropolycyclic aromatic hydrocarbon using a fluorescence detector.
摘要翻译：本发明提供的装置和方法，用于分析包含在柴油机微粒高效nitropolycyclic芳烃。本发明包括使用溶剂，浓缩，干燥由提取步骤得到的提取的步骤中提取与包含在柴油发动机的排气柴油微粒子可溶性有机成分的步骤，和分离，并通过高提取溶液的步骤 - 性能液相色谱仪，通过worin高性能液相色谱分离步骤包括使用硅胶/ C8柱分离步骤，还原步骤中使用在氧化铝/铂 - 铑还原柱，和一个分离步骤中，使用在ODS柱，并且还包括使用荧光检测器定量nitropolycyclic芳香烃的后续步骤。

20. 发明公开

EP0834071A1 METHOD FOR PREDICTING CHEMICAL OR PHYSICAL PROPERTIES OF CRUDE OILS 失效
标题翻译：用于预测原油化学或物理性质
公开(公告)号：EP0834071A1
公开(公告)日：1998-04-08
申请号：EP96921214.0
申请日：1996-05-15
申请人： EXXON RESEARCH AND ENGINEERING COMPANY
发明人： ASHE, Terrence, Rodney , ROUSSIS, Stilianos, George , FEDORA, James, W. , FELSKY, Gerald , FITZGERALD, William, Patrick
IPC分类号： G01N30 , G01N33
CPC分类号： G01N33/2823 , G01N30/7206 , G01N30/8668 , G01N30/8693 , G01N2030/626 , G01N2030/8854 , G01N2201/129
摘要： A method for predicting the properties of crude oils or their boiling fractions which comprises selecting a chemical or perceptual or physical or performance property or groups of properties of the crude oil or its boiling fractions and creating a training set from reference samples which contain characteristic molecular species present in the crude oil or its boiling fractions. The reference samples are subjected to GC/MS analysis wherein the often collinear data generated is treated by multivariate correlation methods. The training set produces coefficients which are multiplied by the matrix generated from a GC/MS analysis of an unknown sample to produce a predicted value of the chemical, performance, perceptual or physical property or groups of properties selected.

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