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141. 发明公开

EP0841347A1 Synthesis of macrocyclic polymers with group IIA and IIB metal cyclic organometallic initiators 失效
标题翻译：与环状Organometallinitiatoren大环聚合物的制备使用组IIA和IIB族的金属
公开(公告)号：EP0841347A1
公开(公告)日：1998-05-13
申请号：EP97117830.6
申请日：1997-10-15
申请人： Bridgestone Corporation
发明人： Hall, James E.
IPC分类号： C08F4/44 , C08F4/50 , C08F4/56 , C07F3/02 , C08G85/00 , C08F36/04 , C08F297/04
CPC分类号： C08G85/00 , C08F4/50 , C08F4/565 , C08F36/04 , C08F297/044 , C08F4/44
摘要： The invention is a practical process for anionically synthesizing commercially significant quantities of macrocyclic polymers from polar and/or non-polar monomers by using Group IIA and IIB metal cyclic organometallic initiators. Activation of the ring metal atom results in anionic polymerization of the monomers by addition into the initiator ring at the bonds between the atom and its two adjacent carbon atoms, the metal atom acting as a bridge between the two living ends of the propagating chain. Coupling of the cyclic polymer living ends by coupling agents produces macrocyclic polymers that are stable in air and moisture and that exhibit desirable properties, such as low viscosities at high molecular weights. Such macrocyclic polymers provide enhanced polymer processability during molding, extruding and the forming of films. Macrocyclic polymers terminated with coupling agents that also provide functional groups may be compounded to produce vulcanizable elastomeric compounds and articles that exhibit reduced hysteresis properties.

142. 发明授权

EP0479542B1 A phosphino binaphthyl compound and transition metal complexes thereof 失效
标题翻译：甲膦基联萘化合物和它们的过渡金属络合物。
公开(公告)号：EP0479542B1
公开(公告)日：1995-11-29
申请号：EP91308957.9
申请日：1991-09-30
申请人： Takasago International Corporation
发明人： Sayo, Noboru, c/o Takasago Res. Inst. Inc. , Kumobayashi, Hidenori, Takasago Res. Inst. Inc.
IPC分类号： C07F9/50 , C07F9/53 , C07F15/00 , C07F3/02 , C07C25/22 , C07B53/00
CPC分类号： B01J31/2457 , B01J2231/643 , B01J2531/0266 , B01J2531/821 , B01J2531/822 , B01J2531/827 , C07B53/00 , C07C25/22 , C07C2602/10 , C07F9/5027 , C07F15/004 , C07F15/0053 , C07F15/008

143. 发明公开

EP0650971A1 Deprotonation of cyclopentadienyl derivatives 失效
标题翻译：取代环戊二烯基酯。
公开(公告)号：EP0650971A1
公开(公告)日：1995-05-03
申请号：EP94116989.8
申请日：1994-10-27
申请人： ALBEMARLE CORPORATION
发明人： Strickler, Jamie Ray , Power, John Mary
IPC分类号： C07F7/10 , C07F3/02
CPC分类号： C07F3/02 , C07F7/10 , C07F17/00
摘要： Cyclopentadienyl derivatives are deprotonated by a process whereby the cyclopentadienyl derivatives are reacted with a Grignard reagent in an inert solvent which contains from about 0.5 to 1.5 equivalents per equivalent of cyclopentadienyl derivative of a cyclic ether or an acyclic polyether, so as to form a dianionic salt of said cyclopentadienyl derivative.
摘要翻译：环戊二烯基衍生物的去质子化。包括使格利雅试剂与衍生物反应。在惰性溶剂中形成衍生物的二偶氮卤化镁盐。溶剂含有0.5-1.5当量。每平方的衍生物。的选自环醚和无环聚醚的醚。以太是首选。 THF。环戊二烯衍生物是（C5Me4H）SiMe2（NH-t-Bu）和衍生物的二阴离子盐。是（MgX）2（（C5Me4）-SiMe2（N-t-Bu））。THF，其中X是卤素。

144. 发明授权

EP0282419B1 Ether free organometallic amide compositions 失效
标题翻译： Ätherfreieorganometallische Amidverbindungen。
公开(公告)号：EP0282419B1
公开(公告)日：1995-04-05
申请号：EP88400593.5
申请日：1988-03-14
申请人： LITHIUM CORPORATION OF AMERICA
发明人： Mehta, Vijay C. , Rathman, Terry Lee , Sanchez, Ramiro , Morrison, Robert Charles
IPC分类号： C07F3/02 , C07F7/10
CPC分类号： C07F3/003 , C07F7/10

145. 发明授权

EP0402755B1 L-Carnitin-Magnesium-Zitrat 失效
标题翻译： L-肉碱 - 镁 - Zitrat
公开(公告)号：EP0402755B1
公开(公告)日：1993-08-25
申请号：EP90110725.0
申请日：1990-06-06
申请人： LONZA AG
发明人： Scholl, Thomas, Dr,. Chemiker , Kohl, Willibald, Dr., Dipl.-Ing.
IPC分类号： C07C229/76 , C07F3/02 , A61K31/195 , A61K31/28
CPC分类号： C07C59/265 , C07C229/22

146. 发明授权

EP0242801B1 Hydrocarbyloxy magnesium halides 失效
标题翻译：氢氯氰菊酯
公开(公告)号：EP0242801B1
公开(公告)日：1993-03-10
申请号：EP87105638.8
申请日：1987-04-16
申请人： LITHIUM CORPORATION OF AMERICA
发明人： Mehta, Vijay Chandrakant
IPC分类号： C07F3/02
CPC分类号： C07C29/72 , C07F3/003 , C07C31/30

147. 发明公开

EP0526941A1 Halomagnesium hydrocarbyloxide composition and process for preparation 失效
标题翻译：卤代烃烃氧化物组合物和制备方法
公开(公告)号：EP0526941A1
公开(公告)日：1993-02-10
申请号：EP92202317.1
申请日：1992-07-28
申请人： Akzo Nobel N.V.
发明人： Smith, Gregory Morgan , Amata, Richard James , Tirendi, Charles Francis , Band, Elliot Isaac
IPC分类号： C07F3/02
CPC分类号： C07F3/003
摘要： A substantially pure, chemically distinct halomagnesium alkoxide compound is formed by reaction of a dihydrocarbylmagnesium compound with a compound which will replace an hydrocarbyl functionality thereon with an hydrocarbyloxy functionality and thereafter reacting the resulting product with a compound which replaces the other hydrocarbyl functionality with a halogen functionality, such as chlorine. The 13 C nuclear magnetic resonance spectrum of the product exhibits no more than one strong, narrow absorption peak for each chemically inequivalent carbon atom in the hydrocarbyloxy ligand of the compound.
摘要翻译：通过使二烃基镁化合物与将用烃氧基官能团取代其上的烃基官能团的化合物反应，然后使所得产物与用卤素官能团取代其它烃基官能团的化合物反应形成基本纯的化学上不同的卤代镁醇盐化合物如氯。该产物的13C核磁共振谱对该化合物的烃氧基配体中的每个化学不等同的碳原子表现出不超过一个强而窄的吸收峰。

148. 发明公开

EP0493642A1 Novel sulfonyl derivatives 失效
标题翻译：新磺酰化
公开(公告)号：EP0493642A1
公开(公告)日：1992-07-08
申请号：EP91100035.4
申请日：1991-01-02
申请人： Takayanagi, Takeo, Dr.
发明人： Takayanagi, Takeo, Dr.
IPC分类号： C07C335/42 , A61K31/63 , C07D203/12 , C07F3/02 , C07F1/08 , C07C311/48 , C07C309/76 , C07C311/53 , C07C309/88 , C07F3/10
CPC分类号： C07D203/08 , C07C309/76 , C07C309/88 , C07C311/49 , C07C311/53 , C07C335/42 , C07D239/69 , C07D473/38 , C07F1/005 , C07F3/003 , C07H19/16
摘要： The present invention relates to novel sulfonyl compounds

wherein R' and R'' are the same or different and are each hydrogen, -COCHR⁴, -COC(R⁴)₃ -SO₂CH₃, -COOCH₂CH₃, -CH₂-CH₂-R⁴, -CONH-CH₂CH₂R⁴, -CONHCH₂COOCH₂CH₃, -CH₂CH₂OCONH₂, and R₄ is Cl or a residue selected from

-NHCOCH₂CH₂OH, -NHCOCH₂CH₃, -NHOH, -NHCH₃, and

R¹ and R² are the same or different and are each selected from

6-mercaptopurinyl, 5-fluorouracily, prednisolyl, salicyl-. hydrazidyl, 1-allyl-2-thiouracilyl, hydroxylamine, isoamidyl, or is an inorganic group consisting of -OH, -SH, -F, -J, -CCl₃, or an organic group consisting of -O-CH₃, -O-CH₂CH₃, -O-CH=CH₂, -O-C₆H₅ or benzhydrol; or an aminoehtyl residue, or an ether group forming oxonium salts consisting of ClCH₂OCH₂Cl, CH₃OCH₂CH₂OCH₃, CH₂ClCH₂OCH₂CH₂Cl, C₄H₉OCH₃, (C₆H₅)₂O,

(CH₂=CHCH₂)₂O, CH₂=CHOCH=CH₂, C₄H₉OC₄H₉, C₆H₅OCH₃, CH₃-O-CHCl₂, ClCH₂-O-C₂H₅, OHCH₂CH₂-O-CH₂CH₂Cl, ClCH₂CHCl-C₂H, and Mt as a metal atom; and wherein the

residue can optionally be changed to a linear, branched or cyclic alkyl having 1 to 6 carbon atoms, halogen or a Hg:N-(C₁-C₆) alkyl group.
The invention further relates to a process for the preparation of the novel sulfonyl compounds and derivatives thereof, as well as for a process for manufacturing a pharmaceutical composition containing the novel sulfonyl compound as an active ingredient. Such novel sulfonyl compound are for example capable in the use for inhibitung tissue growth.
摘要翻译：本发明涉及新的磺酰化合物，其中R'和R“相同或不同，各自为氢，-COCHR 4，-COC（R 4）3 -SO 2 CH 3，-COOCH 2 CH 3， CH 2 -CH 2 -CH 2 R 4，-CONH-CH 2 CH 2 R 4，-CONHCH 2 COOCH 2 CH 3，-CH 2 CH 2 OCONH 2和R 4是Cl或选自下列的残基：CHCO 2 -NHCOCH 2 CH 2 OH，-NHCOCH 2 CH 3，-NHOH，-NHCH 3和CHEM R 1和R 2相同或不同，各自选自6-巯基嘌呤，5-氟尿苷，泼尼松
林，水杨酰基。或者是由-OH，-SH，-F，-J，-CCl 3或由-O-CH 3，-O-（C 1 -C 3）组成的有机基团的无机基团， CH 2 CH 3，-O-CH = CH 2，-O-C 6 H 5或二苯基甲醇; 或C 6 H 9 OCH 3，（C 6 H 5）2 O，CH CH 2（CH 2 = CHCH 2）2 O，CH 2 = CHOCH = CH 2，C 4 H 9 OC 4 H 9，C 6 H 5 OCH 3，CH 3 -O（CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2） -CHCl 2，ClCH 2 -O-C 2 H 5，OHCH 2 CH 2 -O-CH 2 CH 2 Cl，ClCH 2 CHCl-C 2 H和Mt作为金属原子; 并且其中所述残基可任选地改变为具有1至6个碳原子的直链，支链或环状烷基，卤素或Hg：N-（C 1 -C 6）烷基。本发明还涉及制备新的磺酰基化合物及其衍生物的方法，以及制备含有新型磺酰化合物作为活性成分的药物组合物的方法。这样的新型磺酰化合物例如能够用于抑制组织生长。

149. 发明公开

EP0318990A3 Compositions possessing pheromone-like activity 失效
标题翻译：具有类似活动的组合物
公开(公告)号：EP0318990A3
公开(公告)日：1990-09-12
申请号：EP88120067.9
申请日：1988-12-01
申请人： PHILLIPS PETROLEUM COMPANY
发明人： Byers, Jim Don , Drake, Charles Alfred
IPC分类号： C07C45/29 , C07C45/30 , C07C47/21 , C07F5/06 , C07F3/02 , C07F5/02 , C07C29/09 , C07C33/025 , C07C6/06 , A01N35/02
CPC分类号： C07C47/21 , A01N35/02 , C07C6/06 , C07C33/025 , C07C45/29 , C07C45/292 , C07C45/305 , Y02P20/582 , A01N2300/00 , C07C11/12
摘要： The present invention relates to a process for producing an E,Z-9-alkenyl-1-aldehyde component which comprises:
a) disproportionating cyclooctene and an α-olefin in the presence of a suitable disproportionation catalyst under disproportionation conditions suitable to form a 1,9-alkadiene; b) reacting the 1,9-alkadiene obtained in step (a) with a suitable metallating agent under conditions suitable to form a 1-metallo-9-alkene; c) contacting the 1-metallo-9-alkene obtained in step (b) with oxygen under conditions suitable to form a 1-oxymetallo-9-alkene; d) hydrolysing the 1-oxymetallo-9-alkene suit a suitable hydrolysing agent, under suitable hydrolysing conditions to form E,Z-9-alkenyl-1-alcohol. e) oxidizing said E,Z-9-alkenyl-1-alcohol with a suitable oxidizing agent under oxidizing conditions suitable to form E,Z-9-alkenyl-1-aldehyde. Another aspect of the invention pertains to a composition comprising Z-11-hexadecen-1-al, Z-9-tetradecen-1-al and E-9-tetradecen-1-al admixed in sufficient quantities to possess pheromone-like activity for Heliothis zea and Heliothis virescens .

150. 发明公开

EP0294354A3 Preparation of hydrocarbyloxy-magnesium halides 失效
标题翻译：碳氢化合物镁盐的制备
公开(公告)号：EP0294354A3
公开(公告)日：1990-08-08
申请号：EP88850197.0
申请日：1988-06-03
申请人： LITHIUM CORPORATION OF AMERICA
发明人： Mehta, Vijay C.
IPC分类号： C07C29/70 , C07C37/66 , C07C31/30 , C07C39/235 , C07F3/02
CPC分类号： C07C29/70 , C07C37/66 , C07C39/235 , C07C31/30
摘要： The present invention provides a process for making hydrocarbyloxymagnesium halides by reacting in an inert atmosphere under anhydrous conditions activated magnesium metal with an oxygen containing compound of 1 to 20 carbon atoms and an anhydrous hydrogen halide to produce a hydrocarbyloxymagnesium halide.

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