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91. 发明公开

EP0884306A3 Synthesis of amido acids from Carboxylic acids and lactams 失效
标题翻译：从羧酸和内酰胺酰氨基酸生产
公开(公告)号：EP0884306A3
公开(公告)日：1999-12-22
申请号：EP98114127.8
申请日：1994-09-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： Heinzman, Stephen Wayne , Dupont, Jeffrey Scott , Tettenhorst, William Curtis
IPC分类号： C07C231/08 , C07C231/12 , C07C303/32 , C07C303/06 , C07C303/22
CPC分类号： C07C303/06 , C07C231/08 , C07C231/12 , C07C303/22 , C07C303/32 , Y02P20/582 , C07C309/43
摘要： Chemical synthesis of amido acids, and their conversion to amido acid phenyl ester sulfates for use as bleach activators, starting from carboxylic acids and lactams.

92. 发明公开

EP0957085A1 A process for the preparation of sulphonated distyryl-biphenyl compounds 有权
标题翻译： Verfahren zur Herstellung vonulfierten Distyrylbiphenylverbindungen
公开(公告)号：EP0957085A1
公开(公告)日：1999-11-17
申请号：EP99810384.0
申请日：1999-05-04
申请人： Ciba Spezialitätenchemie Holding AG (Ciba Spécialités Chimiques Holding SA) (Ciba Specialty Chemicals Holding Inc.)
发明人： Reinehr, Dieter , Metzger, Georges , Cuesta, Fabienne , Planchenault, Denis , Signoret, Eric
IPC分类号： C07C303/22 , C07C309/32 , C07C303/32 , C07C309/47 , C07C303/06 , D06L3/12 , C11D3/42 , D21H21/30
CPC分类号： C07C309/46 , C07C303/06 , C07C303/22 , C07C303/32 , C11D3/42 , D06L4/621 , D21H21/30 , C07C309/32 , C07C309/44
摘要： A process for the preparation of sulphonated distyryl-biphenyl compounds of formula:
in which R 1 represents hydrogen, C 1 -C 5 alkyl, C 1 -C 5 alkoxy or halogen, R 1A represents hydrogen, C 1 -C 5 alkyl, C 1 -C 5 alkoxy or halogen and M represents hydrogen, an alkaline- or alkaline earth-metal, or ammonium, characterised by reacting a compound of formula:
in which R 2 represents C 1 -C 5 alkyl, with a compound of formula:
whereby R 3 represents phenyl, optionally substituted by C 1 -C 4 alkoxy, halogen or SO 3 M, or C 1 -C 12 alkyl, R 4 represents C 2 -C 6 alkylene, and M, R 1 and R 1A are defined as above, in an alcoholic or dipolar aprotic solvent and in the presence of a strong base. Novel compounds of formulae (3) and (4) and a process for their preparation.
Use of the sulphonated distyryl-biphenyl compounds prepared by the instant process as optical brightening agents in textiles, detergents and paper.
摘要翻译：制备下式的磺化二苯乙烯基联苯化合物的方法：其中R 1表示氢，C 1 -C 5烷基，C 1 -C 5烷氧基或卤素，R 1A表示氢，C 1 -C 5烷基，C 1 -C 5烷氧基或卤素 M表示氢，碱金属或碱土金属或铵，其特征在于使下式化合物：其中R 2表示C 1 -C 5烷基的化合物与下式化合物反应：其中R 3表示苯基，任选被C 1 -C 4烷氧基，卤素或SO 3 M或C 1 -C 12烷基取代，R 4表示C 2 -C 6亚烷基，并且M，R 1和R 1A如上定义，在醇或偶极非质子溶剂中和在强碱存在下。式（3）和（4）的新型化合物及其制备方法。使用本方法制备的磺化二苯乙烯基 - 联苯化合物作为纺织品，洗涤剂和纸张中的荧光增白剂。

93. 发明授权

EP0765306B1 ALKYL SULFOACETATE COMPOSITIONS AND METHODS FOR PREPARING SAME 失效
标题翻译：烷基磺基乙酸盐组合物和方法及其
公开(公告)号：EP0765306B1
公开(公告)日：1999-10-20
申请号：EP95923038.4
申请日：1995-06-13
申请人： STEPAN COMPANY
发明人： THOMPSON, Ralph , ROCKWELL, Ned, M. , MICHELS, Ann, M. , MOHRING, William, R. , KOLBE, Kevin, C. , SIEBOLD, J., Duke , BUTTERWICK, James, M.
IPC分类号： C07C303/32 , C07C303/02 , C07C309/17 , C11D1/12 , A61K7/16
CPC分类号： A61Q11/00 , A61K8/466 , C07C303/02 , C07C303/32 , C11D1/28 , C07C309/17

94. 发明授权

EP0693468B1 A method of making Diaryliodonium fluoroalkyl sulphonate salts 失效
标题翻译：二芳基碘鎓氟烷基磺酸盐的制备方法
公开(公告)号：EP0693468B1
公开(公告)日：1999-06-09
申请号：EP95401727.3
申请日：1995-07-20
申请人： MINNESOTA MINING AND MANUFACTURING COMPANY
发明人： Vogel, Dennis E., c/o Minnesota Mining and , Vogel, Kim M., c/o Minnesota Mining and
IPC分类号： C07C17/263 , C07C25/18 , C07D347/00 , C07C303/32 , C07C309/06
CPC分类号： C07D347/00 , C07C17/12 , C07C25/18 , C07C303/32 , C07C309/06

95. 发明公开

EP0727415A1 Process for the synthesis of fluorinated sulphonic acids 失效
标题翻译： Verfahren zur Herstellung von fluoriertenSulfonsäureverbindungen
公开(公告)号：EP0727415A1
公开(公告)日：1996-08-21
申请号：EP96101465.1
申请日：1996-02-02
申请人： Haldor Topsoe A/S
发明人： Hommeltoft, Sven Ivar , Ekelund, Ole , Zavilla, John
IPC分类号： C07C309/06 , C07C303/32 , C07C303/44
CPC分类号： C07C303/32 , C07C309/06
摘要： Process for the preparation of a fluorinated sulphonic acid compound by hydrolysis of a corresponding fluorinated sulphonyl fluoride, wherein the hydrolysis is carried out in the presence of a tertiary amine, comprising steps of recovering a mixture of a salt of hydrolysed fluorinated sulphonyl fluoride with the tertiary amine and an ammonium fluoride salt of the tertiary amine;
reacting the salt mixture with a sulphonyl compound of the general formula R-SO 2 X, wherein

R = an alkyl group, Cl, F; and
X = Br, Cl
thereby exchanging fluoride of the ammonium fluoride salt in the mixture with the X atom of the sulphonyl compound and converting the sulphonyl compound to a sulphonyl fluoride; and
distilling off the sulphonyl fluoride from the reacted salt mixture.
摘要翻译：通过水解相应的氟化磺酰氟制备氟化磺酸化合物的方法，其中水解在叔胺存在下进行，包括以下步骤：将水解的氟化磺酰氟盐与三级胺和叔胺的氟化铵盐; 使盐混合物与通式为R-SO 2 X的磺酰化合物反应，其中R =烷基，Cl，F; 和X = Br，Cl，从而将氟化铵与磺酰化合物的X原子交换在混合物中，并将磺酰基化合物转化为磺酰氟; 并从反应的盐混合物中蒸馏出磺酰氟。

96. 发明公开

EP0697387A3 Improved method for the preparation of iodonium salts 失效
标题翻译：改进的碘盐制备方法
公开(公告)号：EP0697387A3
公开(公告)日：1996-03-27
申请号：EP95305639.7
申请日：1995-08-11
申请人： DOW CORNING CORPORATION
发明人： Cannady, John Patrick , Wargo, Scott Eric
IPC分类号： C07C17/12 , C07C25/02 , C07C303/32 , C07C309/06
CPC分类号： C07C303/32 , C07C17/12 , C07C25/06 , C07C309/06
摘要： The present invention relates to an improved method for the preparation of iodonium salts. More specifically, the present invention relates to an improved method for the production of symmetric or asymmetric diaryliodonium triflate (trifluoromethane sulfonate) salts. The diaryliodonium salts of the present invention are useful as photoacid catalysts for use in acid-sensitive polymerization and in curing systems such as radiation curable release coating compositions.
摘要翻译：本发明涉及一种制备碘鎓盐的改进方法。更具体地说，本发明涉及制备对称或不对称二芳基碘鎓三氟甲磺酸盐（三氟甲烷磺酸盐）的改进方法。本发明的二芳基碘鎓盐可用作用于酸敏聚合反应和固化体系如可辐射固化防粘涂料组合物中的光酸催化剂。

97. 发明授权

EP0599385B1 Process for preparing sulfonated paraffins with a larger content of polysulfonated species 失效
标题翻译：一种用于具有大含量多磺化的化合物的制备磺化链烷烃过程
公开(公告)号：EP0599385B1
公开(公告)日：1996-03-20
申请号：EP93203194.1
申请日：1993-11-16
申请人： ENIRICERCHE S.p.A. , ENICHEM AUGUSTA INDUSTRIALE S.r.l.
发明人： Marcotullio, Armando , Tinucci, Laura , Ciali, Massimo
IPC分类号： C07C303/14 , C07C303/32 , C07C309/04 , E21B43/22
CPC分类号： C09K8/94 , C07C303/14 , C07C303/32 , C09K8/38 , C07C309/05

98. 发明公开

EP0594297A1 Process for preparing fatty acid esters and amides of sulfonic acid salts 失效
标题翻译： Verfahren zur Herstellung vonFettsäureesternund -amiden vonSulfonsäuresalzen。
公开(公告)号：EP0594297A1
公开(公告)日：1994-04-27
申请号：EP93307155.7
申请日：1993-09-10
申请人： RHONE-POULENC SURFACTANTS AND SPECIALTIES, L.P.
发明人： Tracy, David J. , Wall, Gordon , Ferguson, Mitchell B.
IPC分类号： C07C303/32 , C07C309/12 , C07C309/15
CPC分类号： C07C303/32 , C07C309/12 , C07C309/15
摘要： Fatty acid esters of hydroxyalkylsulfonates and fatty acid amides of aminoalkylsulfonates are prepared by heating an excess of the fatty acids with the sulfonate until the water of condensation is removed. The excess fatty acid is removed by distillation and the isolated fatty acid ester or amide product is directly and rapidly cooled to minimize decomposition and color degradation.
摘要翻译：氨基烷基磺酸盐的羟基烷基磺酸酯和脂肪酸酰胺的脂肪酸酯通过用磺酸盐加热过量的脂肪酸直到除去水来制备。通过蒸馏除去过量的脂肪酸，并将分离的脂肪酸酯或酰胺产物直接且快速冷却以使分解和颜色降解最小化。

99. 发明公开

EP0582248A1 Verfahren zur Herstellung von 3-Sulfobenzoesäure und deren Alkalisalzen 失效
标题翻译： Verfahren zur Herstellung von 3-Sulfobenzoesäureund deren Alkalisalzen。
公开(公告)号：EP0582248A1
公开(公告)日：1994-02-09
申请号：EP93112349.1
申请日：1993-08-02
申请人： HOECHST AKTIENGESELLSCHAFT
发明人： Meier, Michael, Dr.
IPC分类号： C07C303/22 , C07C303/32 , C07C309/58
CPC分类号： C07C303/22 , C07C303/32 , C07C309/58
摘要： Die vorliegende Erfindung betrifft ein Verfahren zur Herstellung von 3-Sulfobenzoesäure und/oder deren Alkalisalzen, indem man 3-Benzoesäuresulfochlorid mit Wasser und einem mit Wasser nicht mischbaren, 3-Sulfobenzoesäure nicht oder nur gering lösendem Lösungsmittel vermischt, aus dem Gemisch Wasser durch Azeotropdestillation entfernt, abkühlt und die gebildete 3-Sulfobenzoesäure gegebenenfalls mit Alkalihydroxid und/oder einer Alkalihydroxid bildenden Substanz versetzt und Wasser erneut durch Azeotropdestillation entfernt.
摘要翻译：本发明涉及通过将3-氯磺酰基苯甲酸与水和不溶于或仅轻微溶解3-磺基苯甲酸的水不混溶溶剂混合来制备3-磺基苯甲酸和/或其碱金属盐的方法，通过共沸蒸馏，冷却和任选地处理由碱金属氢氧化物和/或形成碱金属氢氧化物的物质形成的3-磺基苯甲酸并通过共沸蒸馏再次除去来自混合物的水。

100. 发明公开

EP0506308A1 Method for sulfonating acyloxybenzenes and neutralization of resulting product 失效
标题翻译： Verfahren zur Sulfonierung von Acyloxybenzolen und zur Neutralisierung der resultierenden Produkte。
公开(公告)号：EP0506308A1
公开(公告)日：1992-09-30
申请号：EP92302417.8
申请日：1992-03-20
申请人： The Clorox Company
发明人： Ottoboni, Thomas B. , Zielske, Alfred G. , Kuhner, Lisa M. , Brodbeck, Kevin J. , Sinisi, Leonardo , Martin, Gregory T. , Spillett, Cris Tina , Thompson, Suzanne M. , Steichen, Dale S.
IPC分类号： C07C309/42 , C07C303/32 , C07C303/06
CPC分类号： C11D3/3907 , C07C303/06 , C07C303/32 , C07C309/42
摘要： A method is provided for sulfonating an acyloxy substituted benzene ring to obtain high yields of desired sulfonated compounds that are useful as cleaning, bleaching, or fabric treating additives. A particularly preferred additive so prepared has the structure

where R⁷ is a branched or unbranched alkyl with about 5 to 9 carbons and M is an alkali metal, an alkaline earth metal, or ammonium. The benzene ring is sulfonated by contacting with a molar excess of sulfur trioxide source and then irreversibly reacting the sulfur trioxide excess with a quenching agent. A neutralization process for preparing peracid precursors in high yield by neutralizing sulfonated aryl esters is also provided.
摘要翻译：提供了用于磺化酰氧取代的苯环以获得高产率的用作清洁，漂白或织物处理添加剂的所需磺化化合物的方法。如此制备的特别优选的添加剂具有结构，其中R 7是具有约5至9个碳的支链或非支链烷基，M是碱金属，碱土金属或铵。苯环通过与摩尔过量的三氧化硫源接触而磺化，然后使三氧化硫过氧化物与猝灭剂不可逆地反应。还提供了通过中和磺化芳基酯以高产率制备过酸前体的中和方法。

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