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91. 发明公开

EP1500432A4 METHOD FOR PREPARING RUTHENIUM-CARRYING ALUMINA AND METHOD FOR OXIDIZING ALCOHOL 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG EINES RUTHENIUMTRAGENDEN ALUMINIUMOXIDS UND VERFAHREN ZUR ALKOHOLOXIDATION
公开(公告)号：EP1500432A4
公开(公告)日：2006-02-08
申请号：EP03717729
申请日：2003-04-25
申请人： SUMITOMO CHEMICAL CO
发明人： MIZUNO NORITAKA , YAMAGUCHI KAZUYA , ISHIDA HAJIME
IPC分类号： B01J21/04 , B01J23/46 , B01J37/03 , C07B61/00 , C07C45/38 , C07C45/39 , C07C47/02 , C07C47/127 , C07C47/21 , C07C47/232 , C07C47/54 , C07C47/55 , C07C47/575 , C07C49/04 , C07C49/203 , C07C49/395 , C07C49/403 , C07C49/413 , C07C49/78 , C07C51/235 , C07C53/126 , C07C201/12 , C07C205/44 , C07D333/22 , C07C27/00 , C07C47/542 , C07C49/792
CPC分类号： C07D333/22 , B01J21/04 , B01J23/462 , B01J37/031 , C07C45/38 , C07C45/39 , C07C51/235 , C07C53/126
摘要： A ruthenium-carrying alumina, which is prepared by suspending alumina in a solution containing trivalent ruthenium and adding a base to the suspension, is provided. This ruthenium-carrying alumina is useful as a catalyst for oxidizing alcohols by contacting the alcohols with molecular oxygen, and can be used for oxidizing the alcohols at a high conversion to produce ketones, aldehydes, carboxylic acids, etc. with good productivity.
摘要翻译：提供了一种载持钌的氧化铝，其通过将氧化铝悬浮在含有三价钌的溶液中并将悬浮液加入碱中来制备。该载持钌的氧化铝可用作通过使醇与分子氧接触来醇化的催化剂，并且可以以高转化率用于氧化醇，以生产良好的酮，醛，羧酸等。

92. 发明公开

EP1397336A4 PREPARATION OF POLYARYL CARBOXYLIC ACIDS 审中-公开
标题翻译： HERSTELLUNG VONPOLYARYLCARBONSÄUREN
公开(公告)号：EP1397336A4
公开(公告)日：2005-12-21
申请号：EP02719069
申请日：2002-02-26
申请人： HONEYWELL INT INC
发明人： QIAN ZHENRONG , SU HENG ERIC , DEWITT LEE ALAN
IPC分类号： C07B37/04 , C07C51/367 , C07C63/333 , C07C27/00 , C07C63/33 , C07C63/36 , C07C65/00 , C07D309/00
CPC分类号： C07B37/04 , C07C51/367 , C07C65/24
摘要： Disclosed are methods for preparing polyaromatic carboxylic acids or salts thereof by reacting an aromatic boronic acid with a haol-substituted aromatic carboxylic acid or salt thereof.
摘要翻译：公开了通过芳族硼酸与卤素取代的芳族羧酸或其盐的反应制备聚芳族羧酸或其盐的方法。

93. 发明公开

EP1268383A4 CATALYTIC OXIDATION OF ORGANIC SUBSTRATES BY TRANSITION METAL COMPLEXES IN ORGANIC SOLVENT MEDIA EXPANDED BY SUPERCRITICAL OR SUBCRITICAL CARBON DIOXIDE 有权
标题翻译：有机底使用有机溶剂，用超或亚临界二氧化碳的过渡金属络合物催化氧化正在扩大
公开(公告)号：EP1268383A4
公开(公告)日：2005-12-14
申请号：EP01928364
申请日：2001-04-03
申请人： UNIV KANSAS
发明人： SUBRAMANIAM BALA , BUSCH DARYLE H , MUSIE GHEZAI T , WEI MING
IPC分类号： C07D301/08 , C07B33/00 , C07B41/00 , C07B61/00 , C07C27/12 , C07C29/50 , C07C35/14 , C07C35/18 , C07C45/33 , C07C45/34 , C07C46/04 , C07C46/08 , C07C49/603 , C07C49/713 , C07C50/02 , C07C50/08 , C07D301/06 , C07D303/04 , C08F2/46 , C07C45/00 , C07B41/02 , C07B41/04 , C07C27/00 , C07C29/03 , C07C37/00 , C07C41/00 , C07C49/105 , C07C67/00
CPC分类号： C07D303/04 , C07B41/00 , C07C27/12 , C07C29/50 , C07C45/34 , C07C46/08 , C07C2601/14 , C07C2601/16 , C07D301/06 , Y02P20/544 , C07C49/713 , C07C49/603 , C07C35/14 , C07C35/18
摘要： Improved oxidation methods are provided wherein a reaction mixture comprising a substrate to be oxidized (e.g., phenols, alkenes) and an oxidation catalyst (typically dispersed in an organic solvent system) is supplemented with a compressed gas which expands the reaction mixture, thus accelerating the oxidation reaction. In preferred practice pressurized subcritical or supercritical carbon dioxide is used as the expanding gas, which is introduced into the reaction mixture together with an oxidizing agent. The inventive methods improve the substrate conversion and product selectivity by increasing the solubility of the oxidizing agent in the reaction mixture.

94. 发明公开

EP1288183A4 PROCESS FOR PREPARING UNSATURATED COMPOUNDS BY PYROLYSIS 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VONUNGESÄTTIGTENVERBINDUNGEN DURCH PYROLYSE
公开(公告)号：EP1288183A4
公开(公告)日：2005-01-26
申请号：EP01908356
申请日：2001-03-06
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , TATEMATSU SHIN , SATO MASAKUNI , MUROFUSHI HIDENOBU , YANASE KOICHI , SUZUKI YASUHIRO
IPC分类号： C07C41/18 , C07C43/17 , C07C43/172 , C07C41/01 , C07C27/00 , C07C51/58
CPC分类号： C07C43/17 , C07C41/18 , C07C41/28 , C07C43/172 , C07C2601/14
摘要： A process for preparing unsaturated compounds of the general formula (2) useful as raw materials for the production of fluororesins or the like in a few steps and in high yield by using compounds of the general formula (1) as the starting material. Specifically, a process for preparing compounds represented of the general formula (2): CR?bRc=CRdRe¿ (including CF¿3?CF2CF2OCF=CF2) by pyrolysis of a compound having at least one partial structure represented by the general formula (1): -COOCF2CR?bRc-CXRdRe¿, for example, CF¿3?CF2CF2OCF(CF3)COOCF2CF-(CF3)OCF2CF2CF3, with R?b to Re¿ being each hydrogen, halogeno, a monovalent organic group which is not converted by pyrolysis, or the like.
摘要翻译：本发明通过使用式1的化合物作为起始原料，制备可用作氟树脂原料等的不饱和化合物（式2）。也就是说，本发明提供了通过热解具有至少一个部分的化合物的化合物来制备由CR 3 R c = CR d R e（式2）表示的化合物如CF 3 CF 2 CF 2 OCF = CF 2的方法由CF 3 CF 2 CF 2 OCF（CF 3）COOCF 2 CF（CF 3）OCF 2 CF 2 CF 3表示的结构表示的结构，其中R 1至R e为氢原子，卤原子或通过热解反应不可改变的一价有机基团。

95. 发明公开

EP1470096A1 METHOD FOR REDUCING WATER CONCENTRATION IN A MULTI-PHASE COLUMN REACTOR 审中-公开
标题翻译：一种用于减少水的浓度在多相柱反应器
公开(公告)号：EP1470096A1
公开(公告)日：2004-10-27
申请号：EP02797370.0
申请日：2002-12-16
申请人： ConocoPhillips Company
发明人： ZHANG, Jianping , ESPINOZA, Rafael, L.
IPC分类号： C07C27/00 , B01D37/00 , B01D21/26 , B01D63/00 , B01D3/42 , B01D15/00 , B01D3/34 , B01D11/00 , B01D3/14
CPC分类号： B01J8/228 , B01J8/008 , B01J2208/00761 , B01J2208/00991 , C10G2/32 , C10G2/332 , C10G33/00 , C10G2300/1022
摘要： The present invention relates to a method and apparatus for water removal in multi-phase reactors operating at Fischer-Tropsch conditions. In a preferred embodiment of the present invention, a method of reducing the concentration of water in a multi-phase reactor for Fisher-Tropsch synthesis containing an expanded slurry bed and a water-rich slurry region includes removing a portion of water from the water-rich slurry from a predetermined region in the reactor, removing the water from the water-rich slurry to form a water-reduced slurry, and returning the water-reduced slurry back to the reactor. Preferably the water-rich slurry region is located between 1/2 H to H and 1/2 R to R, where H is the height of the expanded slurry bed and R is the radius of the expanded slurry bed.

96. 发明公开

EP1461343A2 MANUFACTURE OF TRIALKYLALUMINUM COMPOUNDS AND ALPHA-ALCOHOLS 审中-公开
标题翻译：制造三烷基铝和ALPHA醇
公开(公告)号：EP1461343A2
公开(公告)日：2004-09-29
申请号：EP02805575.4
申请日：2002-12-12
申请人： E.I. du Pont de Nemours and Company
发明人： CITRON, Joel, David
IPC分类号： C07F5/06 , C07C27/00
CPC分类号： C07F5/063 , C07C29/09 , C07C29/68 , C07C31/32 , C07C31/125
摘要： Higher trialkylaluminum compounds may be made by forming α-olefin by oligomerizing ethylene using a transition metal containing catalyst, reacting the α-olefins formed with a lower trialkylaluminum compound to form higher trialkylaluminum compound(s). These may optionally be oxidized, as with oxygen, to form higher trialkoxyaluminum compound, which in turn may be hydrolyzed to α-alcohols. In one variation of the process lower α-olefins and higher (relatively) α-alcohols may be formed and isolated. Higher trialkylaluminum compounds and α-alcohols are useful as chemical intermediates, while lower α-olefins are useful as monomers for polyolefins.

97. 发明公开

EP1442002A1 HIGH TEMPERATURE HYDROCARBON CRACKING 审中-公开
标题翻译：高温碳氢化合物开裂
公开(公告)号：EP1442002A1
公开(公告)日：2004-08-04
申请号：EP02776241.8
申请日：2002-10-18
申请人： Bullin, Keith A. , Cantrell, Joel G.
发明人： Bullin, Keith A. , Cantrell, Joel G.
IPC分类号： C07C27/00 , C07C2/00 , C07C11/00 , C07C2/56
CPC分类号： C10G57/02 , C07C2/76 , C10G50/00 , C10G2400/24
摘要： A process for converting natural gas to a liquid hydrocarbon wherein the natural gas feed stream is admixed with a hot gas stream, the hot gas stream being at a temperature sufficient to effect a chemical reaction forming an intermediate product stream containing reactive hydrocarbons, the intermediate product stream being quenched and subsequently reacted in a liquefaction zone to produce hydrocarbon liquids, hydrocarbon gases from the liquefaction zone being recycled to the natural gas feed stream, hydrocarbon liquid product being recovered from the liquefaction zone.
摘要翻译：一种将天然气转化成液态烃的方法，其中天然气进料流与热气流混合，热气流的温度足以进行化学反应，形成含有反应性烃的中间产物流，中间产物将液流骤冷并随后在液化区反应以生产烃液体，将来自液化区的烃气再循环至天然气进料流，从液化区回收烃液体产物。

98. 发明公开

EP1414774A2 OPTIMIZING THE PRODUCTION RATE OF SLURRY BUBBLE REACTORS BY USING LARGE GAS FLOW RATES AND MODERATE SINGLE PASS CONVERSION 审中-公开
标题翻译：优化浆态鼓泡反应器的生产速度采用高气体流速和适度转换过程在一个通
公开(公告)号：EP1414774A2
公开(公告)日：2004-05-06
申请号：EP02759188.2
申请日：2002-07-25
申请人： Conoco Inc.
发明人： ZHANG, Jianping , WRIGHT, Harold, A.
IPC分类号： C07C27/00
CPC分类号： C10G2/342 , B01J8/1809 , B01J8/22 , B01J2208/00274 , B01J2208/003 , B01J2208/00539 , B01J2208/00548 , B01J2219/00006 , B01J2219/00038 , B01J2219/0004
摘要： A gas-agitated multiphase reactor system that is effective for enabling maximum reactor productivity or minimizing reactor volume comprising at least two stages with or without recycle, wherein inlet gas superficial velocity is at least 20 cm/sec at Fischer-Tropsch synthesis, yielding a total syngas conversion of greater than about 90%, while syngas conversion in each reactor is less than 60%. More specifically, the total reactor volume is held to a minimum such that minimum reactor volume is less than 0.02 cubic meters total reactor volume/(kg C5+/hr production).

99. 发明公开

EP1037866A4 A CATALYTIC PROCESS FOR METHANOL SYNTHESIS 审中-公开
标题翻译：催化方法，用于生产甲醇
公开(公告)号：EP1037866A4
公开(公告)日：2004-03-03
申请号：EP98948405
申请日：1998-09-21
申请人： STAUFFER JOHN E
发明人： STAUFFER JOHN E
IPC分类号： B01J27/122 , C07C17/158 , C07C29/124 , C07C27/00
CPC分类号： C07C17/158 , B01J27/122 , C07C29/124 , Y02P20/52 , C07C19/01 , C07C31/04
摘要： A new catalytic process is provided for the synthesis of methyl alcohol by a catalytic reaction where methyl chloride, perchloroethylene, hydrogen chloride, and oxygen are converted to methyl alcohol and hexachloroethylene. The catalytic process is an admixture of an iodine salt with copper chloride enhanced as needed by a chloride of iron, zinc, lead or bismuth or an admixture of an alkali metal bromine salt such as sodium bromide, potassium bromide and cesium bromide substituted for the iodine salt.

100. 发明公开

EP1179519A1 PRECURSORS OF 3-ALKOXYALKANOLS AND PROCESSES FOR THE PREPARATION OF 3-ALKOXYALKANOLS 审中-公开
标题翻译： VORSTUFEN VON 3-ALKOXYALKANOLEN UND VERFAHREN ZUR HERSTELLUNG VON 3-ALKOXYALKANOLEN
公开(公告)号：EP1179519A1
公开(公告)日：2002-02-13
申请号：EP00927778.1
申请日：2000-05-16
申请人： IDEMITSU PETROCHEMICAL CO., LTD.
发明人： YOSHITOME, Toshihide , KAWASAKI, Hiroshi , KAWANO, Naoya , MIYAMOTO, Shinji
IPC分类号： C07C27/00 , C07C41/50 , C07C43/315 , C07C45/64 , C07C47/198 , C07C45/42 , C07C41/26 , C07C43/13
CPC分类号： C07C45/71 , C07C41/26 , C07C41/28 , C07C41/50 , C07C45/515 , C07C45/84 , C07C47/198 , C07C43/315 , C07C43/13
摘要： Processes for the preparation of 3-alkoxyalkanols useful as solvents for coating materials, photoresists, or the like.
Specifcally,

(1) a process which comprises reacting an α,β-unsaturated aldehyde with an alcohol in the presence of an acidic catalyst and subjecting the obtained product to hydrolysis and hydrogenation successively;
(2) a process which comprises subjecting a reaction mixture obtained by the reaction of an α,β-unsaturated aldehyde with an alcohol and comprising the corresponding 1,1,3-trialkoxyalkane and 3-alkoxyalkanal to hydrolysis and hydrogenation at the same time;
(3) a process which comprises recovering a 3-alkoxyalkanal through distillation as an azeotropic mixture thereof with water from a reaction solution obtained by the reaction of an alcohol with acid-containing acrolein or methacrolein prepared by the oxidation of propylene or isobutylene, and hydrogenating the recovered 3-alkoxyalkanal into the corresponding 3-alkoxyalkanol; and
(4) a process which comprises bringing a gas produced by the oxidation of propylene or isobutylene Into contact with an alcohol, conducting the reaction of the gas with the alcohol to form the corresponding 1,1,3-trialkoxyalkane, and subjecting it to hydrolysis and hydrogenation.
摘要翻译：用作制备用作涂料，光致抗蚀剂等的溶剂的3-烷氧基烷醇的方法。具体地，（1）一种方法，其包括在酸性催化剂存在下使α，β-不饱和醛与醇反应，并使所得产物依次水解和氢化; （2）一种方法，其包括使α，β-不饱和醛与醇反应获得的反应混合物与包含相应的1,1,3-三烷氧基烷烃和3-烷氧基烷烃的物质同时进行水解和氢化; （3）一种方法，其包括通过蒸馏作为其与水的共沸混合物从由与丙烯或异丁烯氧化制备的含酸丙烯醛或甲基丙烯醛反应获得的反应溶液中回收3-烷氧基烷烃，并将其氢化将回收的3-烷氧基亚油酸转化为相应的3-烷氧基烷醇; 和（4）一种方法，其包括使由丙烯或异丁烯氧化产生的气体与醇接触，进行气体与醇的反应，形成相应的1,1,3-三烷氧基烷烃，并使其水解和氢化。

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