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    • 97. 发明公开
    • PROCESS FOR ENERGY RECOVERY IN MANUFACTURING CELLULOSE ESTERS
    • 制造纤维素酯中的能量回收过程
    • EP3019534A1
    • 2016-05-18
    • EP14822170.8
    • 2014-07-02
    • Celanese Acetate LLC
    • FALLON, Denis, G.
    • C08B3/16
    • B01D3/36B01D3/009B01D3/143C07C51/46C08B3/00C08B3/22Y02P20/124Y02P20/127Y02P20/57Y02P70/34C07C53/08
    • Integration of an acid recovery system in the manufacturing of cellulose esters may include heat recovery from a carboxylic acid recovery distillation column by solvent extracting a weak acid stream to form a first overhead stream and a first bottoms stream; distilling the first overhead stream in a distillation column to form a second overhead stream and a second bottoms stream; sending at least a portion of the second overhead stream to a heat exchanger via a process inlet; sending a boiler feed water make up stream to the heat exchanger via a water inlet; and cooling the at least a portion of the second overhead stream in the heat exchanger, such that the at least a portion of second overhead stream exits the heat exchanger via a process outlet and the boiler feed water make up stream exits the heat exchanger via a water outlet.
    • 酸回收系统在纤维素酯制造中的集成可包括通过溶剂萃取弱酸流从羧酸回收蒸馏塔中回收热以形成第一塔顶料流和第一塔底料流; 在蒸馏塔中蒸馏所述第一塔顶料流以形成第二塔顶料流和第二塔底料流; 经由过程入口将所述第二顶部料流的至少一部分送至热交换器; 通过进水口将锅炉给水补给到热交换器中; 以及冷却热交换器中的第二塔顶流的至少一部分,使得第二塔顶流的至少一部分经由工艺出口离开热交换器,并且锅炉给水补充流经由热交换器流出热交换器 出水口。