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1. 发明授权

US06610360B2 Buffing diamond-like carbon (DLC) to improve scratch resistance 失效
标题翻译：抛光金刚石碳（DLC），以提高耐刮擦性
公开(公告)号：US06610360B2
公开(公告)日：2003-08-26
申请号：US09994922
申请日：2001-11-28
申请人： Rudolph Hugo Petrmichl , Fabio Reis
发明人： Rudolph Hugo Petrmichl , Fabio Reis
IPC分类号： C23C1626
CPC分类号： C23C14/5886 , C03C17/22 , C03C17/3441 , C03C17/36 , C03C17/3618 , C03C17/3634 , C03C17/3644 , C03C17/3652 , C03C2217/78 , C03C2218/32 , C23C14/0605 , C23C16/26 , Y10T428/30
摘要： Scratch resistance (SR) of a coated article is improved by buffing the coated article after deposition of the layer(s) of the coating. For example, in certain embodiments a diamond-like carbon (DLC) inclusive layer(s) is deposited on a substrate (directly or indirectly), and thereafter buffed in order to improve its scratch resistance.
摘要翻译：通过在涂覆层的沉积之后抛光涂覆的制品来改善涂覆制品的耐划伤性（SR）。例如，在某些实施方案中，将包含金刚石的碳（DLC）层沉积在基底（直接或间接）上，然后抛光以改善其耐刮擦性。

2. 发明授权

US06602371B2 Method of making a curved vehicle windshield 失效
公开(公告)号：US06602371B2
公开(公告)日：2003-08-05
申请号：US09793408
申请日：2001-02-27
申请人： Vijayen S. Veerasamy
发明人： Vijayen S. Veerasamy
IPC分类号： C23C1626
CPC分类号： B32B17/1099 , B32B17/10036 , B32B17/10807 , B32B17/10889 , B60J1/008 , C03B23/0252 , C03B40/00 , C03C17/22 , C03C19/00 , C03C2217/282 , C03C2218/15
摘要： A method of making a vehicle windshield. First and second flat glass sheets are bent together into a shape desired for the windshield. The bent sheets are separated, and an interlayer (e.g., PVB) positioned therebetween. After the sheets have been heat laminated to one another via the interlayer, the convex tin side of the outer sheet is ion beam milled to shave off a portion thereof. Then, a diamond-like carbon (DLC) inclusive coating is deposited using an ion beam(s) on the milled convex shaped surface of the laminate to produce a windshield. In certain optional embodiments, the windshield may be hydrophobic in nature.

3. 发明授权

US06506451B1 Composite structure and process for producing it 失效
标题翻译：复合结构及其生产工艺
公开(公告)号：US06506451B1
公开(公告)日：2003-01-14
申请号：US08647318
申请日：1996-05-09
申请人： Frank Stubhan , Hans-Juergen Fuesser , Mona Ferguson
发明人： Frank Stubhan , Hans-Juergen Fuesser , Mona Ferguson
IPC分类号： C23C1626
CPC分类号： H01L21/02527 , C23C16/02 , C23C16/271 , C23C16/279 , H01L21/02444 , H01L21/02494 , H01L21/02516 , H01L21/0262 , H01L21/02658
摘要： A composite structure having a substantially monocrystalline growth substrate and at least one monocrystalline or polycrystalline layer of diamond or diamond-like material arranged on a surface of the growth substrate, the surface of the growth substrate being provided with crystal growth nuclei having crystal axes which exhibit an inclination of not more than 10%, preferably not more than 7%, with respect to corresponding axes of the crystal lattice of the growth substrate, and a process for producing such a composite structure in which the growth substrate is pretreated and growth nuclei are deposited from a nucleating gas phase of known composition for depositing layers of diamond or diamond-like material, in which during the nucleation the growth substrate is raised to a negative electrical potential relative to the nucleating gas phase.
摘要翻译：一种具有基本单晶生长衬底和布置在生长衬底的表面上的金刚石或类金刚石材料的至少一个单晶或多晶层的复合结构，所述生长衬底的表面设置有具有晶轴的晶体生长核，相对于生长基板的晶格的相应轴线的倾斜度不大于10％，优选不超过7％，以及用于制备其中预处理生长衬底和生长核的复合结构的方法从已知组合物的成核气相沉积，用于沉积金刚石或类金刚石材料层，其中在成核期间，生长衬底相对于成核气相升高至负电位。

4. 发明授权

US06432477B1 Densification of porous bodies 失效
标题翻译：多孔体致密化
公开(公告)号：US06432477B1
公开(公告)日：2002-08-13
申请号：US09857730
申请日：2001-06-08
申请人： Jonathan Graham Peel Binner , Toby John Hutton
发明人： Jonathan Graham Peel Binner , Toby John Hutton
IPC分类号： C23C1626
CPC分类号： H05B6/105 , C04B35/83 , C23C16/045 , C23C16/46 , F16D69/023 , H05B6/36
摘要： A porous preform body is infiltrated with carbon by a thermal gradient process using a multi-portion heating element to heat the body. Selected portions of the heating element are supplied with power to create the thermal gradient between different areas of the preform body.
摘要翻译：多孔预成型体通过使用多部分加热元件的热梯度过程被碳渗透，以加热身体。加热元件的选定部分被供给能量以在预成型体的不同区域之间产生热梯度。

5. 发明授权

US06419997B1 Guide bush and method of forming hard carbon film over the inner surface of the guide bush 失效
标题翻译：引导衬套和在导套内表面上形成硬质碳膜的方法
公开(公告)号：US06419997B1
公开(公告)日：2002-07-16
申请号：US09514896
申请日：2000-02-28
申请人： Yukio Miya , Osamu Sugiyama , Ryota Koike , Takashi Toida , Sosaku Kimura , Kunihiko Kokubo
发明人： Yukio Miya , Osamu Sugiyama , Ryota Koike , Takashi Toida , Sosaku Kimura , Kunihiko Kokubo
IPC分类号： C23C1626
CPC分类号： B23B31/202 , B23B13/125 , B23B2222/28 , B23B2222/88 , B23B2231/2059 , C23C16/0281 , C23C16/045 , C23C16/26 , Y10T279/17418 , Y10T279/17452
摘要： A hard carbon film (15) is formed directly or through an intermediate layer for enhancing adhesion over an inner surface (11b) of a guide bush (11) for holding a workpiece (51) rotatably and axially slidable on an automatic lathe at a position near a cutting tool, to be in sliding contact with the workpiece (51) or directly or through an intermediate layer for enhancing adhesion on the surface of a superhard lining fixed to the inner surface (11b). The guide bush (11) has remarkably enhanced durability and prevents damaging the workpiece (51) and seizing that makes a machining operation impossible even when the guide bush (11) is used for an extended period of time and when the automatic lathe operates for heavy machining. The hard carbon film (15) having satisfactory adhesion to the inner surface (11b) can be efficiently formed in a uniform thickness over the inner surface (11b) by placing the guide bush (11) in a vacuum vessel, extending an auxiliary electrode in the center bore of the guide bush (11) and producing a plasma of a gas containing carbon.
摘要翻译：硬质碳膜（15）直接或通过中间层形成，用于增强在导筒（11）的内表面（11b）上的粘合力，用于保持工件（51）在自动车床上可旋转和轴向滑动的位置靠近切割工具，与工件（51）滑动接触，或直接或通过中间层，以增强固定在内表面（11b）上的超硬衬里的表面上的附着力。引导衬套（11）具有显着增强的耐久性，并且防止损坏工件（51）并且即使当导套（11）长时间使用时也不可能进行加工操作，并且当自动车床操作重加工。通过将引导衬套（11）放置在真空容器中，可以在内表面（11b）上以均匀的厚度有效地形成对内表面（11b）具有令人满意的粘合力的硬质碳膜（15）引导衬套（11）的中心孔并产生含碳气体的等离子体。

6. 发明授权

US06419985B1 Method for producing insulator film 失效
标题翻译：绝缘膜制造方法
公开(公告)号：US06419985B1
公开(公告)日：2002-07-16
申请号：US09578719
申请日：2000-05-26
申请人： Shuichi Ishizuka
发明人： Shuichi Ishizuka
IPC分类号： C23C1626
CPC分类号： H01L21/0212 , B05D1/62 , B05D3/0254 , H01L21/02274 , H01L21/02337 , H01L21/31058 , H01L21/312 , H01L21/3127
摘要： A method for producing an insulator film for use as an interlayer dielectric film in a semiconductor device having a multi-level interconnection structure is disclosed. An inert plasma producing gas, such as argon, is introduced into a vacuum vessel along with a thin film deposition gas, such as a compound gas containing fluorine and carbon. Activation of the plasma producing gas activates the thin film producing gas, resulting in a thin fluorine containing carbon insulator film on the semiconductor device. In order to thermally stabilize the insulator layer, the semiconductor device is annealed.
摘要翻译：公开了一种在具有多层互连结构的半导体器件中制造用作层间绝缘膜的绝缘膜的方法。将惰性等离子体产生气体如氩气与薄膜沉积气体如含氟和碳的复合气体一起引入真空容器中。激活等离子体产生气体激活产生薄膜的气体，在半导体器件上产生薄的含氟碳绝缘膜。为了使绝缘体层热稳定，半导体器件退火。

7. 发明授权

US06410085B1 Method of machining of polycrystalline diamond 有权
标题翻译：多晶金刚石加工方法
公开(公告)号：US06410085B1
公开(公告)日：2002-06-25
申请号：US09682425
申请日：2001-08-31
申请人： Nigel Dennis Griffin , Peter Raymond Hughes
发明人： Nigel Dennis Griffin , Peter Raymond Hughes
IPC分类号： C23C1626
CPC分类号： B22F7/06 , B22F2003/244 , B22F2005/001 , B22F2998/00 , B22F2999/00 , C04B35/52 , C04B35/645 , C04B37/021 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/405 , C04B2235/427 , C04B2235/442 , C04B2237/363 , C04B2237/401 , E21B10/567 , F16C33/043 , F16C2206/04 , Y10T407/27 , Y10T428/12493 , Y10T428/12625 , Y10T428/24942 , Y10T428/26 , Y10T428/265 , Y10T428/30 , B22F2207/03 , B22F1/0014 , C22C26/00
摘要： A method of machining a polycrystalline diamond material including a matrix of interstices containing a catalyzing material and a volume close to a working surface thereof substantially free of catalyzing material which comprises the steps of treating the volume to render the polycrystalline diamond electrically conductive, and using an electron discharge machining technique to machine the polycrystalline diamond. In one embodiment, the treatment comprises applying a conductive material layer to a surface of the diamond.
摘要翻译：一种加工多晶金刚石材料的方法，所述多晶金刚石材料包括含有催化材料的空隙基体和接近其基本上不含催化材料的工作表面的体积，该方法包括以下步骤：处理该体积以使多晶金刚石导电，并使用电子放电加工技术来加工多晶金刚石。在一个实施例中，处理包括将导电材料层施加到金刚石的表面。

8. 发明授权

US06777030B2 Method of ion beam milling a glass substrate prior to depositing a coating system thereon, and corresponding system for carrying out the same 失效
标题翻译：在其上沉积涂层系统之前离子束铣削玻璃基板的方法，以及用于执行其的相应系统
公开(公告)号：US06777030B2
公开(公告)日：2004-08-17
申请号：US10003436
申请日：2001-12-06
申请人： Vijayen S. Veerasamy , Rudolph Hugo Petrmichl
发明人： Vijayen S. Veerasamy , Rudolph Hugo Petrmichl
IPC分类号： C23C1626
CPC分类号： B05D5/083 , B08B17/06 , B08B17/065 , B32B17/1033 , B60S1/54 , B60S1/58 , C03C3/076 , C03C15/00 , C03C15/02 , C03C17/22 , C03C17/3441 , C03C17/3482 , C03C17/36 , C03C17/3634 , C03C17/3644 , C03C17/3652 , C03C17/42 , C03C19/00 , C03C23/006 , C03C23/0075 , C03C2217/282 , C03C2217/76 , C03C2217/78 , C03C2218/151 , C03C2218/31 , C23C16/0272 , C23C16/26
摘要： A glass substrate is ion beam milled in order to smoothen the same and/or reduce or remove nano-cracks in the substrate surface before a coating system (e.g., diamond-like carbon (DLC) inclusive coating system) is deposited thereon. It has been found that such ion beam milling of the substrate prior to deposition of the coating system improves adherence of the coating system to the underlying milled substrate. Moreover, it has surprisingly been found that such ion beam milling of the substrate results in a more scratch resistant coated article when a DLC inclusive coating system is thereafter ion beam deposited on the milled substrate. Amounts sodium (Na) may also be reduced at the surface of the substrate by such milling.
摘要翻译：在涂覆系统（例如包括金刚石碳（DLC）的包覆涂层系统）沉积在其上之前，玻璃基板被离子束研磨以便使其平滑和/或减少或去除衬底表面中的纳米裂纹。已经发现，在沉积涂层系统之前，衬底的这种离子束研磨改善了涂层系统对底层铣削衬底的粘附性。此外，令人惊讶地发现，当其后的DLC包覆涂层系统之后离子束沉积在研磨的基底上时，衬底的这种离子束铣削导致更耐划伤的涂层制品。通过这种研磨，钠（Na）的量也可以在基材的表面上还原。

9. 发明授权

US06699525B2 Method of forming carbon nanotubes and apparatus therefor 失效
标题翻译：形成碳纳米管的方法及其装置
公开(公告)号：US06699525B2
公开(公告)日：2004-03-02
申请号：US09835757
申请日：2001-04-16
申请人： Ahalapitiya H. Jayatissa
发明人： Ahalapitiya H. Jayatissa
IPC分类号： C23C1626
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C23C16/0281 , C23C16/26 , C23C16/44 , C30B25/02 , C30B29/605 , Y10S427/102 , Y10S977/731 , Y10S977/843 , Y10S977/847
摘要： Carbon nanotubes are formed on a substrate by providing a coiled filament in a chemical vapor deposition chamber, supporting a substrate having a catalytic coating provided thereon inside the coiled filament, evacuating air, if present, from the chamber, heating the filament and applying a bias voltage between the filament and the substrate, introducing a reactant gas into the chamber, and pyrolyzing the reactant gas to deposit the carbon nanotubes on the catalytic coating. The substrate can be in the form of a rod or fiber and the carbon nanotubes can be deposited in a radially extending cluster on the substrate. The present invention also contemplates an apparatus for carrying out the inventive method.
摘要翻译：碳纳米管通过在化学气相沉积室中提供螺旋丝而形成在基底上，支撑在其内部设置有催化剂涂层的基底，从腔室排出空气（如果存在），加热细丝并施加偏压在灯丝和衬底之间施加电压，将反应气体引入室中，并热解反应气体以将碳纳米管沉积在催化涂层上。衬底可以是棒或纤维的形式，并且碳纳米管可以沉积在衬底上的径向延伸的簇中。本发明还考虑了用于实施本发明方法的装置。

10. 发明授权

US06660342B1 Pulsed electromagnetic energy method for forming a film 失效
标题翻译：用于形成薄膜的脉冲电磁能法
公开(公告)号：US06660342B1
公开(公告)日：2003-12-09
申请号：US09636222
申请日：2000-08-10
申请人： Akiharu Miyanaga , Tohru Inoue , Shunpei Yamazaki
发明人： Akiharu Miyanaga , Tohru Inoue , Shunpei Yamazaki
IPC分类号： C23C1626
CPC分类号： C23C16/26 , C23C16/515 , C23C16/517 , H01J37/32192 , H01J37/32266 , H01J37/32678 , Y10S427/103 , Y10S427/104
摘要： A method of forming a film by a plasma CVD process in which a high density plasma is generated in the presence of a magnetic field wherein the electric power for generating the plasma has a pulsed waveform. The electric power typically is supplied by microwave, and the pulsed wave may be a complex wave having a two-step peak, or may be a complex wave obtained by complexing a pulsed wave with a stationary continuous wave.
摘要翻译：通过等离子体CVD工艺形成膜的方法，其中在存在用于产生等离子体的电力具有脉冲波形的磁场的情况下产生高密度等离子体。电力通常由微波提供，并且脉冲波可以是具有两步峰值的复波，或者可以是通过使脉冲波与静止连续波相互合成而获得的复波。

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