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1. 发明授权

US6147241A Process for the preparation of organosilicon-disulfanes 失效
标题翻译：制备有机硅二硫化物的方法
公开(公告)号：US6147241A
公开(公告)日：2000-11-14
申请号：US417897
申请日：1999-10-14
申请人： Rudolf Michel , Jorg Munzenberg , Carl Van Der Auwera
发明人： Rudolf Michel , Jorg Munzenberg , Carl Van Der Auwera
IPC分类号： C07F7/02 , C07F7/18 , C08F7/08
CPC分类号： C07F7/1892
摘要： Organosilicon-disulfanes are prepared by decomposing organosilicon thiocyanates with an alkali metal alcoholate.
摘要翻译：有机硅二硫化物通过用碱金属醇化物分解有机硅硫氰酸盐制备。

2. 发明授权

US08153836B2 Silsesquioxane compound mixture, hydrolyzable silane compound, making methods, resist composition, patterning process, and substrate processing 有权
标题翻译：倍半硅氧烷复合混合物，可水解硅烷化合物，制备方法，抗蚀剂组合物，图案化工艺和基材加工
公开(公告)号：US08153836B2
公开(公告)日：2012-04-10
申请号：US11860872
申请日：2007-09-25
申请人： Mutsuo Nakashima , Yoshitaka Hamada , Katsuya Takemura , Kazumi Noda
发明人： Mutsuo Nakashima , Yoshitaka Hamada , Katsuya Takemura , Kazumi Noda
IPC分类号： C08F7/21 , C08F7/08 , G03F7/075
CPC分类号： G03F7/0757 , C08G77/045 , C08G77/06 , G03F7/0397 , Y10S430/106
摘要： In a mixture of silsesquioxane compounds comprising silsesquioxane units having a side chain including a direct bond between a silicon atom and a norbornane skeleton and having a degree of condensation of substantially 100%, a dimethylene chain of the norbornane skeleton remote from the silicon bonded side is substituted with at least one substituent group other than hydrogen, and an isomer having a bulkier substituent group on the dimethylene chain at an exo position is present in a higher proportion.
摘要翻译：在包含具有包含硅原子和降冰片烷骨架之间的直接键合并具有大致100％的缩合度的侧链的倍半硅氧烷单元的硅倍半氧烷化合物的混合物中，远离硅键合侧的降冰片烷骨架的二亚甲基链是被除了氢以外的至少一个取代基取代，并且在外显位置上在二亚甲基链上具有较大取代基的异构体以更高的比例存在。

3. 发明授权

US6162888A Method of making silicone polyether copolymers having reduced odor 有权
标题翻译：制造具有降低气味的硅氧烷聚醚共聚物的方法
公开(公告)号：US6162888A
公开(公告)日：2000-12-19
申请号：US312795
申请日：1999-05-17
申请人： Kenneth Michael Lee , Lenin James Petroff , William James Schulz, Jr.
发明人： Kenneth Michael Lee , Lenin James Petroff , William James Schulz, Jr.
IPC分类号： C08G77/38 , C08G65/336 , C08G77/06 , C08G77/46 , C08L71/02 , C08G77/04 , C08F7/08
CPC分类号： A61Q19/00 , A61K8/894 , C08G65/336 , C08G77/46 , C08L71/02 , C08L83/00
摘要： The present invention relates to a method of making a silicone polyether comprising (I) reacting a mixture comprising an olefin functional polyether, an organohydrogensiloxane, and a homogeneous transition metal hydrosilylation catalyst, and (II) subjecting the product of (I) to hydrogen gas. The method of this invention reduces the amount of olefinic species present which are precursors to odorous compounds. Thus the method of this invention reduces the amount of odor in the silicone polyether product. These odors are objectionable, particularly in personal care applications.
摘要翻译：本发明涉及一种制备硅氧烷聚醚的方法，其包括（I）使包含烯烃官能的聚醚，有机氢硅氧烷和均相的过渡金属氢化硅烷化催化剂的混合物反应，和（II）将（I）的产物。本发明的方法减少了作为无味化合物前体的存在的烯属物质的量。因此，本发明的方法降低了硅氧烷聚醚产品中的气味量。这些气味是令人反感的，特别是在个人护理应用中。

4. 发明专利

IN157914B "AN IMPROVED PROCESS FOR THE PREPARATION OF GRAFT COPOLYMERS OF VINYL AROMATIC COMPOUNDS" 未知
公开(公告)号：IN157914B
公开(公告)日：1986-07-19
申请号：IN243DE1982
申请日：1982-03-24
申请人： SHRI RAM IND RES INST
发明人： NIGAM JAI KRISHNA , DABHOLKAR DATTAPRASAD ACHYOT , UNNIKRISHNAN GEETA
IPC分类号： C08F7/08 , C08F33/00

5. 发明专利

IN140584B PREPARATION OF RIGID POROUS POLYMERIC MATERIAL OF UNCHARGED AND CHARGED TYPES FOR USE AS SORBENTS AND EXCHANGERS 未知
公开(公告)号：IN140584B
公开(公告)日：1976-12-04
申请号：IN1897CA1973
申请日：1973-08-17
申请人： COUNCIL SCIENT IND RES
发明人： RANGANATHAN S , GOVINDAN K , KRISHNASWAMY N
IPC分类号： C08F7/04 , C08F7/08

6. 发明专利

BR7307158D0 未知
公开(公告)号：BR7307158D0
公开(公告)日：1974-07-18
申请号：BR715873
申请日：1973-09-14
申请人： DU PONT
发明人： PROSHOW S
IPC分类号： C08K5/00 , C07F7/18 , C08J7/04 , C08K3/00 , C08K5/34 , C08K5/54 , C08K5/5419 , C08K5/5435 , C08L1/00 , C08L27/00 , C08L69/00 , C08L83/00 , C08L83/04 , C09D7/00 , C09D7/12 , C09D127/12 , C09D161/20 , C09D183/04 , C09K3/00 , C09K15/08 , C08F7/08 , C08F29/26 , C09D3/78
摘要： 1393488 Coated Products E I DU PONT DE NEMOURS & CO 14 Sept 1973 [15 Sept 1972] 43231/73 Heading B2E [Also in Division C3] Quartz, poly (methylinethacrylate) and polycarbonate sheets are coated with UV-screening compositions based on novel UV-absorbing silanes of the formula wherein R denotes a divalent hydrocarbon or oxygen-interrupted hydrocarbon radical of up to 10 carbon atoms, R 1 denotes an aliphatic hydrocarbon radical or acyl radical of less than 5 carbon atoms, or a radical of the formula (CH 2 CH 2 O) u Z wherein u is an integer of from 1 to 8 and Z is an aliphatic hydrocarbon radical of less than 5 carbon atoms, R 2 denotes a stable mono- or divalent hydroxyaromatic radical containing up to four aromatic rings and joined to oxygen through an aromatic carbon and absorbing light in the region of 2,500 to 4,000A, a is 0 or 1 and b is 1 or 2, and containing as further ingredients ethanolic polysilicic acid, tetrafluoroethylene/ 4-hydroxybutyl vinyl ether copolymers, n butanol tert-butanol mixed solvent, and optional amounts of glacial acetic acid, hexa- (methoxymethyl) melamine, a block copolymer of an alkylene oxide and dimethylsiloxane, methanolic potassium thiocyanate and 2, 5, 8, 15, 18, 21-hexaoxa-tricyclo (20.4.0.0 9 14 ) hexacosane.

7. 发明专利

CH437672A Siliziumhaltiges Material mit einem Überzug aus Siloxanen und Verfahren zu dessen Herstellung 未知
公开(公告)号：CH437672A
公开(公告)日：1967-06-15
申请号：CH1315462
申请日：1962-11-09
申请人： DOW CORNING
发明人： EDWIN PAUL PLUEDDEMANN
IPC分类号： C03C17/30 , C03C25/40 , C07F7/08 , C07F7/18 , C08G77/00 , C08G77/28 , C08G77/392 , C08F7/08

8. 发明授权

US5596116A Process for the preparation of silane polysulfides 失效
标题翻译：硅烷多硫化物的制备方法
公开(公告)号：US5596116A
公开(公告)日：1997-01-21
申请号：US526272
申请日：1995-09-11
申请人： Thomas E. Childress , Mark P. Bowman
发明人： Thomas E. Childress , Mark P. Bowman
IPC分类号： C07F7/18 , C08F7/08
CPC分类号： C07F7/1892
摘要： Sulfur-containing organosilicon compounds useful as coupling agents in vulcanizable rubbers to enhance various properties, including low rolling resistance for automobile tires, are prepared. Preferred compounds include .OMEGA., .OMEGA.'-bis (trialkoxysilylalkyl) polysulfides. In one embodiment, the reaction product of ethanolic sodium ethoxide and elemental sulfur is reacted with chloropropyltriethoxysilane. Alternatively, sodium metal is reacted with a mixture of ethanol and elemental sulfur, and then chloropropyltriethoxysilane. The use of sodium metal alcoholates provides an efficient and economical process.
摘要翻译：制备可硫化橡胶中用作偶联剂的硫磺有机硅化合物，以增强各种性能，包括汽车轮胎的低滚动阻力。优选的化合物包括OMEGA，OMEGA'-双（三烷氧基甲硅烷基烷基）多硫化物。在一个实施方案中，乙醇钠和元素硫的反应产物与氯丙基三乙氧基硅烷反应。或者，金属钠与乙醇和元素硫的混合物反应，然后与氯丙基三乙氧基硅烷反应。使用金属醇钠提供了一种有效和经济的过程。

9. 发明授权

US5329036A (alpha, omega)phenylethynyl siloxane monomers, oligomers, and polymers thereof 失效
标题翻译：（α，ω）苯乙炔基硅氧烷单体，低聚物及其聚合物
公开(公告)号：US5329036A
公开(公告)日：1994-07-12
申请号：US939326
申请日：1992-09-02
申请人： Thomas K. Dougherty , William E. Elias
发明人： Thomas K. Dougherty , William E. Elias
IPC分类号： C07F7/08 , C07F7/18 , C08F38/00 , C08F290/00 , C08F299/08 , C08G77/04 , C08G77/20 , C08G77/22 , C08G77/455 , C08F7/08
CPC分类号： C07F7/0896 , C07F7/0836 , C07F7/0847 , C07F7/1844 , C08G77/045 , C08G77/20 , C08G77/455
摘要： Novel acetylene-terminated silicone monomers with (a) silane (Si--H) functionalities, (b) silanol (Si--OH) functionalities, or (c) (alpha,omega)phenylethynyl terminated siloxanes, and a novel synthetic route. The (alpha,omega)phenylethynyl-terminated siloxane monomers are prepared, starting with 1,3-bromobenzene, which is converted to 3-TMS-ethynylbromobenzene, where TMS represents the trimethylsilyl group, by reacting 1,3-dibromobenzene with trimethylsilylacetylene and triethylamine in the presence of a palladium catalyst. The 3-bromo-TMS protected phenyl acetylene is then reacted with an alkyllithium compound, such as n-butyllithium, or with magnesium to form the corresponding lithio or Grignard compound, respectively, followed by reaction with a halogenated compound, such as chlorodimethylsilane, to form 3-trimethylsilyl-ethynylphenyldimethyl silane. Next, the TMS protected ethynylphenyl silane is subjected to deprotection and methanolysis of the Si--H bond to form 3-ethynylphenyldimethyl methoxy silane, employing methanol. This silane is then hydrolyzed to form the corresponding silanol. Finally, the silanol is then condensed by known methods to form the disiloxane. The disiloxane monomer can be reacted with a cyclic siloxane, having .gtoreq.3 silicon atoms, each independently substituted with hydrogen, C.sub.1 to C.sub.6 alkyl, phenyl, or phenyl substituted with one or more alkyl or halogen groups, to form oligomers. Both monomers and oligomers form thermoset polymers by heating to a temperature of at least about 250.degree. C.
摘要翻译：具有（a）硅烷（Si-H）官能团，（b）硅烷醇（Si-OH）官能团或（c）（α，ω））苯基乙炔基封端的硅氧烷的新型乙炔封端的有机硅单体和新的合成路线。制备（α，ω）苯基乙炔基封端的硅氧烷单体，通过1,3-二溴苯与三甲基甲硅烷基乙炔和三乙胺反应，由1,3-溴苯转化成3-TMS-乙炔基溴苯，其中TMS代表三甲基甲硅烷基在钯催化剂存在下。然后将3-溴-TT保护的苯基乙炔与烷基锂化合物如正丁基锂或与镁反应，分别形成相应的锂或格利雅化合物，随后与卤代化合物如氯二甲基硅烷反应，形成3-三甲基甲硅烷基 - 乙炔基苯基二甲基硅烷。接着，使用甲醇对TMS保护的乙炔基苯基硅烷进行Si-H键的去保护和甲醇分解以形成3-乙炔基苯基二甲基甲氧基硅烷。然后将该硅烷水解形成相应的硅烷醇。最后，通过已知的方法使硅烷醇缩合形成二硅氧烷。二硅氧烷单体可与具有大于或等于3个硅原子的环状硅氧烷，各自独立地被氢取代，C1至C6烷基，苯基或被一个或多个烷基或卤素基团取代的苯基，以形成低聚物。单体和低聚物通过加热至至少约250℃的温度形成热固性聚合物

10. 发明授权

US4138421A Process for the polymerization of allyl halides to produce poly(allylsilicoformate) polymers 失效
标题翻译：用于烯丙基卤化物聚合以生产聚（烯丙基二甲基丙烯酸酯）聚合物的方法
公开(公告)号：US4138421A
公开(公告)日：1979-02-06
申请号：US849853
申请日：1977-11-09
申请人： David H. Blount
发明人： David H. Blount
IPC分类号： C08F2/00 , C08F4/16 , C08F8/12 , C08F14/14 , C08F7/08
CPC分类号： C08F14/14 , C08F8/26 , C08F8/42
摘要： Allyl halides are polymerized by a catalyst, silicic or silicoformic acids, to produce poly(allyl halide) polymer and poly(allyl alcohol) polymer.
摘要翻译：烯丙基卤化物通过催化剂，硅酸或硅酸聚合，生成聚（烯丙基卤）聚合物和聚（烯丙醇）聚合物。

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