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1. 发明授权

US06818768B2 Mixtures of triazine derivatives free from polyalkylene oxide 失效
标题翻译：不含聚环氧烷的三嗪衍生物的混合物
公开(公告)号：US06818768B2
公开(公告)日：2004-11-16
申请号：US10205001
申请日：2002-07-25
申请人： Manfred Rätzsch , Martin Burger , Manfred Arnold , Willy Frank
发明人： Manfred Rätzsch , Martin Burger , Manfred Arnold , Willy Frank
IPC分类号： C07D25170
CPC分类号： C07D251/46 , C07D251/42
摘要： Mixtures of triazine derivatives free from polyalkylene oxide Mixtures of triazine derivatives free from polyalkylene oxide are produced from 20 to 70 percent by weight of triazine derivatives with hydroxyalkyl amino groups and 80 to 30 percent by weight of triazine derivatives with bis(hydroxyalkyl) imino groups by catalytic reaction of alkylpropylene oxides with triazine derivatives at a melamine derivative/alkylpropylene oxide molar ratio of 1:1.5 to 1:10 in the presence of metal alkyls, metal hydrides, metal alcoholates and/or metal alkylamides as catalysts. The triazine derivative/hydroxy group mixtures free from polyalkylene oxide are particularly suited for producing plastic materials, flame retardants, additives, pharmaceuticals, textile auxiliaries, and paints or finishes.
摘要翻译：不含聚环氧烷烃的三嗪衍生物的混合物由20至70重量％的具有羟基烷基氨基的三嗪衍生物和80至30重量％的具有双（羟基烷基）亚氨基的三嗪衍生物与双（羟基烷基）亚氨基的三嗪衍生物通过在金属烷基，金属氢化物，金属醇化物和/或金属烷基酰胺作为催化剂的存在下，烷基丙烯氧化物与三嗪衍生物在三聚氰胺衍生物/烷基氧化丙烯摩尔比为1:1.5至1:10的催化反应。三嗪衍生物/羟基不含聚环氧烷的组合混合物特别适用于生产塑料材料，阻燃剂，添加剂，药物，纺织助剂以及涂料或表面处理剂。

2. 发明授权

US06297377B1 Benzocycle-substituted triazine and pyrimidine ultraviolet light absorbers 失效
标题翻译：苯并环取代三嗪和嘧啶紫外光吸收剂
公开(公告)号：US06297377B1
公开(公告)日：2001-10-02
申请号：US09335790
申请日：1999-06-18
申请人： Ram B. Gupta , Dennis J. Jakiela , Robert G. Fischer
发明人： Ram B. Gupta , Dennis J. Jakiela , Robert G. Fischer
IPC分类号： C07D25170
CPC分类号： C07D251/24 , C08K5/3492
摘要： This invention relates generally to benzocycle-substituted pyrimidines and triazines and the use thereof to protect against degradation by environmental forces, inclusive of ultraviolet light, actinic radiation, oxidation, moisture, atmospheric pollutants and combinations thereof. The new class of benzocycle-substituted pyrimidines and triazines comprises a benzocycle attached to the triazine or pyrimidine ring, and preferably an additional aryl ring containing a hydroxyl group, either free or blocked to form a latent stabilizer, ortho- to the point of attachment to the triazine or pyrimidine ring. These materials may, under the appropriate circumstances, be bonded to formulations comprising coatings, polymers, resins, organic compounds and the like via reaction of the bondable functionality with the materials of the formulation. A method for stabilizing a material by incorporating such benzocycle-substituted pyrimidines and triazines is also disclosed.
摘要翻译：本发明一般涉及苯并环取代的嘧啶和三嗪及其用于防止包括紫外光，光化辐射，氧化，水分，大气污染物及其组合在内的环境力降解的用途。新类型的苯并环取代的嘧啶和三嗪包括与三嗪或嘧啶环连接的苯并环，并且优选含有游离或封闭以形成潜稳定剂的羟基的另外的芳环，三嗪或嘧啶环。这些材料可以在适当的情况下通过可结合的官能团与制剂的材料的反应与包含涂料，聚合物，树脂，有机化合物等的制剂结合。还公开了通过掺入这种苯并环取代的嘧啶和三嗪来稳定材料的方法。

3. 发明授权

US06331626B1 Triazinylaminostilbene compounds 有权
标题翻译：三嗪基氨基芪化合物
公开(公告)号：US06331626B1
公开(公告)日：2001-12-18
申请号：US09666768
申请日：2000-09-21
申请人： Peter Rohringer , André Geoffroy , Andreas Burkhard , Erwin Marti , Werner Schreiber , Josef Zelger
发明人： Peter Rohringer , André Geoffroy , Andreas Burkhard , Erwin Marti , Werner Schreiber , Josef Zelger
IPC分类号： C07D25170
CPC分类号： C07D251/68 , C09B67/0025 , D06L4/621 , Y10S8/919
摘要： The present invention provides a hydrate of the 4,4′-di-triazinylamino-2,2′-di-sulfostilbene compound having the formula: in which M and M1 independently represent hydrogen, an alkaline-, an alkaline earth metal or ammonium, x is a number within the range of from 1 to 30, and the crystal form of the hydrate (I) being characterised by an X-ray diffraction pattern which is essentially as set out in the accompanying FIGS. 1 to 11; or a mixture containing one or more of the hydrates of the 4,4′-di-triazinylamino-2,2′-di-sulfostilbene compound having the formula (I); processes for the preparation of the new hydrates; and the use of the new hydrates for the preparation of concentrated aqueous formulations of fluorescent whitening agents.
摘要翻译：本发明提供了具有下式的4,4'-二 - 三嗪基氨基-2,2'-二磺基芪化合物的水合物：其中M和M1独立地表示氢，碱金属，碱土金属或铵， x是1至30范围内的数字，并且水合物（I）的晶体形式的特征在于X射线衍射图，其基本上如附图中所示。 1至11; 或含有一种或多种具有式（I）的4,4'-二 - 三嗪基氨基-2,2'-二磺基芪化合物的水合物的混合物; 新水合物的制备过程; 以及使用新的水合物来制备荧光增白剂的浓缩水性制剂。

4. 发明授权

US06307046B1 Method for modifying melamine derivatives 失效
标题翻译：改性三聚氰胺衍生物的方法
公开(公告)号：US06307046B1
公开(公告)日：2001-10-23
申请号：US09600122
申请日：2000-07-31
申请人： Norio Tanaka , Hiroyuki Kousaka , Yasuyuki Nakajima , Kouichi Masahashi , Takashi Kitabayashi
发明人： Norio Tanaka , Hiroyuki Kousaka , Yasuyuki Nakajima , Kouichi Masahashi , Takashi Kitabayashi
IPC分类号： C07D25170
CPC分类号： C07D251/70
摘要： The present invention provides a method for modifying melamine derivatives that can produce N-substituted melamine derivatives by introducing a substituent group to melamine or N-substituted melamine derivatives. The method is characterized by heating melamine or an N-substituted melamine derivative and an alcohol in the presence of a mixed catalyst comprising a hydrogenation catalyst and a dehydrogenation catalyst and hydrogen to allow reaction or heating melamine or an N-substituted melamine derivative and an alcohol in the presence of a hydrogenation catalyst and hydrogen with addition/coexistence of a metal to allow reaction. The compound groups obtained by introducing a substituent group to the amino group of melamine derivative with an alcohol by the method of the present invention can be used widely as intermediates of fine chemicals such as various agricultural chemicals, medicines, dyes, paints, etc. and as various resin materials and flame retardant materials.
摘要翻译：本发明提供了一种通过将取代基引入三聚氰胺或N-取代的三聚氰胺衍生物来修饰可以产生N-取代的三聚氰胺衍生物的三聚氰胺衍生物的方法。该方法的特征在于在包含氢化催化剂和脱氢催化剂和氢气的混合催化剂存在下加热三聚氰胺或N-取代的三聚氰胺衍生物和醇，以允许反应或加热三聚氰胺或N-取代的三聚氰胺衍生物和醇在氢化催化剂和氢气的存在下，加入/共存金属以允许反应。通过本发明的方法，通过用醇将三聚氰胺衍生物的氨基引入取代基而获得的化合物基团可广泛用作各种农药，药物，染料，油漆等精细化学品的中间体，以及作为各种树脂材料和阻燃材料。

5. 发明授权

US06570011B1 Method for producing a stabilized aqueous alkali metal-2-hydroxy-4,6-dichloro-s-triazine solution and the use thereof 失效
标题翻译：稳定的碱金属碱金属-2-羟基-4,6-二氯-s-三嗪溶液的制备方法及其用途
公开(公告)号：US06570011B1
公开(公告)日：2003-05-27
申请号：US09786734
申请日：2001-03-08
申请人： Thomas Neumann
发明人： Thomas Neumann
IPC分类号： C07D25170
CPC分类号： C07D251/26 , G03C1/305
摘要： This invention relates to a process for the preparation of a stabilized aqueous alkali metal-2-hydroxy-4,6-dichloro-s-triazine (AHDT) solution, which entails starting at 5 to 40° C. with a solution containing either the corresponding alkali hydrogencarbonate, acetone, or a mixture thereof, and then, while cooling, adding cyanuric chloride and an alkali lye simultaneously in such a manner that the reaction temperature does not exceed 25° C. and the pH does not drop below 5.5, and during a subsequent stirring time of 2 to 30 hours adding either a very small quantity of alkali lauryl sulfate if the original starting solution contained hydrogencarbonate, or adding alkali hydrogencarbonate if exclusively acetone was used in the first reaction step, and then finally adding an alkali borate and/or a dialkali hydrogenphosphate and/or potassium hexacyanoferrate (II) as buffer. The pH, which should be ≧7.0 during the entire process, may, if necessary, be adjusted with an acid to a value between 8.0 and 9.5. The invention also provides for the same alkali metal to be used in all steps of the process. In particular as a result of the alkali hydrogencarbonate co-stabilizer, one obtains with this relatively simple process, after very short reaction times, AHDT solutions which remain stable for a long time and which do not release CO2 at any time during their synthesis, storage or use.
摘要翻译：本发明涉及一种制备稳定的碱金属水合羟基-4,6-二氯 - 均三嗪（AHDT）溶液的方法，该溶液需要在5至40℃下开始，使用含有相应的碱金属碳酸氢盐，丙酮或其混合物，然后在冷却下同时加入氰尿酰氯和碱液，使反应温度不超过25℃，pH不降至5.5以下，在随后的搅拌时间为2〜30小时的情况下，如果原始起始溶液含有碳酸氢盐，则添加非常少量的碱金属十二烷基硫酸盐，或者如果在第一反应步骤中仅使用丙酮，则加入碱金属碳酸氢盐，然后最后加入碱金属硼酸盐和/或二烷基磷酸氢盐和/或六氰基铁酸钾（II）作为缓冲液。如果需要，在整个过程中应该> 7.0的pH可以用酸调节至8.0和9.5之间的值。本发明还提供在该方法的所有步骤中使用的相同的碱金属。特别是作为碱式碳酸氢盐共稳定剂的结果，通过这种相对简单的方法得到，在非常短的反应时间后，长时间保持稳定且在其合成，储存期间的任何时间不释放二氧化碳的AHDT溶液或使用。

6. 发明授权

US06455695B1 Process for the preparation of alkylenebismelamines 失效
标题翻译：制备亚烷基二胺的方法
公开(公告)号：US06455695B1
公开(公告)日：2002-09-24
申请号：US09786419
申请日：2001-03-06
申请人： Hiroyuki Kousaka , Yasuyuki Nakajima
发明人： Hiroyuki Kousaka , Yasuyuki Nakajima
IPC分类号： C07D25170
CPC分类号： C07D251/70
摘要： The present invention provides a process which enables easy and inexpensive preparation of alkylenebismelamines usable as components for forming resin materials, particularly aminoplasts, and flame retardants. The present invention is a process for preparation of alkylenebismelamines wherein the alkylene is a linear or branched C2-10 one by reacting an alkylenediamine wherein the alkylene is a linear or branched C2-10 one with melamine in the presence of an acidic catalyst under heating, characterized in that the amount of melamine is at least twice that of the alkylenediamine by mole.
摘要翻译：本发明提供一种能够容易且廉价地制备可用作形成树脂材料，特别是氨基塑料和阻燃剂的组分的亚烷基二胺。本发明是一种制备亚烷基双胺的方法，其中亚烷基是直链或支链C 2-10的亚烷基二胺，其中亚烷基是直链或支链C 2-10与三聚氰胺在酸性催化剂存在下加热，其特征在于三聚氰胺的量为亚烷基二胺的摩尔量的至少两倍。

7. 发明授权

US06288227B1 Solublized 2,6-dinaphthylaminotriazines 有权
标题翻译：溶解的2,6-二萘基氨基三嗪
公开(公告)号：US06288227B1
公开(公告)日：2001-09-11
申请号：US09679922
申请日：2000-10-05
申请人： Ramanuj Goswami , Jean M. Buongiorne , Mary E. Craver
发明人： Ramanuj Goswami , Jean M. Buongiorne , Mary E. Craver
IPC分类号： C07D25170
CPC分类号： G03C7/413 , C07D251/70 , G03C7/421
摘要： Compounds represented by Structure I wherein R is carboxy or sulfo, m is an integer of from 0 to 7 and n is an integer of from 2 to 5 as useful in concentrated aqueous photographic processing compositions.
摘要翻译：由R中的结构I表示的化合物是羧基或磺基，m是0-7的整数，n是2-5的整数，用于浓缩的水性摄影处理组合物。

8. 发明授权

US06797821B2 Phosphorus-containing flame-retardant hardeners, epoxy resins, advanced epoxy resins and cured epoxy resins 失效
标题翻译：含磷阻燃硬化剂，环氧树脂，先进的环氧树脂和固化的环氧树脂
公开(公告)号：US06797821B2
公开(公告)日：2004-09-28
申请号：US10066455
申请日：2002-01-30
申请人： Chun-Shan Wang , Jeng-Yueh Shieh , Ching Hsuan Lin
发明人： Chun-Shan Wang , Jeng-Yueh Shieh , Ching Hsuan Lin
IPC分类号： C07D25170
CPC分类号： C08G59/4021 , C08G59/504 , C08G59/621 , H05K1/0326
摘要： The present invention discloses an active-hydrogen-containing phosphorus compound for cross-linking a resin and for imparting flame-retardancy to the cured resin, and in particular to a cured frame-retardant epoxy resin prepared by reacting the hardener with a di- or poly-functional epoxy resin via an addition reaction between the active hydrogen and the epoxide group. The present invention also discloses an epoxy resin made from the active-hydrogen-containing phosphorus compound and epihalohydrin.
摘要翻译：本发明公开了一种用于交联树脂并赋予固化树脂阻燃性的含活性氢的磷化合物，特别是固化的阻燃环氧树脂，其通过使硬化剂与二 - 或二 - 多官能环氧树脂通过活性氢和环氧基团之间的加成反应。本发明还公开了由含活性氢的磷化合物和表卤代醇制成的环氧树脂。

9. 发明授权

US06469165B1 Process for preparation of polyaminotriazines 失效
标题翻译：聚氨基三嗪的制备方法
公开(公告)号：US06469165B1
公开(公告)日：2002-10-22
申请号：US08363780
申请日：1994-12-27
申请人： Kenji Kimura , Shinya Tanaka , Manji Sasaki
发明人： Kenji Kimura , Shinya Tanaka , Manji Sasaki
IPC分类号： C07D25170
CPC分类号： C07D401/14
摘要： Polyaminotriazines represented by formula (I) can be prepared by conducting a reduction alkylamination of a tetramethylpiperidone with a diamine represented by formula (IIb), NH2—R—NH2, in the presence of a hydrogenating catalyst, removing the catalyst upon completion of the reaction to obtain an unrefined crude product (A); and, conducting a polycondensation reaction of the unrefined crude product (A) and a dichlorotriazine in an aromatic solvent and in the presence of an inorganic base.
摘要翻译：由式（I）表示的聚氨基三嗪可以通过在氢化催化剂存在下用式（IIb），NH 2 -R-NH 2代表的二胺进行四甲基哌啶酮的还原烷基化，在反应完成时除去催化剂得到未精制粗产物（A）; 并且在芳族溶剂中和在无机碱的存在下进行未精制粗产物（A）和二氯三嗪的缩聚反应。

10. 发明授权

US06288228B1 Triazine angiogenesis inhibitors 失效
标题翻译：三嗪血管生成抑制剂
公开(公告)号：US06288228B1
公开(公告)日：2001-09-11
申请号：US09680383
申请日：2000-10-05
申请人： Jack Henkin , Donald J. Davidson , George S. Sheppard , Keith W. Woods , Richard W. McCroskey
发明人： Jack Henkin , Donald J. Davidson , George S. Sheppard , Keith W. Woods , Richard W. McCroskey
IPC分类号： C07D25170
CPC分类号： C07D401/04 , C07D251/18 , C07D401/10 , C07D401/12 , C07D403/04 , C07D405/04 , C07D407/04 , C07D407/10 , C07D409/04 , C07D409/06 , C07D409/10 , C07D413/10 , C07D417/04 , C07D453/02
摘要： Compounds having Formula I or pharmaceutically acceptable salts or prodrugs thereof, are useful for treating pathological states which arise from or are exacerbated by angiogenesis. The invention also relates to pharmaceutical compositions comprising these compounds and to methods of inhibiting angiogenesis in a mammal.
摘要翻译：具有式I的化合物或其药学上可接受的盐或前药可用于治疗由血管发生引起或加重的病理状态。本发明还涉及包含这些化合物的药物组合物和抑制哺乳动物血管生成的方法。

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