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1. 发明专利

JPS5757450B1 失效
公开(公告)号：JPS5757450B1
公开(公告)日：1982-12-04
申请号：JP7546972
申请日：1972-07-27
申请人： ICI PLC
发明人： JON ANSONII FUEAAUEZAA , RONARUDO JEEMUSU DARUTON
IPC分类号： C07C7/00 , C07C7/177 , C10G29/16 , C10G53/04 , C10G61/04 , C07C15/02 , C07C61/02

2. 发明授权

US3634504A Alpha-monochlorination of carboxylic acids 失效
标题翻译：羧酸的羧酸单氯化
公开(公告)号：US3634504A
公开(公告)日：1972-01-11
申请号：US3634504D
申请日：1968-08-09
申请人： DOW CHEMICAL CO
发明人： YOUNG ARNOLD E
IPC分类号： C07C51/363 , C07C53/19 , C07C53/16 , C07C61/02 , C07C63/10
CPC分类号： C07C51/363 , C07C53/19
摘要： CARBOXYLIC ACIDS HAVING AT LEAST ONE HYDROGEN ATOM ATTACHED TO A CARBON ATOM THAT IS ALPHA TO THE CARBOXY GROUP ARE CHLORINATED TO GIVE THEIR ALPH-MONOCHLORINATED DERIVATIVES BY A PROCESS COMPRISING CONTACTING THEM WITH CHLORINE AT A TEMPERATURE BETWEEN 75 AND 225*C. WHILE IN THE PRESENCE OF A CATALYTIC AMOUNT OF TRICHLOROACETYL CHLORIDE, TRICHLOROACETIC ANHYDRIDE, TRIFLUOROACETYL CHLORIDE OR TRIFFUOROACETIC ANHYDRIDE.

3. 发明授权

US3629328A Purification of organic acids 失效
标题翻译：有机酸的纯化
公开(公告)号：US3629328A
公开(公告)日：1971-12-21
申请号：US3629328D
申请日：1969-05-20
申请人： CELANESE CORP
发明人： STAUTZENBERGER ADIN L , MACLEAN ALEXANDER F
IPC分类号： C07C51/42 , C07C61/02
CPC分类号： C07C51/42 , C07C63/26
摘要： PROCESS FOR PURIFYING RELATIVELY INSOLUBLE CARBOXYLIC ACIDS SUCH AS TEREPHTHALIC ACID BY TREATING THE INSOLUBLE ACID DISSOLVED IN AQUEOUS SOLUTIONS OF WEAK ACID SALTS, THE WEAK ACID SALTS BEING OF LITHIUM, MAGNESIUM, TERTIARY AMINES OR BEING TETRAALKYL QUATERNARY AMMONIUM SALTS. THE INSOLUBLE ACID IS RECOVERED IN THE FREE ACID FORM BY MERELY COOLING THE SOLUTION TO RECRYSTALLIZE THE INSOLUBLE ACID.

4. 发明专利

HK30180A A PROCESS FOR THE PREVENTION OF FORMATION OF FUR DEPOSITS ON HEATING SURFACES, AND A WATER ADDITIVE THEREFOR 未知
公开(公告)号：HK30180A
公开(公告)日：1980-06-06
申请号：HK30180
申请日：1980-05-29
申请人： GRILLO WERKE AG
发明人： DESAI N B
IPC分类号： C23F14/02 , C02F5/00 , C02F5/08 , C02F5/10 , C02F101/10 , C02B5/06 , C07C61/02 , C07C61/32 , C07D307/93
摘要： The reaction product of long-chain unsaturated hydrocarbons (fatty derivatives) with maleic acid anhydride and/or maleic acid is added to the salt-containing water of a thermal desalination installation to increase the solubility of the calcium and magnesium salts and prevent encrustation of heating surfaces thereby.

5. 发明专利

GB1551894A PROCESS FOR THE PREVENTION OF FORMATION ON FUR DEPOSITS ON HEATING SURFACES AND A WATER ADDITIVES THEREFOR 未知
公开(公告)号：GB1551894A
公开(公告)日：1979-09-05
申请号：GB3950677
申请日：1977-09-22
申请人： TAPROGGE L , GRILLO WERKE AG
IPC分类号： C23F14/02 , C02F5/00 , C02F5/08 , C02F5/10 , C02F101/10 , C02B5/06 , C07C61/02 , C07C61/32 , C07D307/93
摘要： The reaction product of long-chain unsaturated hydrocarbons (fatty derivatives) with maleic acid anhydride and/or maleic acid is added to the salt-containing water of a thermal desalination installation to increase the solubility of the calcium and magnesium salts and prevent encrustation of heating surfaces thereby.

6. 发明专利

GB1513913A PROSTANE DERIVATIVES 未知
公开(公告)号：GB1513913A
公开(公告)日：1978-06-14
申请号：GB2635275
申请日：1975-06-20
申请人： ICI LTD
IPC分类号： A61K31/12 , A61P1/00 , C07C67/00 , C07C401/00 , C07C405/00 , C07D307/935 , C07D309/12 , C07F9/40 , A61K31/00 , C07C61/02 , C07C69/74 , C07C177/00 , C07D307/93 , C07F7/18
摘要： 1513913 15 - Cycloalkylprostaglandins IMPERIAL CHEMICAL INDUSTRIES Ltd 27 May 1976 26352/75 Heading C2C [Also in Division C3] The invention comprises 15-cycloalkylprostaglandins of the formula wherein R 1 is carboxy, hydroxymethyl, (C 1-4 alkoxy)carbonyl or (C 1-4 alkoxy)methyl; R 2 and R 3 each are H or C 1-4 alkyl; X is ethylene or vinylene; Y is ethylene or trans-vinylene; n is 1, 2 or 3; and R 4 is C 1-4 alkyl or a phenyl, phenoxy, phenylthio or phenyl-(C 1-4 alkyl) radical in which the benzene ring is optionally substituted by one or more halogen atoms or nitro, phenyl, C 1-4 alkyl, C 1-4 alkoxy, C 1-4 haloalkyl or di(C 1-4 alkyl)amino radicals, provided that when n is 1 and R 4 is alkyl or optionally substituted phenyl, at least one of R 2 and R 7 is alkyl, and for those compounds in which R 1 is carboxy, the pharmaceutically or veterinarily acceptable salts thereof; and their preparation. The compounds are obtained by one of the following methods: (a) for those compounds wherein R 1 is carboxy, (C 1-4 alkoxy) carbonyl or (C 1-4 alkoxy) methyl and R 3 is H; the hydrolysis under acidic conditions of compounds of the Formula II wherein R 5 is carboxy (C 1-4 alkoxy carbonyl) or (C 1-4 alkoxy)methyl; (b) for those compounds in which R 1 is (C 1-4 alkyoxy) carbonyl, the esterification of the corresponding compounds in which R 1 is carboxy; (c) for those compounds in which R 1 is hydroxymethyl, the reaction of compounds of the Formula III wherein R 7 is OH, C 1-4 alkoxy, ureido or thioureido, with nitrites, in acetic acids; (d) for those compounds in which R 3 is C 1-4 alkyl, the hydrolysis of compounds of the Formula IV wherein R 3 is C 1-4 alkyl and R 8 , R 9 and R 10 each are C 1-4 alkyl; or the selective oxidation of compounds of the Formula V wherein R 3 is C 1-4 alkyl. The following intermediates are also prepared: 1 - butylcyclopentanecarboxylic acid and the methyl ester thereof; 1-butylcyclohexanecarboxylic acid and the methyl ester thereof; methyl 1 - (3 - chlorobenzyl) - cyclobutanecarboxylate; methyl 1-phenethylcyclobutanecarboxylate, methyl 1 - benzylcyclobutanecarboxylate; 1 - bromocyclobutanecarboxylic acid and its methyl ester; methyl 1 - (3 - chlorophenoxy)cyclobutanecarboxylate; methyl (2- chlorophenoxy)cyclobutanecarboxylate, methyl 1 - (3 - trifluoromethylphenoxy)cyclobutanecarboxylate; compounds of the Formula II above in which R 2 and R 3 are H, R 1 is carboxyl and Y is trans-vinylene; 4#À{3-[1-butylcyclopentyl (or cyclohexyl)] - 3 - oxo - 1 - transpropenyl} - 5α - (4 - phenylbenzoyloxy) - 3,3a#,- 4,5,6,6a# - hexahydro - 2H - cyclo - penta[b]- furan - 2 - one; 4# - {3 - [1 - butylcyclopentyl (or cyclohexyl)] - 3 - hydroxy - 1 - trans - propenyl} - 5α - (4 - phenylbenzoyloxy) - 3,3a#,- 4,5,6,6α# - hexahydro - 2H - cyclopenta[b]furon- 2 - one; 4# - {3 - [1 - butylcyclopentyl (or cyclohexyl)] - 3 - hydroxy - 1 - trans - propenyll - 5α- hydroxy - 3,3a#,4,5,6,6a# - hexahydro - 2H- cyclopenta[b]furan - 2 - one and the bis(2- tetrahydropyronyl)ether thereof; 4# - 3 - {[1- butylcyclopentyl (or cyclohexyl) - 3 - (tetrahydropyran - 2 - yloxy] - 1 - trans -propenyl}- 3,3a#,4,5,6,6a# - hexahydro - 2H - cyclopenta- [b]furan - 2 - ol; and the 11,15 - bis(2 - tetrahydropyranyl) ethers of compounds of the Formula V in which R 2 and R 3 are both H, Y is trans-vinylene and R 1 is earboxy; Dimethyl 2 - (1 - butylcyclopentyl) - 2 - oxoethylphosphonate and diisopropyl 2 - ( 1- butylcyclohexyl) - 2 - oxoethylphosphonate are prepared by reacting the appropriate dialkyl methylphosphonate with methyl 1-butylcyclopentane carboxylate and methyl 1-butylcyolohexanecarboxylate respectively in the presence of butyllithium. Pharmaceutical compositions, suitable for oral administration contain the above prostaglandins or salts thereof together with pharmaceutically or veterinarily acceptable diluents or carriers. The compounds inhibit gastric acid production in mammals

7. 发明专利

HU168443B 未知
公开(公告)号：HU168443B
公开(公告)日：1976-04-28
申请号：HUSE001720
申请日：1974-04-10
IPC分类号： A01N35/06 , A01N53/00 , C07C45/00 , C07C45/63 , C07C49/457 , C07C49/477 , C07C49/647 , C07C49/657 , C07C49/687 , C07C49/697 , C07C51/00 , C07C61/04 , C07C61/12 , C07C61/35 , C07C61/39 , C07C67/00 , C07C61/02

8. 发明专利

GB1323183A CYCLOPROPANE ESTERS AND ACIDS THEREOF 未知
公开(公告)号：GB1323183A
公开(公告)日：1973-07-11
申请号：GB1323183D
申请日：1971-01-14
申请人： BDH PHARMACEUTICALS LTD
IPC分类号： C07C67/00 , A61K20060101 , C07C20060101 , C07C51/00 , C07C61/04 , C07C69/00 , C07C69/74 , C07C61/02
摘要： 1323183 Cyclopropane esters and acids thereof BDH PHARMACEUTICALS Ltd 22 Dec 1971 [14 Jan 1971] 1874/71 Heading C2C Dicyclopropanecarboxylic acids and esters thereof of formula wherein X represents a C 1-6 alkyl group or an aryl group and R represents a hydrogen atom or a C 1-6 alkyl group, optionally substituted by a C 1-6 alkoxy group, or represents a C 3-6 cycloalkyl group or an aryl group, and Hal represents a halogen atom are prepared by subjecting an ester of formula in which X and R have the above-stated meanings to the effect of a dihalocarbene forming reaction mixture in the presence of a strong base, if desired with subsequent hydrolysis of the ester to form the acid. The invention also comprises compounds of the above formula in which X represents a (C 1-6 ) alkyl group, or an aryl group and R represents (C 1-6 ) alkyl group substituted by (C 1-6 ) alkoxy group, or represents a (C 3-6 ) cycloalkyl group or represents an aryl group and Hal represents a halogen atom.

9. 发明专利

CH425773A Procédé de préparation d'un monoester de l'acide camphorique 未知
公开(公告)号：CH425773A
公开(公告)日：1966-12-15
申请号：CH516264
申请日：1964-04-21
申请人： ZAMBELETTI SPA L
发明人： GIANI MARIO DR , MOLTENI LUIGI DR
IPC分类号： A61K31/21 , C07C61/02

10. 发明专利

FI55328C 未知
公开(公告)号：FI55328C
公开(公告)日：1979-07-10
申请号：FI167173
申请日：1973-05-23
申请人： SUMITOMO CHEMICAL CO
发明人： SUZUKI YOSHIO , MINAI MASAYOSHI , HAMMA NORITAKA , MURAYAMA EIICHI , AONO SHUNJI
IPC分类号： C07C62/08 , A61K20060101 , A61K31/19 , A61K31/215 , A61P9/10 , A61P29/00 , C07C20060101 , C07C51/00 , C07C61/00 , C07C61/06 , C07C61/08 , C07C61/12 , C07C62/34 , C07C63/00 , C07C67/00 , C07C69/66 , C07C69/74 , C07C69/757 , C07C69/76 , C07C61/02

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