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    • 6. 发明申请
    • ELECTROANALYTICAL, DROPPING MERCURY ELECTRODE CELL
    • 电解,电镀汞电极
    • WO1996035117A1
    • 1996-11-07
    • PCT/EP1996001794
    • 1996-04-30
    • RDC - RAFAEL DEVELOPMENT CORPORATION LTD.BRAUN, Ori, JosephYARNITZKY, Chaim, Noah
    • RDC - RAFAEL DEVELOPMENT CORPORATION LTD.BRAUN, Ori, Joseph
    • G01N27/34
    • G01N27/34
    • An electroanalytical, voltammetric cell, comprises: a) a cell body housing, in addition to a reference electrode, a working electrode and, in its lowermost portion, a counter-electrode; b) means for removing oxygen from the sample solution; c) means for feeding the sample solution to said deoxygenation means, means for feeding a stream of an inert gas to said deoxygenation means, and means for causing said solution to flow in said deoxygenation means, whereby oxygen is removed therefrom by contact with said inert gas; d) a means for removing said inert gas from said deoxygenation means after deoxygenation of the sample solution; e) an inlet for the deoxygenated sample solution provided in said cell body in the space between said working electrode and said counter-electrode; f) an exit for the sample solution provided in said cell body at a level above said working electrode; and g) vacuum and/or pressure means for causing said sample solution to flow to said exit, to be discharged from the cell above said working electrode, thus assuring that the space between said working electrode and said counter-electrode is constantly filled with said sample solution.
    • 一种电分析伏安电池,包括:a)电池体,除了参考电极外,还包括工作电极,并且在其最下部分包含反电极; b)从样品溶液中除去氧气的装置; c)用于将样品溶液供给到所述脱氧装置的装置,用于将惰性气体流输送到所述脱氧装置的装置,以及用于使所述溶液在所述脱氧装置中流动的装置,由此通过与所述惰性气体接触除去氧气。 加油站; d)在样品溶液脱氧后从所述脱氧装置中除去所述惰性气体的方法; e)在所述工作电极和所述对电极之间的空间中设置在所述电池体中的脱氧样品溶液的入口; f)设置在所述电池体内的样品溶液在所述工作电极上方的出口; 以及g)用于使所述样品溶液流到所述出口的真空和/或压力装置,以从所述工作电极上方的单元排出,从而确保所述工作电极和所述对电极之间的空间始终被所述 样品溶液。