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1. 发明公开

CN104781425A 用于淬灭生物质原料水解反应的瞬时冷却失效
公开(公告)号：CN104781425A
公开(公告)日：2015-07-15
申请号：CN201380056462.9
申请日：2013-11-08
申请人：瑞恩麦特克斯股份有限公司
发明人：安德斯·卡利尤斯 , 安德列亚斯·格拉姆 , 戈兰·卡尔森 , 赫伊屈尔·约翰内松 , 托尔斯滕·沃纳
IPC分类号： C13K1/02 , B01J3/00 , C07H1/08 , C12P7/10
CPC分类号： C13K1/02 , B01J3/006 , B01J2203/00 , Y02E50/16
摘要：本发明描述了用于淬灭一种生物质原料的水热、稀酸水解反应的一种方法，其中通过一种水性单体和/或低聚体糖混合物的瞬时冷却来减缓或终止该水性单体和/或低聚体糖混合物的降解，并且其中该瞬时冷却保证通过一种正在形成的蒸汽流除去一部分已溶解且具挥发性的降解副产物，并且其中将一种木质素组分，如果存在的话，固化为具有良好脱水特性的结构，允许之后通过分离去除木质素组分，所述方法产生了糖单体和/或低聚体的水解液。

2. 发明授权

CN104781425B 用于淬灭生物质原料水解反应的瞬时冷却失效
公开(公告)号：CN104781425B
公开(公告)日：2018-08-07
申请号：CN201380056462.9
申请日：2013-11-08
申请人：瑞恩麦特克斯股份有限公司
发明人：安德斯·卡利尤斯 , 安德列亚斯·格拉姆 , 戈兰·卡尔森 , 赫伊屈尔·约翰内松 , 托尔斯滕·沃纳
IPC分类号： C13K1/02 , B01J3/00 , C07H1/08 , C12P7/10
CPC分类号： C13K1/02 , B01J3/006 , B01J2203/00 , Y02E50/16
摘要：本发明描述了用于淬灭种生物质原料的水热、稀酸水解反应的种方法,其中通过种水性单体和/或低聚体糖混合物的瞬时冷却来减缓或终止该水性单体和/或低聚体糖混合物的降解,并且其中该瞬时冷却保证通过种正在形成的蒸汽流除去部分已溶解且具挥发性的降解副产物,并且其中将种木质素组分,如果存在的话,固化为具有良好脱水特性的结构,允许之后通过分离去除木质素组分,所述方法产生了糖单体和/或低聚体的水解液。

3. 发明授权

US08628802B2 Continuous process for microspheres production by using expanded fluids 失效
标题翻译：通过使用膨胀液进行微球生产的连续工艺
公开(公告)号：US08628802B2
公开(公告)日：2014-01-14
申请号：US12670852
申请日：2008-07-25
申请人： Ernesto Reverchon , Giovanna Della Porta
发明人： Ernesto Reverchon , Giovanna Della Porta
IPC分类号： A61K9/16 , B01F3/00 , B01J3/00
CPC分类号： A61K9/16 , A61K9/1635 , A61K9/1647 , A61K9/1694 , B01F3/0092 , B01F2003/0064 , B01J3/008 , B01J2203/00
摘要： The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an “expanded liquid” for the production of micro- and/or nano-particles or micro- and/or nano-spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds.The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.
摘要翻译：本发明涉及一种用于连续处理由“膨胀液体”辅助的乳液和/或微乳液的方法，用于生产微米和/或纳米颗粒或微米和/或纳米球体，其中含有一种或多种更活跃的成分。特别地，通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液接触，或者由通过压缩CO 2膨胀的液体的外部相形成的W / O乳液或多重乳液接触。膨胀的液体形成具有乳液分散相的溶液，并提取它，诱导所需溶解化合物颗粒的形成。该方法在逆流填充塔中进行，其中从顶部进料发泡乳液，同时从底部进料膨胀的液体。由于存在膨胀的液体，避免了在包装元件上产生的固体颗粒的任何沉积，从而防止任何柱堵塞。所需产物的微结构颗粒的悬浮液可以在塔的底部连续收集。

4. 发明申请

US20150292049A1 FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK 审中-公开
标题翻译：用于絮凝生物质饲料的水解反应的闪蒸冷却
公开(公告)号：US20150292049A1
公开(公告)日：2015-10-15
申请号：US14441427
申请日：2013-11-08
申请人： REAC FUEL AB
发明人： Anders Carlius , Andreas Gram , Göran Karlsson , Haukur Jóhannesson , Torsten Werner
IPC分类号： C13K1/02 , B01J3/00
CPC分类号： C13K1/02 , B01J3/006 , B01J2203/00 , Y02E50/16
摘要： The present invention describes a process for quenching a hydrothermal, dilute acid hydrolysis reaction of a biomass feedstock, wherein degradation of an aqueous monomer and/or oligomer sugar mixture is slowed down or stopped by flash cooling of the aqueous monomer and/or oligomer sugar mixture, and wherein the flash cooling ensures that a fraction of dissolved and volatile degradation byproducts are removed by a forming vapor stream, and wherein a lignin component, if present, is solidified into a structure with good de-watering characteristics, allowing for subsequent removal of the lignin component by separation, said process resulting in a hydrolyzed solution of sugar monomers and/or oligomers.
摘要翻译：本发明描述了一种用于淬灭生物质原料的水热，稀酸水解反应的方法，其中水性单体和/或低聚糖混合物的降解通过快速冷却含水单体和/或低聚糖混合物而降低或停止，并且其中所述闪蒸冷却确保通过形成蒸气流除去一部分溶解和挥发性降解副产物，并且其中木质素组分（如果存在）固化成具有良好脱水特性的结构，允许随后除去木质素组分通过分离，所述方法得到糖单体和/或低聚物的水解溶液。

5. 发明申请

US20100203145A1 CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS 失效
标题翻译：使用膨胀液生产微生物的连续工艺
公开(公告)号：US20100203145A1
公开(公告)日：2010-08-12
申请号：US12670852
申请日：2008-07-25
申请人： Ernesto Reverchon , Giovanna Della Porta
发明人： Ernesto Reverchon , Giovanna Della Porta
IPC分类号： A61K9/14 , A61K31/5415 , A61K31/405 , A61K31/196 , A61P29/00 , B01F13/00
CPC分类号： A61K9/16 , A61K9/1635 , A61K9/1647 , A61K9/1694 , B01F3/0092 , B01F2003/0064 , B01J3/008 , B01J2203/00
摘要： The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an “expanded liquid” for the production of micro- and/or nano-particles or micro- and/or nano-spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds.The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.
摘要翻译：本发明涉及一种用于连续处理由“膨胀液体”辅助的乳液和/或微乳液的方法，用于生产包含一种或多种微粒和/或纳米颗粒或微米和/或纳米球体的微粒和/或纳米球体，更活跃的成分。特别地，通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液接触，或者通过外部相形成的W / O乳液或多重乳液，其本身是通过压缩的CO 2膨胀的液体。膨胀的液体形成具有乳液分散相的溶液，并提取它，诱导所需溶解化合物颗粒的形成。该方法在逆流填充塔中进行，其中从顶部进料发泡乳液，同时从底部进料膨胀的液体。由于存在膨胀的液体，避免了在包装元件上产生的固体颗粒的任何沉积，从而防止任何柱堵塞。所需产物的微结构颗粒的悬浮液可以在塔的底部连续收集。

6. 发明公开

EP2185131A2 CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS 审中-公开
标题翻译：连续工艺生产微型BALLS深受广大液体的
公开(公告)号：EP2185131A2
公开(公告)日：2010-05-19
申请号：EP08790080.9
申请日：2008-07-25
申请人： Universita' Degli Studi di Salerno
发明人： REVERCHON, Ernesto , DELLA PORTA, Giovanna
IPC分类号： A61K9/16 , A61K31/00
CPC分类号： A61K9/16 , A61K9/1635 , A61K9/1647 , A61K9/1694 , B01F3/0092 , B01F2003/0064 , B01J3/008 , B01J2203/00
摘要： The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an 'expanded liquid' for the production of micro- and/or nano-particles or micro- and/or nano- spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds. The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.

7. 发明公开

EP2917376A1 FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK 审中-公开
标题翻译：闪电战冷却而进行淬火水解生物质原材料
公开(公告)号：EP2917376A1
公开(公告)日：2015-09-16
申请号：EP13853191.8
申请日：2013-11-08
申请人： Renmatix, Inc.
发明人： CARLIUS, Anders , GRAM, Andreas , KARLSSON, Göran , JÓHANNESSON, Haukur , WERNER, Torsten
IPC分类号： C13K1/02 , B01J3/00 , C07H1/08 , C12P7/10
CPC分类号： C13K1/02 , B01J3/006 , B01J2203/00 , Y02E50/16
摘要： The present invention describes a process for quenching a hydrothermal, dilute acid hydrolysis reaction of a biomass feedstock, wherein degradation of an aqueous monomer and/or oligomer sugar mixture is slowed down or stopped by flash cooling of the aqueous monomer and/or oligomer sugar mixture, and wherein the flash cooling ensures that a fraction of dissolved and volatile degradation byproducts are removed by a forming vapor stream, and wherein a lignin component, if present, is solidified into a structure with good de-watering characteristics, allowing for subsequent removal of the lignin component by separation, said process resulting in a hydrolyzed solution of sugar monomers and/or oligomers.

8. 发明公开

EP2917376A4 FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK 审中-公开
标题翻译： BLITZKÜHLUNGZUM ABSCHRECKEN EINER HYDROLYSEREAKING EINES BIOMASSEROHSTOFFS
公开(公告)号：EP2917376A4
公开(公告)日：2016-06-22
申请号：EP13853191
申请日：2013-11-08
申请人： RENMATIX INC
发明人： CARLIUS ANDERS , GRAM ANDREAS , KARLSSON GÖRAN , JÓHANNESSON HAUKUR , WERNER TORSTEN
IPC分类号： C13K1/02 , B01J3/00 , C07H1/08 , C12P7/10
CPC分类号： C13K1/02 , B01J3/006 , B01J2203/00 , Y02E50/16

9. 发明申请

WO2014074066A1 FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK 审中-公开
标题翻译：用于絮凝生物质饲料的水解反应的闪蒸冷却
公开(公告)号：WO2014074066A1
公开(公告)日：2014-05-15
申请号：PCT/SE2013/051324
申请日：2013-11-08
申请人： REAC FUEL AB
发明人： CARLIUS, Anders , GRAM, Andreas , KARLSSON, Göran , JÓHANNESSON, Haukur , WERNER, Torsten
IPC分类号： C13K1/02 , B01J3/00 , C07H1/08 , C12P7/10
CPC分类号： C13K1/02 , B01J3/006 , B01J2203/00 , Y02E50/16
摘要： The present invention describes a process for quenching a hydrothermal, dilute acid hydrolysis reaction of a biomass feedstock, wherein degradation of an aqueous monomer and/or oligomer sugar mixture is slowed down or stopped by flash cooling of the aqueous monomer and/or oligomer sugar mixture, and wherein the flash cooling ensures that a fraction of dissolved and volatile degradation byproducts are removed by a forming vapor stream, and wherein a lignin component, if present, is solidified into a structure with good de-watering characteristics, allowing for subsequent removal of the lignin component by separation, said process resulting in a hydrolyzed solution of sugar monomers and/or oligomers.
摘要翻译：本发明描述了一种用于淬灭生物质原料的水热，稀酸水解反应的方法，其中水性单体和/或低聚糖混合物的降解通过快速冷却含水单体和/或低聚糖混合物而降低或停止，并且其中所述闪蒸冷却确保通过形成蒸气流除去一部分溶解和挥发性降解副产物，并且其中木质素组分（如果存在）固化成具有良好脱水特性的结构，允许随后除去木质素组分通过分离，所述方法得到糖单体和/或低聚物的水解溶液。

10. 发明公开

EP3393651A1 VERFAHREN ZUR REGELUNG EINER CHEMISCHEN REAKTION UND VORRICHTUNG ZUR DURCHFÜHRUNG DES VERFAHRENS 有权转让
公开(公告)号：EP3393651A1
公开(公告)日：2018-10-31
申请号：EP16837975.8
申请日：2016-12-21
申请人： Ledwon, Anton , Heine, Christian , Heine, Andreas
发明人： LEDWON, Anton
IPC分类号： B01J19/28 , B01J19/00
CPC分类号： B01J19/087 , B01J19/002 , B01J19/008 , B01J19/18 , B01J19/1812 , B01J19/28 , B01J2203/00 , B01J2219/00162 , B01J2219/00488
摘要： The invention relates to a method for controlling a chemical reaction which creates a product, wherein at least one reactant that is present in a liquid phase is subjected to a pressure change. According to the invention, the minimum value of the pressure corresponds to a maximum 105 %, preferably a maximum 103 %, and especially preferably a maximum 101 % of the cavitation pressure of the reactant, without causing cavitation in the reactant. The invention provides a method which permits improved kinetic control, achieved by conducting a reaction close to the cavitation point, preferably supported by suitable frequencies, electrical fields and/or currents. Thus, kinetically controlled products, which as metastable, reactive compounds, are more valuable and more versatile in terms of their application, can thus be obtained with improved yields and at low cost. In particular, fuels can be refined cost-effectively in such a manner. In addition, the invention relates to an apparatus (201) which can be used to carry out the method according to the invention.

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